SU414785A3 - Способ получения этаноантраценов - Google Patents
Способ получения этаноантраценовInfo
- Publication number
- SU414785A3 SU414785A3 SU1118632A SU1118632A SU414785A3 SU 414785 A3 SU414785 A3 SU 414785A3 SU 1118632 A SU1118632 A SU 1118632A SU 1118632 A SU1118632 A SU 1118632A SU 414785 A3 SU414785 A3 SU 414785A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- ether
- chloro
- ethano
- solution
- dihydro
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 5
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 16
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 9
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 8
- 239000012280 lithium aluminium hydride Substances 0.000 description 6
- -1 lithium aluminum hydride Chemical compound 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 238000001816 cooling Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- XBDQKXXYIPTUBI-UHFFFAOYSA-N Propionic acid Substances CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 3
- 125000003118 aryl group Chemical group 0.000 description 3
- 229910052801 chlorine Inorganic materials 0.000 description 3
- 125000001309 chloro group Chemical group Cl* 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 229910052987 metal hydride Inorganic materials 0.000 description 3
- 150000004681 metal hydrides Chemical class 0.000 description 3
- 238000001953 recrystallisation Methods 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- KGMDODIDEQTIRA-UHFFFAOYSA-N 1,2-dihydrocyclobuta[a]anthracene Chemical compound C1=CC2=CC3=CC=CC=C3C=C2C2=C1CC2 KGMDODIDEQTIRA-UHFFFAOYSA-N 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 125000001664 diethylamino group Chemical group [H]C([H])([H])C([H])([H])N(*)C([H])([H])C([H])([H])[H] 0.000 description 2
- 125000002147 dimethylamino group Chemical group [H]C([H])([H])N(*)C([H])([H])[H] 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- JVLRJYDOJMOUNK-UHFFFAOYSA-N 2-anthracen-9-ylpropanoic acid Chemical compound C1=CC=C2C(C(C(O)=O)C)=C(C=CC=C3)C3=CC2=C1 JVLRJYDOJMOUNK-UHFFFAOYSA-N 0.000 description 1
- 241001331845 Equus asinus x caballus Species 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- QKIUAMUSENSFQQ-UHFFFAOYSA-N dimethylazanide Chemical compound C[N-]C QKIUAMUSENSFQQ-UHFFFAOYSA-N 0.000 description 1
- PSLIMVZEAPALCD-UHFFFAOYSA-N ethanol;ethoxyethane Chemical compound CCO.CCOCC PSLIMVZEAPALCD-UHFFFAOYSA-N 0.000 description 1
- 239000012259 ether extract Substances 0.000 description 1
- 125000001033 ether group Chemical group 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- MGJXBDMLVWIYOQ-UHFFFAOYSA-N methylazanide Chemical compound [NH-]C MGJXBDMLVWIYOQ-UHFFFAOYSA-N 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/16—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms acylated on ring nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1708665A CH448069A (de) | 1960-11-29 | 1965-12-10 | Verfahren zur Herstellung neuer Amine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU414785A3 true SU414785A3 (ru) | 1974-02-05 |
Family
ID=4422644
Family Applications (4)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1717552A SU424348A3 (enrdf_load_stackoverflow) | 1965-12-10 | 1966-12-10 | |
| SU1118632A SU414785A3 (ru) | 1965-12-10 | 1966-12-10 | Способ получения этаноантраценов |
| SU1717390A SU549077A3 (ru) | 1965-12-10 | 1971-11-24 | Способ получени аминоэтаноантраценов или их солей |
| SU1717378A SU549076A3 (ru) | 1965-12-10 | 1971-11-24 | Способ получени аминоэтаноантрацентов или их солей |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1717552A SU424348A3 (enrdf_load_stackoverflow) | 1965-12-10 | 1966-12-10 |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1717390A SU549077A3 (ru) | 1965-12-10 | 1971-11-24 | Способ получени аминоэтаноантраценов или их солей |
| SU1717378A SU549076A3 (ru) | 1965-12-10 | 1971-11-24 | Способ получени аминоэтаноантрацентов или их солей |
Country Status (11)
| Country | Link |
|---|---|
| AT (12) | AT273946B (enrdf_load_stackoverflow) |
| BE (3) | BE690940A (enrdf_load_stackoverflow) |
| BR (3) | BR6685268D0 (enrdf_load_stackoverflow) |
| DE (1) | DE1568355A1 (enrdf_load_stackoverflow) |
| DK (3) | DK130175B (enrdf_load_stackoverflow) |
| FR (6) | FR6355M (enrdf_load_stackoverflow) |
| GB (2) | GB1149557A (enrdf_load_stackoverflow) |
| GT (1) | GT197119100A (enrdf_load_stackoverflow) |
| NL (3) | NL6617369A (enrdf_load_stackoverflow) |
| SE (2) | SE324788B (enrdf_load_stackoverflow) |
| SU (4) | SU424348A3 (enrdf_load_stackoverflow) |
-
1966
- 1966-12-02 DE DE19661568355 patent/DE1568355A1/de active Pending
- 1966-12-09 AT AT173468A patent/AT273946B/de active
- 1966-12-09 AT AT1135266A patent/AT271459B/de active
- 1966-12-09 AT AT173968A patent/AT276364B/de active
- 1966-12-09 BE BE690940A patent/BE690940A/xx unknown
- 1966-12-09 BE BE690939D patent/BE690939A/xx unknown
- 1966-12-09 DK DK638766A patent/DK130175B/da unknown
- 1966-12-09 BR BR18526866A patent/BR6685268D0/pt unknown
- 1966-12-09 DK DK638866A patent/DK130176B/da unknown
- 1966-12-09 NL NL6617369A patent/NL6617369A/xx unknown
- 1966-12-09 AT AT173868A patent/AT272328B/de active
- 1966-12-09 DK DK638666A patent/DK130786B/da unknown
- 1966-12-09 NL NL6617367A patent/NL6617367A/xx unknown
- 1966-12-09 SE SE1690666A patent/SE324788B/xx unknown
- 1966-12-09 AT AT173568A patent/AT271461B/de active
- 1966-12-09 AT AT1135566A patent/AT272327B/de active
- 1966-12-09 SE SE1690766A patent/SE354850B/xx unknown
- 1966-12-09 AT AT196468A patent/AT273084B/de active
- 1966-12-09 BE BE690941D patent/BE690941A/xx unknown
- 1966-12-09 BR BR18526766A patent/BR6685267D0/pt unknown
- 1966-12-09 AT AT1135366A patent/AT272326B/de active
- 1966-12-09 BR BR18526666A patent/BR6685266D0/pt unknown
- 1966-12-09 AT AT196568A patent/AT273085B/de active
- 1966-12-09 NL NL6617368A patent/NL6617368A/xx unknown
- 1966-12-09 AT AT174168A patent/AT271463B/de active
- 1966-12-09 AT AT1966A patent/AT278766B/de not_active IP Right Cessation
- 1966-12-09 AT AT174068A patent/AT271462B/de active
- 1966-12-10 SU SU1717552A patent/SU424348A3/ru active
- 1966-12-10 SU SU1118632A patent/SU414785A3/ru active
- 1966-12-12 GB GB5555466A patent/GB1149557A/en not_active Expired
- 1966-12-12 GB GB5555366A patent/GB1143999A/en not_active Expired
-
1967
- 1967-03-02 FR FR97138A patent/FR6355M/fr not_active Expired
- 1967-03-02 FR FR97140A patent/FR6357M/fr not_active Expired
- 1967-03-02 FR FR97137A patent/FR6354M/fr not_active Expired
- 1967-03-02 FR FR97139A patent/FR6356M/fr not_active Expired
- 1967-03-02 FR FR97135A patent/FR6436M/fr not_active Expired
- 1967-03-02 FR FR97136A patent/FR6353M/fr not_active Expired
-
1971
- 1971-01-18 GT GT197119100A patent/GT197119100A/es unknown
- 1971-11-24 SU SU1717390A patent/SU549077A3/ru active
- 1971-11-24 SU SU1717378A patent/SU549076A3/ru active
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