SU373934A1 - - Google Patents
Info
- Publication number
- SU373934A1 SU373934A1 SU1461172A SU1461172A SU373934A1 SU 373934 A1 SU373934 A1 SU 373934A1 SU 1461172 A SU1461172 A SU 1461172A SU 1461172 A SU1461172 A SU 1461172A SU 373934 A1 SU373934 A1 SU 373934A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- methanol
- acetate
- distillation
- mol
- metal
- Prior art date
Links
- 238000000034 method Methods 0.000 claims description 14
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 84
- 238000004821 distillation Methods 0.000 claims 16
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims 12
- 229910052751 metal Inorganic materials 0.000 claims 12
- 239000002184 metal Substances 0.000 claims 12
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 claims 11
- -1 alkenyl alcohols Chemical class 0.000 claims 11
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims 10
- 239000003054 catalyst Substances 0.000 claims 8
- HVAMZGADVCBITI-UHFFFAOYSA-M pent-4-enoate Chemical compound [O-]C(=O)CCC=C HVAMZGADVCBITI-UHFFFAOYSA-M 0.000 claims 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 6
- 239000000203 mixture Substances 0.000 claims 6
- 238000004458 analytical method Methods 0.000 claims 5
- 238000009835 boiling Methods 0.000 claims 4
- PATYJMUHSCRQSS-UHFFFAOYSA-N 2,4,4-trimethylpent-1-enyl acetate Chemical class CC(=O)OC=C(C)CC(C)(C)C PATYJMUHSCRQSS-UHFFFAOYSA-N 0.000 claims 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims 3
- 150000004703 alkoxides Chemical class 0.000 claims 3
- 125000004432 carbon atom Chemical group C* 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 claims 3
- 238000006467 substitution reaction Methods 0.000 claims 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims 2
- 150000001298 alcohols Chemical class 0.000 claims 2
- 238000006136 alcoholysis reaction Methods 0.000 claims 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 238000005194 fractionation Methods 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- 150000003839 salts Chemical class 0.000 claims 2
- 239000002699 waste material Substances 0.000 claims 2
- GXDHCNNESPLIKD-UHFFFAOYSA-N 2-methylhexane Natural products CCCCC(C)C GXDHCNNESPLIKD-UHFFFAOYSA-N 0.000 claims 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims 1
- AEXMKKGTQYQZCS-UHFFFAOYSA-N 3,3-dimethylpentane Chemical compound CCC(C)(C)CC AEXMKKGTQYQZCS-UHFFFAOYSA-N 0.000 claims 1
- 101100057236 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) mus-21 gene Proteins 0.000 claims 1
- 101150100500 TEL1 gene Proteins 0.000 claims 1
- 229960000583 acetic acid Drugs 0.000 claims 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 150000002009 diols Chemical class 0.000 claims 1
- 239000000945 filler Substances 0.000 claims 1
- 238000004817 gas chromatography Methods 0.000 claims 1
- 229910052736 halogen Inorganic materials 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- 230000003301 hydrolyzing effect Effects 0.000 claims 1
- 238000002955 isolation Methods 0.000 claims 1
- GCICAPWZNUIIDV-UHFFFAOYSA-N lithium magnesium Chemical compound [Li].[Mg] GCICAPWZNUIIDV-UHFFFAOYSA-N 0.000 claims 1
- JILPJDVXYVTZDQ-UHFFFAOYSA-N lithium methoxide Chemical compound [Li+].[O-]C JILPJDVXYVTZDQ-UHFFFAOYSA-N 0.000 claims 1
- OTCKOJUMXQWKQG-UHFFFAOYSA-L magnesium bromide Chemical compound [Mg+2].[Br-].[Br-] OTCKOJUMXQWKQG-UHFFFAOYSA-L 0.000 claims 1
- 229910001623 magnesium bromide Inorganic materials 0.000 claims 1
- 238000005259 measurement Methods 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- 125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 claims 1
- BQZSFXARLMHSGX-UHFFFAOYSA-N oct-1-enyl acetate Chemical compound CCCCCCC=COC(C)=O BQZSFXARLMHSGX-UHFFFAOYSA-N 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 235000015927 pasta Nutrition 0.000 claims 1
- PGMYKACGEOXYJE-UHFFFAOYSA-N pentyl acetate Chemical compound CCCCCOC(C)=O PGMYKACGEOXYJE-UHFFFAOYSA-N 0.000 claims 1
- 230000000737 periodic effect Effects 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 239000001294 propane Substances 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 238000005292 vacuum distillation Methods 0.000 claims 1
- KNIUHBNRWZGIQQ-UHFFFAOYSA-N 7-diethoxyphosphinothioyloxy-4-methylchromen-2-one Chemical compound CC1=CC(=O)OC2=CC(OP(=S)(OCC)OCC)=CC=C21 KNIUHBNRWZGIQQ-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE1939142A DE1939142B2 (de) | 1969-08-01 | 1969-08-01 | Verfahren zur Herstellung primärer Alkenole |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| SU373934A1 true SU373934A1 (enrdf_load_stackoverflow) | |
| SU373934A3 SU373934A3 (enrdf_load_stackoverflow) | 1973-03-12 |
Family
ID=5741596
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1461172A SU373934A3 (enrdf_load_stackoverflow) | 1969-08-01 | 1970-07-21 |
Country Status (15)
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5845409B2 (ja) * | 1978-09-07 | 1983-10-08 | ジェイエスアール株式会社 | ジオ−ルの製造方法 |
| SA07280020B1 (ar) | 2006-02-02 | 2011-04-24 | شوا دينكو كيه. كيه. | طريقة تقطير ازيوتروبية |
| JP5530606B2 (ja) * | 2008-07-10 | 2014-06-25 | 国立大学法人 東京大学 | トリフェニレンカルボン酸エステルの製造方法 |
-
1969
- 1969-08-01 DE DE1939142A patent/DE1939142B2/de not_active Withdrawn
-
1970
- 1970-07-01 CH CH1000070A patent/CH542165A/de not_active IP Right Cessation
- 1970-07-06 LU LU61267D patent/LU61267A1/xx unknown
- 1970-07-06 ZA ZA704636A patent/ZA704636B/xx unknown
- 1970-07-16 RO RO63940A patent/RO58852A/ro unknown
- 1970-07-21 SU SU1461172A patent/SU373934A3/ru active
- 1970-07-27 JP JP45065093A patent/JPS4820524B1/ja active Pending
- 1970-07-28 AT AT687170A patent/AT299139B/de not_active IP Right Cessation
- 1970-07-29 NL NL7011240A patent/NL7011240A/xx unknown
- 1970-07-29 BE BE754095D patent/BE754095A/xx unknown
- 1970-07-30 GB GB36834/70A patent/GB1293035A/en not_active Expired
- 1970-07-30 ES ES382317A patent/ES382317A1/es not_active Expired
- 1970-07-30 PL PL1970142377A patent/PL79790B1/pl unknown
- 1970-07-31 FR FR7028467A patent/FR2057920A5/fr not_active Expired
- 1970-07-31 SE SE10561/70A patent/SE357959B/xx unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Kimel et al. | The rearrangement of allyl-type esters of β-keto acids | |
| US2165962A (en) | Production of alkylidene diethers or ether-esters | |
| US2571212A (en) | Preparation of ether-substituted unsaturated esters | |
| US8415496B2 (en) | Biobased polyesters | |
| SU373934A1 (enrdf_load_stackoverflow) | ||
| US3408388A (en) | Process for preparing esters of unsaturated alcohols from monoesters of saturated 2, 2, 4-trisubstituted-1, 3-diols | |
| JPS6348255B2 (enrdf_load_stackoverflow) | ||
| US2579411A (en) | Production of vinyl ethers | |
| US4278808A (en) | Method of preparing a 3-alkoxy-2-alkyl-propionic acid ester derivative and intermediate therefor | |
| WO2008092655A1 (en) | Process for preparing dienones | |
| US2920081A (en) | Production of 2, 5-dialkoxy-tetrahydrofuran | |
| CASON et al. | BRANCHED-CHAIN FATTY ACIDS. VII. SIMPLIFIED METHODS FOR PREPARING PURE BRANCHED-CHAIN ALCOHOLS AND HALIDES | |
| US3869517A (en) | Process for preparing hydroxy citronellal by saponification of the hydroxy ester | |
| DE69706528T2 (de) | Verfahren zur herstellung von 1,2-diacetoxy estern | |
| US3639445A (en) | Process for making substituted crotonates | |
| JP7434289B2 (ja) | モノビニルエーテルを製造する方法 | |
| US3057914A (en) | Process for the preparation of isobutyrate esters | |
| GB2061925A (en) | Cyclisation of y-chlorocarboxylic acid esters | |
| US7518003B2 (en) | Production process of tetrahydropyran compound and tetrahydropyran compound produced by the production process | |
| US2221275A (en) | Halo-aliphatic esters of 2-chloroallyl alcohol | |
| US3287372A (en) | Process and intermediates for manufacture of 2-(dialkylmethyl)-5-alkyl-2-cyclohexen-1-ones | |
| US4160109A (en) | Cyclohexene-(1)-dione-(3,6)-tetraalkyldiketals and process | |
| JPS62106060A (ja) | 純粋な塩素不含シクロプロパン−カルボン酸エステルの製造方法 | |
| JPH08225479A (ja) | モノビニルエーテルの製法 | |
| JP6424153B2 (ja) | ２−イソプロペニル−５−メチル−４−ヘキセン−１−イル３−メチル−２−ブテノエートの製造方法 |