SU278691A1 - - Google Patents

Info

Publication number

SU278691A1

SU278691A1 SU1337675A SU1337675A SU278691A1 SU 278691 A1 SU278691 A1 SU 278691A1 SU 1337675 A SU1337675 A SU 1337675A SU 1337675 A SU1337675 A SU 1337675A SU 278691 A1 SU278691 A1 SU 278691A1

Authority

SU

USSR - Soviet Union

Prior art keywords

reaction mixture

sulfur

iodine

sulfides

followed

Prior art date

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• 238000000034 method Methods 0.000 claims description 7
• 239000011541 reaction mixture Substances 0.000 claims description 5
• 229910052717 sulfur Inorganic materials 0.000 claims description 4
• OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 3
• NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 3
• PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims description 3
• 239000011593 sulfur Substances 0.000 claims description 3
• 150000001351 alkyl iodides Chemical class 0.000 claims description 2
• 238000009835 boiling Methods 0.000 claims 1
• 238000002955 isolation Methods 0.000 claims 1
• 238000005987 sulfurization reaction Methods 0.000 claims 1
• 150000003568 thioethers Chemical class 0.000 claims 1
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 12
• ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
• 238000006243 chemical reaction Methods 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 2
• 150000004763 sulfides Chemical class 0.000 description 2
• PIOZWDBMINZWGJ-UHFFFAOYSA-N trioctyl(sulfanylidene)-$l^{5}-phosphane Chemical compound CCCCCCCCP(=S)(CCCCCCCC)CCCCCCCC PIOZWDBMINZWGJ-UHFFFAOYSA-N 0.000 description 2
• UWLHSHAHTBJTBA-UHFFFAOYSA-N 1-iodooctane Chemical compound CCCCCCCCI UWLHSHAHTBJTBA-UHFFFAOYSA-N 0.000 description 1
• ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical group [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
• SEZQDNQSZRLJFH-UHFFFAOYSA-N C(CCCCCCCCCCCC)[PH2]=S Chemical class C(CCCCCCCCCCCC)[PH2]=S SEZQDNQSZRLJFH-UHFFFAOYSA-N 0.000 description 1
• PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 239000008139 complexing agent Substances 0.000 description 1
• 238000009833 condensation Methods 0.000 description 1
• 230000005494 condensation Effects 0.000 description 1
• 238000000605 extraction Methods 0.000 description 1
• 229910001385 heavy metal Inorganic materials 0.000 description 1
• 229910052740 iodine Inorganic materials 0.000 description 1
• 239000007788 liquid Substances 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• 229910000510 noble metal Inorganic materials 0.000 description 1
• 239000000575 pesticide Substances 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 229910052938 sodium sulfate Inorganic materials 0.000 description 1
• 235000011152 sodium sulphate Nutrition 0.000 description 1
• 235000010265 sodium sulphite Nutrition 0.000 description 1
• 239000007858 starting material Substances 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• OKQKDCXVLPGWPO-UHFFFAOYSA-N sulfanylidenephosphane Chemical compound S=P OKQKDCXVLPGWPO-UHFFFAOYSA-N 0.000 description 1
• 125000004434 sulfur atom Chemical group 0.000 description 1
• 238000003786 synthesis reaction Methods 0.000 description 1