SG10201803332YA - Molding for a hydrophobic zeolitic material and process for its production - Google Patents

Molding for a hydrophobic zeolitic material and process for its production

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Publication number
SG10201803332YA
SG10201803332YA SG10201803332YA SG10201803332YA SG10201803332YA SG 10201803332Y A SG10201803332Y A SG 10201803332YA SG 10201803332Y A SG10201803332Y A SG 10201803332YA SG 10201803332Y A SG10201803332Y A SG 10201803332YA SG 10201803332Y A SG10201803332Y A SG 10201803332YA
Authority
SG
Singapore
Prior art keywords
molding
zeolitic material
production
hydrophobic
iii
Prior art date
Application number
SG10201803332YA
Other languages
English (en)
Inventor
Andrei-Nicolae Parvulescu
Ulrich Müller
Hans-Jürgen Lützel
Joaquim Henrique Teles
Dominic Riedel
Bianca Seelig
Daniel Urbanczyk
Ulrike Wegerle
Michael Hesse
Andreas Walch
Volker Bendig
Veit Stegmann
Henning Althöfer
Boris Gaspar
Frank Stallmach
Anne Kristin Pusch
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=49486349&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=SG10201803332Y(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Se filed Critical Basf Se
Publication of SG10201803332YA publication Critical patent/SG10201803332YA/en

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    • B01J29/89Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B01J20/16Alumino-silicates
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    • B01J20/183Physical conditioning without chemical treatment, e.g. drying, granulating, coating, irradiation
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    • B01J35/40Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
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    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
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SG10201803332YA 2013-10-23 2014-10-22 Molding for a hydrophobic zeolitic material and process for its production SG10201803332YA (en)

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Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2701867T3 (es) 2014-10-14 2019-02-26 Basf Se Uso de hexadeca-8,15-dienal como producto químico aromático
WO2016128917A1 (en) 2015-02-12 2016-08-18 Basf Se Process for the preparation of a dealuminated zeolitic material having the bea framework structure
JP6741687B2 (ja) 2015-05-04 2020-08-19 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se メロナールの調製方法
WO2017009462A1 (en) 2015-07-15 2017-01-19 Basf Se Process for preparing an arylpropene
CN107848930A (zh) 2015-07-15 2018-03-27 巴斯夫欧洲公司 制备芳基丙烯的方法
EP3325457B1 (en) 2015-07-22 2020-01-01 Basf Se Process for preparing furan-2,5-dicarboxylic acid
CN117046513A (zh) * 2016-12-20 2023-11-14 巴斯夫欧洲公司 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途
EP3558516A1 (en) * 2016-12-20 2019-10-30 Basf Se A process for preparing an extrudable composition comprising a titanium-containing zeolitic material having framework type mww
US10780432B2 (en) * 2017-01-18 2020-09-22 Basf Se Process for preparing a molding comprising zinc and a titanium-containing zeolite
KR20210066913A (ko) * 2018-10-09 2021-06-07 바스프 에스이 골격 유형 mfi를 갖는 제올라이트 물질을 포함하는 몰딩
EP3872033A4 (en) 2018-10-25 2022-08-17 Tosoh Corporation PENTASIL ZEOLITE AND PRODUCTION PROCESS THEREOF
BR112021019270A2 (pt) * 2019-04-29 2022-01-04 Basf Se Moldagem química, processo para preparar uma moldagem química, usos de uma moldagem, de uma dispersão coloidal de sílica em água e da mistura, e, mistura
CN114929384A (zh) * 2019-12-19 2022-08-19 巴斯夫欧洲公司 钛硅酸盐沸石材料的连续合成、所述沸石材料、由其制备的模制品以及它们的用途
RU2734985C1 (ru) * 2020-05-21 2020-10-27 Федеральное государственное бюджетное учреждение науки "Федеральный исследовательский центр "Институт катализа им. Г.К. Борескова Сибирского отделения Российской академии наук" (ИК СО РАН, Институт катализа СО РАН) Способ приготовления катализатора и способ получения изопропилбензола (варианты)
JP2023540681A (ja) * 2020-08-04 2023-09-26 ビーエーエスエフ ソシエタス・ヨーロピア 2,2,4,6,6-ペンタメチル-1,2,5,6-テトラヒドロ-ピリミジンを生成するための不均一系触媒プロセス
TWI749754B (zh) * 2020-09-07 2021-12-11 國立宜蘭大學 金屬觸媒及其製法和用於處理丙酮之應用

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3066427B2 (ja) 1990-04-16 2000-07-17 東ソー株式会社 高強度a型ゼオライト成形体およびその製造法
DE4202671A1 (de) * 1991-05-27 1992-12-03 Degussa Formkoerper enthaltend dealuminierten zeolith y und das verfahren zu ihrer herstellung
DE19623609A1 (de) 1996-06-13 1997-12-18 Basf Ag Oxidationskatalysator und Verfahren zur Herstellung von Epoxiden aus Olefinen, Wasserstoff und Sauerstoff unter Verwendung des Oxidationskatalysators
DE19723751A1 (de) * 1997-06-06 1998-12-10 Basf Ag Formkörper und Verfahren zu dessen Herstellung
BE1011577A3 (fr) 1997-11-27 1999-11-09 Solvay Catalyseur d'epoxydation, son utilisation et procede d'epoxydation en presence de catalyseur.
WO2000066263A1 (en) * 1999-05-05 2000-11-09 Exxon Chemical Patents Inc. Zeolite bound catalyst containing at least three different zeolites; use for hydrocarbon conversion
DE19939416A1 (de) 1999-08-20 2001-02-22 Basf Ag Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs
US20040054199A1 (en) 2002-09-17 2004-03-18 Basf Aktiengesellschaft Process for epoxidation and catalyst to be used therein
DE10320634A1 (de) 2003-05-08 2004-11-18 Basf Ag Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid
DE10321876A1 (de) 2003-05-15 2004-12-02 Bayer Materialscience Ag Katalysator
KR100599251B1 (ko) * 2003-09-20 2006-07-13 에스케이 주식회사 디메틸에테르 합성용 촉매와 촉매의 제조방법
DE10356184A1 (de) 2003-12-02 2005-07-07 Basf Ag Zeolithisches Material vom Pentasil-Strukturtyp, seine Herstellung und seine Verwendung
US7589041B2 (en) * 2004-04-23 2009-09-15 Massachusetts Institute Of Technology Mesostructured zeolitic materials, and methods of making and using the same
WO2007033934A2 (de) 2005-09-20 2007-03-29 Basf Se Verfahren zur ermittlung der tortuosität, katalysatorträger, katalysator und verfahren zur dehydrierung von kohlenwasserstoffen
JP5050466B2 (ja) * 2006-09-21 2012-10-17 三菱化学株式会社 プロピレンの製造方法
CN101641426B (zh) * 2007-03-20 2014-04-16 三井化学株式会社 使用沸石成形催化剂的烃转换方法
EP2504098B1 (en) * 2009-11-27 2016-07-06 Basf Se Process for the preparation of a titanium zeolite catalyst
RU2588575C2 (ru) 2010-12-07 2016-07-10 Басф Се Способ получения пропиленоксида
US8680344B2 (en) * 2011-01-25 2014-03-25 Zeochem Llc Molecular sieve adsorbent blends and uses thereof
AU2012240093B2 (en) * 2011-04-08 2015-06-11 W. R. Grace & Co.-Conn. Mesoporous framework-modified zeolites
RU2623575C2 (ru) * 2012-02-07 2017-06-28 Басф Се МИКРОПОРОШОК И ФОРМОВАННОЕ ИЗДЕЛИЕ, СОДЕРЖАЩИЕ ЦЕОЛИТНЫЙ МАТЕРИАЛ, СОДЕРЖАЩИЙ Ti И Zn
JP6177880B2 (ja) * 2012-04-24 2017-08-09 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se ゼオライト材料及びその製造方法並びにその使用方法
CN104918886B (zh) * 2012-11-13 2018-08-10 巴斯夫欧洲公司 沸石材料的制备和在将氧合物转化成烯烃的方法中的用途

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JP2016535718A (ja) 2016-11-17
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EP3060340B1 (en) 2023-08-16
EP4249115A3 (en) 2023-12-20
KR20160077124A (ko) 2016-07-01
RU2670616C2 (ru) 2018-10-24
EP4249115A2 (en) 2023-09-27
US10434503B2 (en) 2019-10-08
US20160250624A1 (en) 2016-09-01
EP3060340A1 (en) 2016-08-31
JP6538039B2 (ja) 2019-07-03
ES2961911T3 (es) 2024-03-14
BR112016007918B1 (pt) 2020-12-29
CN105848781B (zh) 2020-07-17
RU2016119585A (ru) 2017-11-28
SG11201602956PA (en) 2016-05-30
ZA201603297B (en) 2020-01-29
RU2016119585A3 (es) 2018-05-07
CN105848781A (zh) 2016-08-10
WO2015059171A1 (en) 2015-04-30

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