SA519410752B1 - طريقة لإنتاج إيثيلين أمينات. - Google Patents

طريقة لإنتاج إيثيلين أمينات.

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Publication number
SA519410752B1
SA519410752B1 SA519410752A SA519410752A SA519410752B1 SA 519410752 B1 SA519410752 B1 SA 519410752B1 SA 519410752 A SA519410752 A SA 519410752A SA 519410752 A SA519410752 A SA 519410752A SA 519410752 B1 SA519410752 B1 SA 519410752B1
Authority
SA
Saudi Arabia
Prior art keywords
catalyst
elements
active metals
amination
groups
Prior art date
Application number
SA519410752A
Other languages
English (en)
Inventor
ريجين هيلجا بيبينسى
باربارا بيكير
افا كوش
هيرمان لويكين
جوهان بيتير ميلدير
توماس هيديمان
Original Assignee
باسف اس اي
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by باسف اس اي filed Critical باسف اس اي
Publication of SA519410752B1 publication Critical patent/SA519410752B1/ar

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00—Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/04—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
    • C07C215/06—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
    • C07C215/08—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic with only one hydroxy group and one amino group bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/46—Ruthenium, rhodium, osmium or iridium
    • B01J23/462—Ruthenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/75—Cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1872—Details of the fluidised bed reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/066—Zirconium or hafnium; Oxides or hydroxides thereof

Abstract

يتعلق الاختراع بعمليات لتحضير ألكانول أمينات alkanolamines وإيثيلين أمينات ethyleneamines في طور سائل liquid phase، عن طرق تفاعل إيثيلين جليكول ethylene glycol و/أو مونو إيثانول أمين monoethanolamine مع الأمونيا ammonia في وجود محفز معالجة بالأمين amination catalyst يشتمل على واحد أو أكثر من الفلزات النشطة التي يتم اختيارها من قصدير tin (Sn) وعناصر المجموعة 8، 9، 10 و 11 بالجدول الدوري للعناصر، حيث يتم الحصول على محفز المعالجة بالأمين عن طريق كلسنة اختزالية reductive calcination للمادة المنتجة للمحفز catalyst precursor. ويفضل تحضير المادة المنتجة للمحفز هنا عن طريق ملامسة مادة حاملة تقليدية أو حفزية مع واحد أو أكثر من المركبات القابلة للذوبان soluble compounds من الفلزات النشطة وبشكل اختياري واحد أو أكثر من المركبات القابلة للذوبان من العناصر المحفزة المضافة added catalyst elements. كما يتعلق الاختراع الحالي بعملية لتحضير محفز معالجة بالأمين تشتمل على واحد أو أكثر من الفلزات النشطة من قصدير وعناصر المجموعات 8، 9، 10 و 11 بالجدول الدوري للعناصر، ويتم الحصول على محفز المعالجة بالأمين عن
SA519410752A 2017-06-09 2019-12-08 طريقة لإنتاج إيثيلين أمينات. SA519410752B1 (ar)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP17175151 2017-06-09
PCT/EP2018/063589 WO2018224315A1 (de) 2017-06-09 2018-05-24 Verfahren zur herstellung von ethylenaminen

Publications (1)

Publication Number Publication Date
SA519410752B1 true SA519410752B1 (ar) 2022-07-16

Family

ID=59034559

Family Applications (1)

Application Number Title Priority Date Filing Date
SA519410752A SA519410752B1 (ar) 2017-06-09 2019-12-08 طريقة لإنتاج إيثيلين أمينات.

Country Status (7)

Country Link
US (1) US11214535B2 (ar)
EP (1) EP3634934B1 (ar)
JP (1) JP7105813B2 (ar)
CN (1) CN110709380A (ar)
BR (1) BR112019025307B1 (ar)
SA (1) SA519410752B1 (ar)
WO (1) WO2018224315A1 (ar)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018224316A1 (de) * 2017-06-09 2018-12-13 Basf Se Verfahren zur herstellung von ethylenaminen
WO2019081285A1 (de) 2017-10-27 2019-05-02 Basf Se Verfahren zur herstellung von ethylenaminen
CN111263746B (zh) 2017-10-27 2024-01-19 巴斯夫欧洲公司 制备亚乙基胺的方法
CN116440893A (zh) * 2022-01-06 2023-07-18 中国科学院大连化学物理研究所 一种催化剂及其制备方法和在乙醇氨化脱氢制乙腈中的应用
WO2023135035A1 (en) 2022-01-14 2023-07-20 Basf Se Method for the manufacture or conversion of alkanolamines
WO2024002748A1 (en) 2022-06-29 2024-01-04 Basf Se Method for manufacture of ethyleneamines
WO2024002740A1 (en) 2022-06-29 2024-01-04 Basf Se Method for manufacture of ethyleneamines

Family Cites Families (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3137730A (en) 1960-04-12 1964-06-16 Allied Chem Production of ethylenediamine
DE1172268B (de) 1962-02-21 1964-06-18 Basf Ag Verfahren zur Herstellung von Diaminen
US4123462A (en) 1976-01-07 1978-10-31 Union Carbide Corporation Amination process using nickel-rhenium catalysts
SE461095B (sv) 1983-09-09 1990-01-08 Berol Kemi Ab Amineringsfoerfarande med anvaendning av en ruteniumdopad nickel och/eller kovoltkatalysator
US4653677A (en) 1985-04-16 1987-03-31 The Dow Chemical Company Vessel having a molten material outlet
US4806690A (en) * 1985-05-13 1989-02-21 The Dow Chemical Company Method of producing amines
US5817593A (en) 1995-06-02 1998-10-06 The Dow Chemical Company Catalyst and process for producing amines
DE19645047A1 (de) 1996-10-31 1998-05-07 Basf Ag Katalysatoren für die Aminierung von Alkylenoxiden, Alkoholen, Aldehyden und Ketonen
DE19644107A1 (de) * 1996-10-31 1998-05-07 Basf Ag Katalysatoren für die Aminierung von Alkylenoxiden, Alkoholen, Aldehyden und Ketonen
WO2000006756A1 (en) 1998-07-28 2000-02-10 E.I. Du Pont De Nemours And Company Sulfur metabolism enzymes
DE50007278D1 (de) 1999-12-06 2004-09-09 Basf Ag Verfahren zur Herstellung von Aminen
DE102004023529A1 (de) * 2004-05-13 2005-12-08 Basf Ag Verfahren zur kontinuierlichen Herstellung eines Amins
EP2029520B1 (de) 2006-02-14 2013-07-31 Basf Se Verfahren zur herstellung von ethylenaminen und ethanolaminen aus monoethylenglykol (meg)
JP4761461B2 (ja) * 2006-06-07 2011-08-31 旭化成ケミカルズ株式会社 Ｎｂを主成分とする酸化物触媒及びこれを用いた不飽和化合物の製造方法
WO2008006750A1 (de) 2006-07-14 2008-01-17 Basf Se Verfahren zur herstellung eines amins
WO2008006749A1 (de) 2006-07-14 2008-01-17 Basf Se Verfahren zur herstellung eines amins
EP2166481A4 (en) 2007-07-09 2011-11-02 Fujitsu Ltd DEVICE, METHOD AND USER AUTHENTICATION PROGRAM
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EP2225030B1 (de) 2007-12-21 2012-04-18 Basf Se Verfahren zur herstellung eines amins
CN101903092B (zh) 2007-12-21 2013-03-20 巴斯夫欧洲公司 生产胺的方法
WO2010031719A1 (de) 2008-09-19 2010-03-25 Basf Se Verfahren zur kontinuierlichen herstellung eines amins unter verwendung eines aluminium-kupfer-katalysators
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CN102233272A (zh) 2010-04-22 2011-11-09 张家港惠尔化学科技有限公司 乙二醇氨化制乙二胺的催化剂及其制备方法
EP2780109B1 (de) * 2011-11-17 2016-04-13 Basf Se Verfahren zur herstellung von sn-haltigen katalysatoren
WO2018224316A1 (de) * 2017-06-09 2018-12-13 Basf Se Verfahren zur herstellung von ethylenaminen

Also Published As

Publication number Publication date
JP2020522547A (ja) 2020-07-30
CN110709380A (zh) 2020-01-17
US11214535B2 (en) 2022-01-04
BR112019025307B1 (pt) 2023-05-09
US20200102262A1 (en) 2020-04-02
JP7105813B2 (ja) 2022-07-25
EP3634934A1 (de) 2020-04-15
EP3634934B1 (de) 2022-04-06
BR112019025307A2 (pt) 2020-06-23
WO2018224315A1 (de) 2018-12-13

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