RU2289619C1 - Method for producing vodka "kolesnik luks" - Google Patents

Abstract

FIELD: liqueur and vodka industry.

SUBSTANCE: method involves preparing an aqueous-alcoholic solution (mixture) from rectified ethyl alcohol "Luks" and purified drinking water with the content of natural silver ions up to 0.03 mg/dm³ to provide preparing ready vodka with the strength 40%. Prepared mixture is stirred thoroughly and after its correction for the strength value is pumped over into supply tank followed by feeding in carbon-cleansing battery. The filtration rate of mixture through carbon layer with height 4 m is up to 40 dal/h for fresh carbon and up to 30 dal/h for regenerated one. Vodka filtered off on carbon-cleansing battery is fed into finishing tank. Glucose is dissolved in purified water, filtered and added into finishing tank at intensive stirring. Sodium hydrocarbonate is divided for two parts. Succinic acid is dissolved in softened water in the volume 1.5-2.0 l and sodium hydrocarbonate is added at constant stirring gradually. Each the next portion is added after the complete reaction of previous portion with succinic acid. After the complete dissolving added components the prepared solution is filtered and added into finishing tank, vodka is stirred thoroughly and the strength value is controlled. After control filtration vodka is bottled. Components used in preparing vodka are used in the following ratio, l per 1000 dal of ready product: glucose, 5.8-6.2; succinic acid, 0.08-0.12; sodium hydrocarbonate, 0.18-0.22, and rectified ethyl alcohol "Luks" and purified drinking water with the content of natural silver ions up to 0.03 mg/dm³, the balance, to provide the strength value 40%. Invention provides accelerating the process by 40-45 min, simplifying the process based on elimination for preparing two solutions, their following mixing and enhancing stability of organoleptic indices based on using water containing silver ions up to 3 years.

EFFECT: improved producing method.

3 ex

Description

The invention relates to the distillery industry.

A known method for the production of vodka, providing for the preparation of sorting of rectified ethyl alcohol "Lux" and drinking water corrected with a content of natural silver ions of 0.025-0.035 mg / dm ³ , purifying it, dissolving citric acid in water, and alcohol in anise oil, adding a solution acids and oils in vodka, adding sugar in the form of sugar syrup or an aqueous solution, thoroughly mixing vodka with the ingredients added and pouring with control filtration (RF patent 2090605, CL 12 G 3/06, 1997).

The disadvantage of this method is not sufficiently high organoleptic characteristics of the finished product.

A known method of producing vodka, providing for the preparation of sorting rectified ethyl alcohol "Lux" and drinking corrected water, purifying it, dissolving sodium bicarbonate in water, adding the solution and succinic acid to vodka, adding sugar in the form of sugar syrup or aqueous solution, obtaining an infertility wheat flakes, adding it to vodka, thoroughly mixing and bottling with control filtration (RF patent 2140447, CL 12 G 3/06, 2000).

The disadvantage of this method is the high cost of the finished product.

A known method for the production of vodka, providing for the preparation of an aqueous-alcoholic solution (sorting) by mixing rectified ethyl alcohol “Extra” and corrected drinking water, thoroughly mixing it, adjusting the strength, treating it with activated carbon and filtering the sorting, feeding vodka to the liquefied vat, separating sodium bicarbonate into servings, obtaining a solution of sodium bicarbonate, citric and succinic acids is carried out by mixing citric and succinic acids in a ratio of 1: 1, dissolving the mixture in 2-3 liters of mind lambered water and gradual with constant stirring, a portion of the addition of sodium bicarbonate in an acid solution, filtering the mixture solution, adding the filtrate of the mixture at the same time as vodka into the finishing vat, adding sugar in the form of sugar syrup of 65.8% or aqueous solution to sorting or vodka, thorough mixing of vodka, checking the strength, control filtering and bottling with the fact that (RF patent 224594, CL 12 G 3/06, 2003).

The disadvantage of this method is that vodka has insufficiently high organoleptic characteristics.

The closest method to the proposed one is the method of producing vodka, which involves the preparation of an aqueous-alcoholic solution (sorting) by mixing rectified ethyl alcohol "Lux" and corrected drinking water, thoroughly mixing it, adjusting the strength, treating it with activated carbon and filtering the sorting, supplying vodka to a refined vat dissolving fructose in softened water, adding it to vodka before filtration, dissolving sodium bicarbonate and succinic acid in softened water, mixing the thieves in a ratio of 1: 2, holding the mixture for 30-40 minutes, filtering and sorting before treating it with activated carbon, thoroughly mixing vodka after making the ingredients, checking the strength, control filtering and bottling (RF patent 2143485, class C 12 G 3/08, 1999).

The disadvantages of this method are the duration and complexity of the process, the low stability of organoleptic indicators.

The technical result of the invention consists in accelerating and simplifying the process, increasing the stability of organoleptic indicators.

The technical result is achieved by the fact that the method of producing vodka, which involves preparing an aqueous-alcoholic solution (sorting) by mixing rectified ethyl alcohol “Luxe” and corrected drinking water, thoroughly mixing it, adjusting the strength, treating it with activated charcoal and filtering the sorting, supplying vodka to a refined vat dissolving succinic acid in softened water, mixing the solution with sodium bicarbonate, filtering the solution, adding the filtrate, dissolving sugar in the corrected water, making solution in vodka, thorough mixing of vodka by Fortress, control filtration and bottling provides, as drinking water corrected using water drinking corrected with the natural content of silver ions and 0.03 mg / dm ^3, to carry sodium bicarbonate separation into portions, to mix a solution of succinic acid with sodium bicarbonate by gradually adding each portion of sodium bicarbonate with constant stirring after the complete reaction of the previous portion with succinic acid, and filtering The solution obtained should be carried out in vodka in a liqueur vat, glucose should be used as sugar, the solution of which should be filtered and added to the liqueur vat, and the ingredients included in vodka should be used at the following content, kg per 1000 dal of the finished product:

glucose 5.8-6.2 succinic acid 0.08-0.12 sodium bicarbonate 0.18-0.22 rectified ethyl alcohol "Lux" and corrected drinking water containing natural ions silver up to 0.03 mg / dm ³ rest until   fortress 40%

The proposed vodka "Kolesnik LUX" is produced as follows.

To make vodka use:

rectified ethyl alcohol "Lux" according to GOST R 51652-2000;

drinking water according to GOST R 51232-98 and SanPiN 2.1.4.1074-01 with a hardness of up to 1 mol / m ³ for natural non-softened water and up to 0.20 mol / m ³ for corrected water with a content of natural silver ions up to 0.03 mg / dm ³ ;

glucose according to GOST 975-88 or according to FS 42-24-19-86;

sodium bicarbonate in accordance with GOST 2156-76;

succinic acid according to GOST 6341-75;

crushed active charcoal grade BAU-A according to GOST 6217-74.

From rectified ethyl alcohol "Lux" and corrected drinking water with a natural silver ion content of up to 0.03 mg / dm ^{3, an} aqueous-alcoholic solution (sorting) is prepared based on the preparation of finished vodka with a strength of 40%.

The resulting sorting is thoroughly mixed and, after adjusting its strength, is pumped to a pressure tank, from where it is sent to a coal-cleaning battery. The filtering speed of sorting through a layer of coal 4 m high is up to 40 dal / h for fresh coal and up to 30 dal / h for regenerated.

Filtered on a coal-cleaning battery, vodka is sent to a clean-up vat.

Glucose is dissolved in corrected water, filtered and introduced into the liqueur vat with vigorous stirring.

Sodium bicarbonate is divided into portions. Succinic acid is dissolved in softened water in a volume of 1.5-2.0 L and sodium bicarbonate is added gradually with constant stirring, each subsequent portion of which is added after the previous portion has completely reacted with succinic acid. After complete dissolution of the introduced ingredients, the resulting solution is filtered and introduced into vodka in a finishing vat.

After the ingredients are added to the vat, the vodka is thoroughly mixed and the strength is checked. If you deviate from the standard, correct vodka in the same vat by adding alcohol or water, followed by mixing and checking the strength.

After control filtration, the finished vodka is bottled.

The ingredients included in vodka are used in the following contents, l per 1000 gave the finished product:

glucose 5.8-6.2 succinic acid 0.08-0.12 sodium bicarbonate 0.18-0.22 rectified ethyl alcohol "Lux" and corrected drinking water containing natural ions silver up to 0.03 mg / dm ³ rest until   fortress 40%

Example 1

From rectified ethyl alcohol "Lux" and corrected drinking water with a natural silver ion content of up to 0.03 mg / dm ^{3, an} aqueous-alcoholic solution (sorting) is prepared based on the preparation of finished vodka with a strength of 40%.

The resulting sorting is thoroughly mixed and, after adjusting its strength, is pumped to a pressure tank, from where it is sent to a coal-cleaning battery. Sort filtration rate - up to 40 dal / h for fresh coal.

Filtered on a coal-cleaning battery, vodka is sent to a clean-up vat.

Glucose is dissolved in corrected water, filtered and introduced into the liqueur vat with vigorous stirring.

Sodium bicarbonate is divided into portions. Succinic acid is dissolved in softened water in a volume of 1.5 l, and sodium bicarbonate is added gradually with constant stirring, each subsequent portion of which is added after the previous portion has completely reacted with succinic acid. After complete dissolution of the introduced ingredients, the resulting solution is filtered and introduced into vodka in a finishing vat.

After the ingredients are added to the vat, the vodka is thoroughly mixed and the strength is checked. If you deviate from the standard, correct vodka in the same vat by adding alcohol or water, followed by mixing and checking the strength.

After control filtration, the finished vodka is bottled.

The ingredients included in vodka are used in the following contents, l per 1000 gave the finished product:

glucose 5.8 succinic acid 0.08 sodium bicarbonate 0.1 rectified ethyl alcohol "Lux" and corrected drinking water containing natural ions silver up to 0.03 mg / dm ³ rest until   fortress 40%

Example 2

From rectified ethyl alcohol "Lux" and corrected drinking water with a natural silver ion content of up to 0.03 mg / dm ^{3, an} aqueous-alcoholic solution (sorting) is prepared based on the preparation of finished vodka with a strength of 40%.

The resulting sorting is thoroughly mixed and, after adjusting its strength, is pumped to a pressure tank, from where it is sent to a coal-cleaning battery. Sort filtration rate - up to 40 dal / h for fresh coal.

Filtered on a coal-cleaning battery, vodka is sent to a clean-up vat.

Glucose is dissolved in corrected water, filtered and introduced into the liqueur vat with vigorous stirring.

Sodium bicarbonate is divided into portions. Succinic acid is dissolved in softened water in a volume of 1.7 L and sodium bicarbonate is added gradually with constant stirring, each subsequent portion of which is added after the previous portion has completely reacted with succinic acid. After complete dissolution of the introduced ingredients, the resulting solution is filtered and introduced into vodka in a finishing vat.

After the ingredients are added to the vat, the vodka is thoroughly mixed and the strength is checked. If you deviate from the standard, correct vodka in the same vat by adding alcohol or water, followed by mixing and checking the strength.

After control filtration, the finished vodka is bottled.

The ingredients included in vodka are used in the following contents, l per 1000 gave the finished product:

glucose 6.0 succinic acid 0.1 sodium bicarbonate 0.2 rectified ethyl alcohol "Lux" and corrected drinking water containing natural ions silver up to 0.03 mg / dm ³ rest until   fortress 40%

Example 3

From rectified ethyl alcohol "Lux" and corrected drinking water with a natural silver ion content of up to 0.03 mg / dm ^{3, an} aqueous-alcoholic solution (sorting) is prepared based on the preparation of finished vodka with a strength of 40%.

The resulting sorting is thoroughly mixed and, after adjusting its strength, is pumped to a pressure tank, from where it is sent to a coal-cleaning battery. The filtering speed of sorting through a layer of coal is up to 30 dal / h for regenerated coal.

Filtered on a coal-cleaning battery, vodka is sent to a clean-up vat.

Glucose is dissolved in corrected water, filtered and introduced into the liqueur vat with vigorous stirring.

Sodium bicarbonate is divided into portions. Succinic acid is dissolved in softened water in a volume of 2.0 L and sodium bicarbonate is added gradually with constant stirring, each subsequent portion of which is added after the previous portion has completely reacted with succinic acid. After complete dissolution of the introduced ingredients, the resulting solution is filtered and introduced into vodka in a finishing vat.

After the ingredients are added to the vat, the vodka is thoroughly mixed and the strength is checked. If you deviate from the standard, correct vodka in the same vat by adding alcohol or water, followed by mixing and checking the strength.

After control filtration, the finished vodka is bottled.

The ingredients included in vodka are used in the following contents, l per 1000 gave the finished product:

glucose 6.2 succinic acid 0.12 sodium bicarbonate 0.22 rectified ethyl alcohol "Lux" and corrected drinking water containing natural ions silver up to 0.03 mg / dm ³ rest until   fortress 40%

Indicators of vodka "Kolesnik LUX".

Physicochemical:

fortress,% 40,0 alkalinity - the volume of hydrochloric acid concentration s (HCl) = 0.12 mol / dm ³ spent on titration 100 cm ³ vodka, cm ³ , no more 2.0 mass concentration of acetic aldehyde in 1 DM ³ anhydrous alcohol, mg, no more 3.0 mass concentration of fusel oil (1-propanol, 2-propanol, isobutyl alcohol, 1-butanol, isoamyl alcohol) in 1 dm ³ anhydrous alcohol, mg, no more 6.0 mass concentration of esters in 1 DM ³ anhydrous alcohol, mg, no more 5,0 volume fraction of methyl alcohol in terms of anhydrous alcohol,%, no more 0.02

Organoleptic:

appearance - a transparent liquid without impurities and sediment

taste - soft, inherent to vodka, barely perceptible aftertaste of watermelon

color - colorless

aroma - characteristic, vodka.

The average score for vodka is 9.61 points.

The present invention provides an acceleration of 40-45 minutes and simplification of the process by eliminating the preparation of two solutions, their subsequent mixing, increasing the stability of organoleptic characteristics due to the use of water with silver ions up to 3 years.

Claims (1)

A method of producing vodka, which involves the preparation of an aqueous-alcoholic solution (sorting) by mixing rectified ethyl alcohol “Lux” and drinking corrected water, thoroughly mixing it, adjusting the strength, treating it with activated charcoal and filtering the sorting, supplying vodka to a liquefied vat, dissolving succinic acid in softened water, mixing the solution with sodium bicarbonate, filtering the solution, adding the filtrate, dissolving sugar in the corrected water, adding the solution to vodka, thoroughly mixing regia, by Fortress, control filtration and bottling vodka, characterized in that water as drinking water drinking corrected using the corrected with the content of natural silver ions and 0.03 mg / ^dm3, sodium bicarbonate is separated into portions, succinic acid solution is mixed with sodium bicarbonate by gradually adding each portion of sodium bicarbonate with constant stirring after the complete reaction of the previous portion with succinic acid, and the filtrate of the resulting solution is carried out in vodka in ovodny vat, glucose is used as sugar, the solution of which is filtered and added to the vat, and the ingredients in vodka are used at the following content, kg per 1000 decaliters of the finished product: Glucose 5.8-6.2 succinic acid 0.08-0.12 Sodium bicarbonate 0.18-0.22 Rectified ethyl alcohol "Lux" and corrected drinking water containing natural ions silver up to 0.03 mg / dm ³ Rest to   fortress 40%