RU2156802C1 - Method of vodka production - Google Patents

Abstract

FIELD: liqueur and vodka industry. SUBSTANCE: hardness value of drinking water is brought about to from 1.5 to 6 mole/m³. Treated water is mixed with rectified ethyl alcohol "Ekstra" and in 10-20 min after process onset in moment of the most heat generation preliminary swollen defatted milk is added in the amount 3-4.5 l/1000 dal and remained to swell for 2-3 h. An aqueous-spirituous solution is settled, filtered and mixture of rye bread and 65.8%-th sugar syrup taken in the amount 9-11 kg and 14-15 l/1000 dal of vodka respectively, is added. Mixture is stirred for 50-60 min, fed into injector vacuum cavity under pressure where activated powder-like carbon suspension taken in the amount 0.8-1.2 kg/1000 dal is added. Vodka is filtered, proof is corrected, subjected for control filtration, fed to collector of ready production and pouring. Invention ensures to obtain vodka enriched with complex of biologically active components. EFFECT: high stability, improved quality, broadened assortment. 3 ex

Description

 The invention relates to the distillery industry.

A known method for the production of vodka, involving the preparation of sorting by mixing rectified ethyl alcohol "Extra" and corrected water with a hardness of 1 to 7 mg equiv / dm ³ , introducing sugar and an aqueous-alcoholic infusion of starfish, milk powder, dissolved and swollen in water , mixing the mixture, settling, removing from the precipitate, filtering, cleaning with activated carbon and filling (RF patent 2050412, class C 12 G 3/06, 1995).

 The disadvantage of this method is not sufficiently high organoleptic characteristics of the finished product.

 A known method for the production of vodka, involving the preparation of sorting, the introduction of activated carbon, egg white, rye flour and rye crackers, all the processes of preparing the sorting and its purification with egg white and activated charcoal, as well as the introduction of the necessary components, which use rye flour and rye crackers are carried out in an injector (RF, patent 2074242, class C 12 G 3/06, 1997).

 The disadvantage of this method is the complexity of the process, as well as the need for additional equipment for steaming rye flour and rye crackers.

 A known method for the production of vodka, providing for the softening of water, mixing it with alcohol, removing organic impurities by introducing skimmed milk powder, treating with active charcoal, introducing honey and glycerin and bottling (RF patent, 2043403, class C 12 G 3/06, 1995 g.).

 The disadvantage of this method is the lack of stability of vodka during storage.

 Closest to the proposed method is the production of Posolskaya vodka, which involves the preparation of aqueous-alcoholic liquid by mixing natural drinking water and rectified ethyl alcohol, the introduction of skimmed milk powder, mixing the mixture, settling, removing the precipitate by filtration, adjusting the strength, and purifying it coal-cleaning battery, final filtration and bottling (USSR Author's Certificate N 401713, class C 12 G 3/06, 1973, as well as "Recipes for alcoholic beverages and vodka", M., "Light and food industry, 1981, pp. 286 and 287).

 Despite the high quality of the obtained vodka, it is not enriched with a complex of biologically active substances necessary for the human body, and the use of natural untreated water will reduce the biological stability of vodka during storage.

 The technical result of the present invention is to increase the biological value of vodka and its stability during storage.

This is achieved by the fact that in the method of producing vodka, which includes the preparation of sorting (water-alcohol liquid) by mixing drinking water and rectified ethyl alcohol, introducing skimmed milk powder, mixing the mixture, removing the precipitate by filtration, adjusting the strength, cleaning with activated carbon, final filtration and bottling, is provided for preparing collation use the treated water with a hardness of 1.5 to 6 mol / m ^3, and the introduction of skimmed milk powder is carried out and the stage of mixing the treated water and rectified ethyl alcohol "Extra" after 10-20 minutes from the beginning of the process, and after removing the precipitate, a mixture of rye bread and 65.8% sugar syrup is introduced into the filtrate, mixed for 50-60 minutes and the mixture is sent to activated carbon purification, which is carried out in the injector by injecting a suspension of powdered activated carbon into the stream of the sorting mixture with the introduced ingredients, while the finished vodka has the following ratio of ingredients, kg per 1000 dal:
rye bread - 9 - 11
Skimmed milk powder - 3 - 4,5
as well, l
65.8% sugar syrup - 14 - 15
rectified ethyl alcohol - to the fortress
"Extra" and water treated with hardness from 1.5 to 6 mol / m ³ - 40%
In the proposed method, skim milk is introduced during the period of the greatest heat generation in the sorting with stirring of treated water and alcohol, which speeds up the cleaning process, and the introduction of rye bread mixed with sugar syrup enriches the sorting with a whole complex of biologically active substances (protein, enzymes, vitamins, amino acids, trace elements).

 In addition, when activated carbon is cleaned in the injector in the presence of rye bread and sugar, the process of selective adsorption of harmful impurities by coal and the formation of a pleasant aroma-forming complex are intensified, which gives the vodka a subtle honey-rye taste.

The proposed method is as follows. Using any generally available method, a hardness of 1.5 to 6 mol / m ^{3 is} established in drinking water. The treated water is mixed with rectified ethyl alcohol "Extra" and after 10-20 minutes from the start of the process, at the moment of the highest heat generation, skimmed milk powder is introduced in the amount of 3-4.5 liters per 1000 dal. Pre-skimmed milk powder is poured with warm water at a temperature of 40-45 ^o C, stirred until smooth and left to swell for 2-3 hours, and then introduced in the process of preparing the sorting.

 The sorting is defended, filtered and a mixture of rye bread and 65.8% sugar syrup is introduced into the filtrate in an amount equal to 9-11 kg and 14-15 l per 1000 dal of vodka. The mixture is stirred for 50-60 minutes and the filtrate stream with the introduced ingredients is directed under pressure into the vacuum cavity of the injector, where a suspension of activated powdered carbon is injected in an amount of 0.8-1.2 kg per 1000 dal.

 Vodka is purified from coal particles by filtration, the fortress is adjusted, subjected to control filtration and sent to the collection of finished products, and then to the bottling.

Example 1. For the preparation of vodka "ATAMAN PLATES" is used:
- rectified ethyl alcohol "Extra" GOST 5962-67;
- Skimmed cow's milk powder GOST 10970-87;
- rye bread GOST 2077-84;
- Refined granulated sugar and state standard specification 22-94 refined sugar;
- drinking water according to GOST 2874 with a hardness of 1.5 mol / m ³ ;
- crushed active charcoal brand BAU-A according to GOST 6217-74, crushed to a powder state.

 A water-alcohol solution (sorting) is prepared in such a way as to obtain vodka with a strength of 40%.

 The stainless steel sorting vat is first served with alcohol and then with water.

 Stirred for 10 minutes and make dry, previously swollen, milk in the amount of 4 kg per 1000 dal, and then leave to settle for 2 hours.

 At the end of sedimentation, the water-alcohol mixture with the formed flakes of coagulated protein is subjected to filtration on a Progress type filter press. From the filter press, 10 kg of fresh rye bread and 14.5 l of 65.8% sugar syrup are set into a clarified water-alcohol mixture (filtrate), the stream is mixed for 50 minutes and fed under pressure by a centrifugal pump to the vacuum cavity of the injection unit, where a suspension of powdered activated carbon BAU-A is injected at a rate of 1 kg per 1000 dal.

 Vodka containing the smallest particles of coal is sent from the injection unit to the pressure tanks and then by gravity to the purification filters, where the sorbent is completely separated from the vodka.

 The quality of the finished vodka collected in liquefied vats is re-checked by the laboratory and after its conclusion on compliance with the requirements, the vodka is sent to pressure vessels for subsequent packaging in glass containers.

 Before packaging, the finished product is subjected to control filtration through nylon filters installed on the pipeline supplying vodka to the bottling machine. Recoverable marriage from all stages of the technological process is collected and used in the preparation of the next batch of sorting, incorrigible marriage is collected in a separate collection and sent to the distillery for industrial processing.

Example 2. The method is carried out as in example 1, only water treatment is carried out to a hardness of 3 mol / m ³ , and skimmed milk powder is introduced into sorting in an amount of 3 kg per 1000 dal after 20 minutes from the start of the mixing process.

 Rye bread and 65.8% sugar syrup are introduced into the filtrate in an amount of 9 kg and 14 l, respectively, and stirred for 60 minutes.

 Powdered activated carbon is introduced into the sorting stream in an amount of 0.8 kg per 1000 dal of the finished product.

Example 3. The method is carried out as in example 1, only water treatment is carried out to a hardness of 6 mol / m ³ , and after 15 minutes from the start of mixing of rectified ethyl alcohol and treated water, skimmed milk powder is introduced in an amount of 4.5 kg.

 Rye bread and 65.8% sugar syrup are added to the sorting filtrate in amounts of 11 kg and 15 l, respectively, and powdered activated carbon in the injector is 1.2 kg per 1000 dal.

 Stirring after administration of the ingredients is carried out for 55 minutes.

 The proposed method allows to obtain biologically active vodka with high stability. This is achieved through the use of water with optimal parameters, the introduction of a coagulant - skim milk at a certain stage of the technological process, which allows to speed up the gluing process during the period of maximum heat generation, enrich vodka with a complex of biologically active substances of rye bread (protein, enzymes, vitamins, microelements).

 The intensive process of gluing and cleaning activated carbon in the injector with the direct introduction of activated carbon into the sorting allows you to get a highly stable multicomponent system.

 Vodka in the aftertaste acquires a subtle honey-rye tone, while expanding the range of vodkas.

Claims (1)

Method for the production of vodka, involving the preparation of sorting (water-alcohol liquid) by mixing drinking water and rectified ethyl alcohol "Extra", the introduction of skimmed milk powder, mixing the mixture, removing precipitation by filtration, cleaning with activated carbon, filtering and bottling, characterized in that for sorting preparations use treated water with a hardness of 1.5 - 6 mol / m ³ , and the introduction of skimmed milk powder is carried out at the stage of mixing the treated water and ethyl alcohol rectifier hardened "Extra" after 10 to 20 minutes from the start of the process, while after removing the precipitates, a mixture of rye bread and 65.8% sugar syrup is introduced into the filtrate, stirred for 50 - 60 minutes and sent for cleaning with activated carbon to the injector the next the ratio of ingredients, kg per 1000 gave the finished product:
Rye bread - 9 - 11
Skimmed milk powder - 3 - 4,5,
as well, l
65.8% sugar syrup - 14 - 15
Rectified ethyl alcohol "Extra" and treated water with a hardness of 1.5 - 6 mol / m ³ - Up to 40% strength of the finished product