RU2016102166A - Способ получения частиц бикарбоната щелочного металла - Google Patents
Способ получения частиц бикарбоната щелочного металла Download PDFInfo
- Publication number
- RU2016102166A RU2016102166A RU2016102166A RU2016102166A RU2016102166A RU 2016102166 A RU2016102166 A RU 2016102166A RU 2016102166 A RU2016102166 A RU 2016102166A RU 2016102166 A RU2016102166 A RU 2016102166A RU 2016102166 A RU2016102166 A RU 2016102166A
- Authority
- RU
- Russia
- Prior art keywords
- alkali metal
- metal bicarbonate
- additive
- solution
- crystallization
- Prior art date
Links
- 229910052783 alkali metal Inorganic materials 0.000 title claims 22
- 239000002245 particle Substances 0.000 title claims 22
- 150000001340 alkali metals Chemical class 0.000 title claims 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 title claims 3
- 238000004519 manufacturing process Methods 0.000 title claims 2
- 239000000654 additive Substances 0.000 claims 23
- 238000000034 method Methods 0.000 claims 22
- -1 alkali metal bicarbonate Chemical class 0.000 claims 20
- 230000000996 additive effect Effects 0.000 claims 18
- 238000002425 crystallisation Methods 0.000 claims 12
- 230000008025 crystallization Effects 0.000 claims 12
- 239000000243 solution Substances 0.000 claims 12
- 238000001816 cooling Methods 0.000 claims 6
- 238000003763 carbonization Methods 0.000 claims 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims 4
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims 4
- 239000000783 alginic acid Substances 0.000 claims 4
- 235000010443 alginic acid Nutrition 0.000 claims 4
- 229920000615 alginic acid Polymers 0.000 claims 4
- 229960001126 alginic acid Drugs 0.000 claims 4
- 150000004781 alginic acids Chemical group 0.000 claims 4
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 4
- 239000001768 carboxy methyl cellulose Substances 0.000 claims 4
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims 4
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims 4
- 238000010000 carbonizing Methods 0.000 claims 3
- 244000007835 Cyamopsis tetragonoloba Species 0.000 claims 2
- 229920002907 Guar gum Polymers 0.000 claims 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 2
- 150000001412 amines Chemical class 0.000 claims 2
- 229910002092 carbon dioxide Inorganic materials 0.000 claims 2
- 239000001569 carbon dioxide Substances 0.000 claims 2
- 239000011549 crystallization solution Substances 0.000 claims 2
- 238000004090 dissolution Methods 0.000 claims 2
- 238000001704 evaporation Methods 0.000 claims 2
- 239000000665 guar gum Substances 0.000 claims 2
- 235000010417 guar gum Nutrition 0.000 claims 2
- 229960002154 guar gum Drugs 0.000 claims 2
- 238000012986 modification Methods 0.000 claims 2
- 230000004048 modification Effects 0.000 claims 2
- 229920001282 polysaccharide Polymers 0.000 claims 2
- 239000005017 polysaccharide Substances 0.000 claims 2
- 150000004804 polysaccharides Chemical class 0.000 claims 2
- 238000000926 separation method Methods 0.000 claims 2
- 229910052708 sodium Inorganic materials 0.000 claims 2
- 239000011734 sodium Substances 0.000 claims 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- 229910019142 PO4 Inorganic materials 0.000 claims 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims 1
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical class OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 claims 1
- 238000005299 abrasion Methods 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 229940005740 hexametaphosphate Drugs 0.000 claims 1
- 150000004028 organic sulfates Chemical class 0.000 claims 1
- 150000008379 phenol ethers Chemical class 0.000 claims 1
- 235000021317 phosphate Nutrition 0.000 claims 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims 1
- 229920005646 polycarboxylate Polymers 0.000 claims 1
- 229920000570 polyether Polymers 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 150000003141 primary amines Chemical class 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 229910052938 sodium sulfate Inorganic materials 0.000 claims 1
- 235000011152 sodium sulphate Nutrition 0.000 claims 1
- IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical class NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 claims 1
- 150000003871 sulfonates Chemical class 0.000 claims 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/38—Preparation in the form of granules, pieces or other shaped products
- C01D7/40—Influencing the crystallisation process
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/10—Preparation of bicarbonates from carbonates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/22—Purification
- C01D7/24—Crystallisation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/02—Particle morphology depicted by an image obtained by optical microscopy
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/51—Particles with a specific particle size distribution
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/11—Powder tap density
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Medicinal Preparation (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Cosmetics (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1356160 | 2013-06-26 | ||
| FR1356160A FR3007753A1 (fr) | 2013-06-26 | 2013-06-26 | Procede de preparation de particules de bicarbonate de metal alcalin |
| PCT/EP2014/063555 WO2014207120A2 (fr) | 2013-06-26 | 2014-06-26 | Procédé de préparation de particules de bicarbonate de métal alcalin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2016102166A true RU2016102166A (ru) | 2017-07-31 |
Family
ID=50023636
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2016102166A RU2016102166A (ru) | 2013-06-26 | 2014-06-26 | Способ получения частиц бикарбоната щелочного металла |
Country Status (12)
| Country | Link |
|---|---|
| US (4) | US9815708B2 (https=) |
| EP (3) | EP3013749B1 (https=) |
| JP (2) | JP6630270B2 (https=) |
| CN (4) | CN105492392B (https=) |
| AU (1) | AU2014301127B2 (https=) |
| BR (1) | BR112015032278A2 (https=) |
| CA (1) | CA2916157A1 (https=) |
| FR (1) | FR3007753A1 (https=) |
| MX (1) | MX2015017859A (https=) |
| PL (2) | PL3013751T3 (https=) |
| RU (1) | RU2016102166A (https=) |
| WO (3) | WO2014207120A2 (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013092754A1 (en) | 2011-12-23 | 2013-06-27 | Solvay Sa | Process for the joint production of sodium carbonate and sodium bicarbonate |
| FR3007753A1 (fr) | 2013-06-26 | 2015-01-02 | Solvay | Procede de preparation de particules de bicarbonate de metal alcalin |
| US10392257B2 (en) | 2015-09-23 | 2019-08-27 | Solvay Sa | Method for enhancing sodium bicarbonate flowability |
| EP3353115A1 (en) * | 2015-09-23 | 2018-08-01 | Solvay SA | Production of crystalline sodium bicarbonate |
| EP3574021B1 (en) | 2017-01-24 | 2025-07-02 | Nutrition & Biosciences USA 4, Inc. | Processes for producing precipitated calcium carbonate using polysaccharides |
| KR102022939B1 (ko) * | 2018-01-30 | 2019-09-19 | 가톨릭대학교 산학협력단 | 수산화나트륨이 용해된 알코올-물 혼합 수용액의 탄산화를 통한 중탄산나트륨 제조방법 |
| JP7448926B1 (ja) | 2023-05-31 | 2024-03-13 | 株式会社徳岡テクノ | 二酸化炭素吸着方法、二酸化炭素処理装置、及び、二酸化炭素吸着システム |
Family Cites Families (32)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE502604A (https=) * | 1950-04-24 | |||
| US2954282A (en) * | 1954-12-13 | 1960-09-27 | Fmc Corp | Method of crystallizing |
| US2954262A (en) | 1957-06-26 | 1960-09-27 | Bendix Corp | Anti-skid device |
| US3072466A (en) * | 1960-08-12 | 1963-01-08 | Fmc Corp | Method of crystallizing sodium bicarbonate |
| US3111379A (en) * | 1961-04-12 | 1963-11-19 | Fmc Corp | Manufacture of potassium bicarbonate |
| US3347623A (en) * | 1966-11-03 | 1967-10-17 | Kali Chemie Ag | Preparation of potassium bicarbonate |
| JPS4817160B1 (https=) * | 1970-01-14 | 1973-05-26 | ||
| US3653847A (en) * | 1970-09-14 | 1972-04-04 | American Potash & Chem Corp | Inhibition of sodium bicarbonate crystallization during crystallization of other materials using polyphosphates |
| US3725014A (en) * | 1971-04-21 | 1973-04-03 | Allied Chem | Sodium carbonate crystallization process with foam prevention |
| US3852427A (en) | 1973-04-12 | 1974-12-03 | Allied Chem | Sodium bicarbonate spherulites from sodium d esquicarbonate |
| US3855397A (en) * | 1973-04-12 | 1974-12-17 | Allied Chem | Method of producing sodium carbonate and bicarbonate spherules from brine |
| US3981686A (en) * | 1974-10-24 | 1976-09-21 | Intermountain Research And Development Corporation | Clarifier process for producing sodium carbonate |
| DE2940614C2 (de) * | 1979-10-06 | 1982-09-16 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur Herstellung von Natriumhydrogencarbonat und Chlorwasserstoff |
| US4478599A (en) * | 1982-05-25 | 1984-10-23 | Kerr-Mcgee Chemical Corporation | Method of continuously controlling crystal fines formation |
| FR2646154B1 (fr) * | 1989-04-24 | 1991-06-28 | Solvay | Bicarbonate de sodium et procede pour la cristallisation de bicarbonate de sodium |
| JPH0397617A (ja) | 1989-06-29 | 1991-04-23 | Tosoh Corp | 重炭酸ナトリウムの製造方法 |
| US6042622A (en) * | 1996-07-31 | 2000-03-28 | Basf Corporation | Process for crystallization of alkali metal bicarbonate salts |
| US6270740B2 (en) * | 1997-03-20 | 2001-08-07 | General Chemical Corporation | Method of producing modified sodium carbonate crystals for the production of sodium bicarbonate |
| CA2284967A1 (en) * | 1998-10-13 | 2000-04-13 | Aristos Capital Corporation | Method of formulating alkali earth salts |
| JP4817160B2 (ja) | 2001-03-07 | 2011-11-16 | 日立バルブ株式会社 | 空気調和システム及び電動操作機 |
| US6667021B2 (en) * | 2001-09-12 | 2003-12-23 | General Chemical Corporation | Method for producing enhanced sodium carbonate crystals for making sodium bicarbonate |
| MY146571A (en) * | 2003-04-24 | 2012-08-30 | Lion Corp | Surface-treated particles of water-soluble inorganic compound, method for production thereof, and granular detergent composition |
| CN100348489C (zh) * | 2003-04-24 | 2007-11-14 | 狮王株式会社 | 表面处理水溶性无机化合物颗粒及其制造方法、以及粒状洗涤剂组合物 |
| US20060150892A1 (en) | 2003-04-29 | 2006-07-13 | Akzo Nobel N.V. | Processes Involving the Use of Antisolvent Crystallisation |
| CN1780671A (zh) | 2003-04-29 | 2006-05-31 | 阿克佐诺贝尔股份有限公司 | 涉及使用反溶剂结晶的方法 |
| WO2007108236A1 (ja) | 2006-03-15 | 2007-09-27 | Asahi Glass Company, Limited | 高純度炭酸水素ナトリウム結晶粒子とその製造方法 |
| EP2399866A1 (en) * | 2010-06-22 | 2011-12-28 | Solvay SA | Process for the joint production of sodium carbonate and sodium bicarbonate |
| EP2607312A1 (en) | 2011-12-21 | 2013-06-26 | Solvay Sa | Process for preparing sodium bicarbonate particles |
| WO2013092754A1 (en) | 2011-12-23 | 2013-06-27 | Solvay Sa | Process for the joint production of sodium carbonate and sodium bicarbonate |
| GB201202797D0 (en) | 2012-02-20 | 2012-04-04 | Eminate Ltd | Sodium bicarbonate product |
| CN102940307B (zh) * | 2012-11-19 | 2016-06-08 | 湖南中烟工业有限责任公司 | 一种用于口含型烟草制品的缓释碱性微胶囊及其制备方法和应用 |
| FR3007753A1 (fr) | 2013-06-26 | 2015-01-02 | Solvay | Procede de preparation de particules de bicarbonate de metal alcalin |
-
2013
- 2013-06-26 FR FR1356160A patent/FR3007753A1/fr active Pending
-
2014
- 2014-06-26 RU RU2016102166A patent/RU2016102166A/ru not_active Application Discontinuation
- 2014-06-26 CA CA2916157A patent/CA2916157A1/en not_active Abandoned
- 2014-06-26 EP EP14735513.5A patent/EP3013749B1/fr active Active
- 2014-06-26 BR BR112015032278A patent/BR112015032278A2/pt not_active IP Right Cessation
- 2014-06-26 EP EP14758095.5A patent/EP3013751B1/fr active Active
- 2014-06-26 CN CN201480047406.3A patent/CN105492392B/zh active Active
- 2014-06-26 US US14/900,524 patent/US9815708B2/en active Active
- 2014-06-26 WO PCT/EP2014/063555 patent/WO2014207120A2/fr not_active Ceased
- 2014-06-26 CN CN201480047401.0A patent/CN105492391B/zh active Active
- 2014-06-26 WO PCT/EP2014/063559 patent/WO2014207124A2/fr not_active Ceased
- 2014-06-26 US US14/900,514 patent/US10308517B2/en active Active
- 2014-06-26 JP JP2016522504A patent/JP6630270B2/ja active Active
- 2014-06-26 US US14/900,533 patent/US9873615B2/en active Active
- 2014-06-26 WO PCT/EP2014/063558 patent/WO2014207123A2/fr not_active Ceased
- 2014-06-26 CN CN201480047400.6A patent/CN105492390B/zh active Active
- 2014-06-26 PL PL14758095T patent/PL3013751T3/pl unknown
- 2014-06-26 AU AU2014301127A patent/AU2014301127B2/en not_active Expired - Fee Related
- 2014-06-26 CN CN201810548049.9A patent/CN109553117A/zh active Pending
- 2014-06-26 MX MX2015017859A patent/MX2015017859A/es unknown
- 2014-06-26 PL PL14735513T patent/PL3013749T3/pl unknown
- 2014-06-26 EP EP14735515.0A patent/EP3013750A2/fr not_active Withdrawn
-
2019
- 2019-05-28 US US16/423,709 patent/US20190276326A1/en not_active Abandoned
- 2019-07-08 JP JP2019126800A patent/JP2019206474A/ja active Pending
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FA92 | Acknowledgement of application withdrawn (lack of supplementary materials submitted) |
Effective date: 20180730 |