RU2015149954A - Улучшенная в органических соединениях или относящиеся к органическим соединениям - Google Patents

Улучшенная в органических соединениях или относящиеся к органическим соединениям Download PDF

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RU2015149954A
RU2015149954A RU2015149954A RU2015149954A RU2015149954A RU 2015149954 A RU2015149954 A RU 2015149954A RU 2015149954 A RU2015149954 A RU 2015149954A RU 2015149954 A RU2015149954 A RU 2015149954A RU 2015149954 A RU2015149954 A RU 2015149954A
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perfume
compound
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Ален АЛЬХЕНБЕРГЕР
Хлои БЕРБЕ
Клар ФИНН
Доминик ЛЕЛЬЕВР
Мартин Алан ЛОВЧИК
Розелин ПУАНЬОН-МАРТЕЛЬ
Жиль РОМИ
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Живодан Са
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    • C07C29/04—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by addition of hydroxy groups to unsaturated carbon-to-carbon bonds, e.g. with the aid of H2O2 by hydration of carbon-to-carbon double bonds
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    • C07C45/70—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction with functional groups containing oxygen only in singly bound form
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Claims (27)

1. Соединение 5,9-диметил-9-гидрокси-децен-4-аль формулы (I)
Figure 00000001
2. Соединение по п. 1, где от 50 до 70 масс. % находится в Е-форме, и от 30 до 50 масс. % находится в Z-форме.
3. Парфюмерная смесь, содержащая соединение формулы (I) по п. 1 или 2 и соединение формулы (II)
Figure 00000002
4. Парфюмерная смесь по п. 3, где отношение (масс./масс.) соединения (I) к соединению (II) составляет 99:1, более предпочтительно 99,1 к 0,9; 99,2 к 0,8; 99,3 к 0,7; 99,4 к 0,6; 99,5 к 0,5; 99,6 к 0,4; 99,7 к 0,3; 99,8 к 0,2; 99,9 к 0,1; 99,95 к 0,05; или 99,99 к 0,01.
5. Парфюмерная композиция, содержащая соединение или парфюмерную смесь по любому из пп. 1-4 и одно или более чем одно соединение, выбранное из группы, состоящей из 2-циклогексилиден-2-фенилацетонитрила, 4-(октагидро-4,7-метано-5Н-инден-5-илиден)бутаналя и 4-метил-2-(2-метилпропил)тетрагидро-2Н-пиран-4-ола.
6. Парфюмерная композиция по п. 5, где 2-циклогексилиден-2-фенилацетонитрил используют в количестве от 0,001 до 10 частей по массе на 1 часть по массе 5,9-диметил-9-гидрокси-децен-4-аля.
7. Парфюмерная композиция по п. 5, где 4-метил-2-(2-метилпропил)тетрагидро-2Н-пиран-4-ол используют в количестве от 0,001 до 20 частей по массе на 1 часть по массе 5,9-диметил-9-гидрокси-децен-4-аля.
8. Парфюмерная композиция по п. 5, где 4-(октагидро-4,7-метано-5Н-инден-5-илиден)бутаналь используют в количестве от 0,001 до 0,5 частей по массе на 1 часть по массе 5,9-диметил-9-гидрокси-децен-4-аля.
9. Парфюмерная композиция по п. 5, где соединение или парфюмерная смесь присутствуют в указанной композиции в количестве от 1 до 30% по массе в расчете на общую массу указанной парфюмерной композиции.
10. Парфюмерная композиция по п. 5, имеющая запах ландыша.
11. Парфюмерная композиция по п. 5, содержащая по меньшей мере один дополнительный парфюмерный ингредиент.
12. Парфюмерная композиция по п. 11, где указанный по меньшей мере один дополнительный парфюмерный ингредиент не представляет собой циклогексаль.
13. Композиция для личной гигиены или бытового использования или композиция с тонким запахом, содержащая соединение по п. 1 или 2, парфюмерную смесь по п. 3 или 4 или парфюмерную композицию по любому из пп. 5-12.
14. Соединение по п. 1 или 2, дополнительно содержащее антиоксидант.
15. Парфюмерная смесь по п. 3 или 4, содержащая антиоксидант.
16. Парфюмерная композиция по любому из пп. 5-12, содержащая антиоксидант.
17. Композиция для личной гигиены или бытового использования или композиция с тонким запахом по п. 13, содержащая антиоксидант.
18. Способ придания запаха ландыша парфюмерной композиции, или продукту для личной гигиены или бытового использования, или композиции с тонким запахом, включающий стадию добавления к ним соединения по п. 1 или 2 или парфюмерной смеси по п. 3 или 4.
19. Способ получения 5,9-диметил-9-гидрокси-децен-4-аля (I) из реакционной смеси, включающий стадию получения реакционной смеси в форме по существу свободной от любой кислоты или основания и дистилляции смеси 5,9-диметил-9-гидрокси-децен-4-аля из реакционной смеси.
20. Способ по п. 19, где реакционную смесь получают путем взаимодействия аллилового спирта формулы
Figure 00000003
дивинилового эфира диэтиленгликоля или дивинилового эфира триэтиленгликоля в присутствии кислоты или металлического катализатора при атмосферном давлении и температуре в диапазоне от температуры окружающей среды до 200°C,
где
Figure 00000004
представляет собой двойную связь или простую связь, и
Figure 00000005
OR представляет собой гидроксильную группу или защищенную гидроксильную группу, такую как ацетат, силиловый эфир или смешанный ацеталь, при условии, что
Figure 00000006
OR присутствует только в случае, когда
Figure 00000007
представляет собой простую связь.
RU2015149954A 2013-06-10 2014-06-10 Улучшения в органических соединениях или относящиеся к органическим соединениям RU2667901C2 (ru)

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WO2014198709A1 (en) 2014-12-18
IL242437B (en) 2018-05-31
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GB2515128A (en) 2014-12-17
ZA201508404B (en) 2020-01-29
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KR102321134B1 (ko) 2021-11-03
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MX2015015906A (es) 2016-03-09
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AU2014280241A1 (en) 2015-11-26
CN105283435A (zh) 2016-01-27
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GB201313641D0 (en) 2013-09-11
EP2920139B1 (en) 2017-02-01
JP2016521739A (ja) 2016-07-25
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