RU2007122003A - METHOD FOR PRODUCING 1-HYDROXY-1,2-DIHYDRO [60] FULLERENA - Google Patents

METHOD FOR PRODUCING 1-HYDROXY-1,2-DIHYDRO [60] FULLERENA Download PDF

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RU2007122003A
RU2007122003A RU2007122003/04A RU2007122003A RU2007122003A RU 2007122003 A RU2007122003 A RU 2007122003A RU 2007122003/04 A RU2007122003/04 A RU 2007122003/04A RU 2007122003 A RU2007122003 A RU 2007122003A RU 2007122003 A RU2007122003 A RU 2007122003A
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Russia
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dihydro
hydroxy
producing
fullerene
fullerena
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RU2007122003/04A
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RU2349575C1 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Айрат Рамилевич Туктаров (RU)
Айрат Рамилевич Туктаров
Арслан Рифхатович Ахметов (RU)
Арслан Рифхатович Ахметов
Марко Пудас (FI)
Марко Пудас
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Филиза Габдуллаевна Валямова (RU)
Филиза Габдуллаевна Валямова
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Abstract

Способ получения 1-гидрокси-1,2-дигидро[60]фуллерена общей формулы (1)отличающийся тем, что фуллерен Сподвергают взаимодействию с водой в присутствии катализатора цирконацендихлорида в мольном соотношении С:НО:CpZrCl, равном 0,01:(45-65):(0,0015-0,0025), в среде толуола в качестве растворителя при температуре 70-90°С в течение 0,5-1,5 ч.A method of producing 1-hydroxy-1,2-dihydro [60] fullerene of the general formula (1) characterized in that fullerene is reacted with water in the presence of a zirconacenedichloride catalyst in a molar ratio of C: HO: CpZrCl equal to 0.01: (45- 65) :( 0.0015-0.0025), in toluene, as a solvent, at a temperature of 70-90 ° C for 0.5-1.5 hours

Claims (1)

Способ получения 1-гидрокси-1,2-дигидро[60]фуллерена общей формулы (1)The method of obtaining 1-hydroxy-1,2-dihydro [60] fullerene of the General formula (1)
Figure 00000001
Figure 00000001
 отличающийся тем, что фуллерен С60 подвергают взаимодействию с водой в присутствии катализатора цирконацендихлорида в мольном соотношении С60:Н2О:Cp2ZrCl2, равном 0,01:(45-65):(0,0015-0,0025), в среде толуола в качестве растворителя при температуре 70-90°С в течение 0,5-1,5 ч.characterized in that the fullerene C 60 is reacted with water in the presence of a zirconacene dichloride catalyst in a molar ratio of C 60 : H 2 O: Cp 2 ZrCl 2 equal to 0.01: (45-65) :( 0.0015-0.0025) in toluene medium as a solvent at a temperature of 70-90 ° C for 0.5-1.5 hours
RU2007122003/04A 2007-06-13 2007-06-13 Method of producing 1-hydroxy-1,2-dihydro[60]fullerene RU2349575C1 (en)

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RU2007122003/04A RU2349575C1 (en) 2007-06-13 2007-06-13 Method of producing 1-hydroxy-1,2-dihydro[60]fullerene

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RU2007122003/04A RU2349575C1 (en) 2007-06-13 2007-06-13 Method of producing 1-hydroxy-1,2-dihydro[60]fullerene

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RU2349575C1 RU2349575C1 (en) 2009-03-20

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Publication number Priority date Publication date Assignee Title
RU2495821C2 (en) * 2010-06-04 2013-10-20 Закрытое акционерное общество "Инновации ленинградских институтов и предприятий" (ЗАО ИЛИП) Method of producing mixture of fullerenols
RU2497751C2 (en) * 2011-12-28 2013-11-10 Евгений Александрович Козеев Fullerenol c60 and method of its obtaining from glycerin

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