RU2008103305A - METHOD FOR PRODUCING 1-PHENOXY-1,2-DIHYDRO [60] FULLERENA - Google Patents

METHOD FOR PRODUCING 1-PHENOXY-1,2-DIHYDRO [60] FULLERENA Download PDF

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RU2008103305A
RU2008103305A RU2008103305/04A RU2008103305A RU2008103305A RU 2008103305 A RU2008103305 A RU 2008103305A RU 2008103305/04 A RU2008103305/04 A RU 2008103305/04A RU 2008103305 A RU2008103305 A RU 2008103305A RU 2008103305 A RU2008103305 A RU 2008103305A
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phenoxy
fullerena
dihydro
producing
dihydrofullerene
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RU2008103305/04A
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Russian (ru)
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RU2385859C2 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Айрат Рамилевич Туктаров (RU)
Айрат Рамилевич Туктаров
Арслан Рифхатович Ахметов (RU)
Арслан Рифхатович Ахметов
Марко Пудас (FI)
Марко Пудас
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Леонард Мухибович Халилов (RU)
Леонард Мухибович Халилов
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Институт Нефтехимии И Катализа Российская Академия Наук (Ru)
Институт Нефтехимии И Катализа Российская Академия Наук
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Abstract

Способ получения 1-фенокси-1,2-дигидрофуллерена формулы (1) ! ! отличающийся тем, что фуллерен С60 подвергают взаимодействию с фенолом в присутствии катализатора гафноцендихлорида в мольном соотношении С60:Ph-OH:Cp2HfCl2, равном 0,01:(5-10):(0,0015-0,0025), в среде толуола в качестве растворителя при температуре 130-180°С в течение 5-7 ч.The method of obtaining 1-phenoxy-1,2-dihydrofullerene of the formula (1)! ! characterized in that the fullerene C60 is reacted with phenol in the presence of a hafnocene dichloride catalyst in a molar ratio of C60: Ph-OH: Cp2HfCl2 equal to 0.01: (5-10) :( 0.0015-0.0025) in toluene medium in as a solvent at a temperature of 130-180 ° C for 5-7 hours

Claims (1)

Способ получения 1-фенокси-1,2-дигидрофуллерена формулы (1)The method of obtaining 1-phenoxy-1,2-dihydrofullerene of the formula (1)
Figure 00000001
Figure 00000001
 отличающийся тем, что фуллерен С60 подвергают взаимодействию с фенолом в присутствии катализатора гафноцендихлорида в мольном соотношении С60:Ph-OH:Cp2HfCl2, равном 0,01:(5-10):(0,0015-0,0025), в среде толуола в качестве растворителя при температуре 130-180°С в течение 5-7 ч. characterized in that the fullerene C 60 is reacted with phenol in the presence of a hafnocene dichloride catalyst in a C 60 : Ph-OH: Cp 2 HfCl 2 molar ratio of 0.01: (5-10) :( 0.0015-0.0025) , in the environment of toluene as a solvent at a temperature of 130-180 ° C for 5-7 hours
RU2008103305/04A 2008-01-28 2008-01-28 Method of producing 1-phenoxy-1,2-dihydro[60]fullerene RU2385859C2 (en)

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RU2497751C2 (en) * 2011-12-28 2013-11-10 Евгений Александрович Козеев Fullerenol c60 and method of its obtaining from glycerin
RU2714319C1 (en) * 2019-08-15 2020-02-14 Федеральное государственное бюджетное научное учреждение Уфимский федеральный исследовательский центр Российской академии наук Method for selective production of substituted 1-styryl-2-hydrofullerenes

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