RU2008108332A - METHOD FOR PRODUCING 2 - [(2-DIMETHYLAMINO) METHYL] PHENOL - Google Patents

METHOD FOR PRODUCING 2 - [(2-DIMETHYLAMINO) METHYL] PHENOL Download PDF

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RU2008108332A
RU2008108332A RU2008108332/04A RU2008108332A RU2008108332A RU 2008108332 A RU2008108332 A RU 2008108332A RU 2008108332/04 A RU2008108332/04 A RU 2008108332/04A RU 2008108332 A RU2008108332 A RU 2008108332A RU 2008108332 A RU2008108332 A RU 2008108332A
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phenol
dimethylamino
methyl
bisamine
producing
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RU2008108332/04A
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Russian (ru)
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RU2384567C2 (en
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Мария Геннадьевна Шайбакова (RU)
Мария Геннадьевна Шайбакова
Ирина Геннадьевна Титова (RU)
Ирина Геннадьевна Титова
Гилемдар Адыхамович Махмудияров (RU)
Гилемдар Адыхамович Махмудияров
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
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ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА Российской академии наук (RU)
ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА Российской Академии Наук
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Abstract

Способ получения 2-[(диметиламино)метил]фенола формулы (1): ! ! взаимодействием фенола с бисамином (N,N,N,N-тетраметилметилендиамином), отличающийся тем, что реакцию проводят в присутствии катализатора хлорида меди (I) при мольном соотношении реагентов фенол: бисамин: CuCl=10:(10-11):(0,2-0,4) при температуре 50°С и атмосферном давлении в течение 3,5-4,5 ч.The method of obtaining 2 - [(dimethylamino) methyl] phenol of the formula (1):! ! the interaction of phenol with bisamine (N, N, N, N-tetramethylmethylenediamine), characterized in that the reaction is carried out in the presence of a catalyst of copper (I) chloride at a molar ratio of reagents phenol: bisamine: CuCl = 10: (10-11) :( 0 , 2-0.4) at a temperature of 50 ° C and atmospheric pressure for 3.5-4.5 hours

Claims (1)

Способ получения 2-[(диметиламино)метил]фенола формулы (1):The method of obtaining 2 - [(dimethylamino) methyl] phenol of the formula (1):
Figure 00000001
Figure 00000001
 взаимодействием фенола с бисамином (N,N,N,N-тетраметилметилендиамином), отличающийся тем, что реакцию проводят в присутствии катализатора хлорида меди (I) при мольном соотношении реагентов фенол: бисамин: CuCl=10:(10-11):(0,2-0,4) при температуре 50°С и атмосферном давлении в течение 3,5-4,5 ч. the interaction of phenol with bisamine (N, N, N, N-tetramethylmethylenediamine), characterized in that the reaction is carried out in the presence of a catalyst of copper (I) chloride at a molar ratio of reagents phenol: bisamine: CuCl = 10: (10-11) :( 0 , 2-0.4) at a temperature of 50 ° C and atmospheric pressure for 3.5-4.5 hours
RU2008108332/04A 2008-03-03 2008-03-03 Method of producing 2-[(dimethylamino)methyl]phenol RU2384567C2 (en)

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RU2490378C1 (en) * 2012-03-23 2013-08-20 Общество с ограниченной ответственностью Научно-производственный центр "УВИКОМ" (ООО НПЦ "УВИКОМ") Method of producing carbon fiber material
CN103923073B (en) * 2014-04-16 2016-06-29 中国农业科学院兰州畜牧与兽药研究所 The preparation method of puerarin derivate

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