RU2007121961A - METHOD FOR PRODUCING 2, 3-FULLERO-7-TIABICYCLO [2.2.1] HEPTAN - Google Patents

METHOD FOR PRODUCING 2, 3-FULLERO-7-TIABICYCLO [2.2.1] HEPTAN Download PDF

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RU2007121961A
RU2007121961A RU2007121961/04A RU2007121961A RU2007121961A RU 2007121961 A RU2007121961 A RU 2007121961A RU 2007121961/04 A RU2007121961/04 A RU 2007121961/04A RU 2007121961 A RU2007121961 A RU 2007121961A RU 2007121961 A RU2007121961 A RU 2007121961A
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fullero
producing
tiabicyclo
heptan
thiophan
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RU2007121961/04A
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RU2349593C1 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Айрат Рамилевич Туктаров (RU)
Айрат Рамилевич Туктаров
Арслан Рифхатович Ахметов (RU)
Арслан Рифхатович Ахметов
Марко Пудас (FI)
Марко Пудас
Пасхат Габдрахманович Ибрагимов (RU)
Пасхат Габдрахманович Ибрагимов
Альфия Зуфаровна Шарипова (RU)
Альфия Зуфаровна Шарипова
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Способ получения 2,3-фуллеро-7-тиабицикло[2.2.1]гептана общей формулы (1)характеризующийся тем, что фуллерен Свзаимодействует с тиофаном в присутствии катализатора гафнацендихлорида в мольном соотношении С: тиофан: CpHfCl=0,01:(0,045-0,055):(0,0015-0,0025) в среде толуола при температуре 140-160°С в течение 5-7 ч.A method for producing 2,3-fullero-7-thiabicyclo [2.2.1] heptane of the general formula (1) characterized in that fullerene interacts with thiophan in the presence of a hafnacenedichloride catalyst in a molar ratio C: thiophan: CpHfCl = 0.01: (0.045- 0.055) :( 0.0015-0.0025) in toluene at a temperature of 140-160 ° C for 5-7 hours.

Claims (1)

Способ получения 2,3-фуллеро-7-тиабицикло[2.2.1]гептана общей формулы (1)The method of obtaining 2,3-fullero-7-thiabicyclo [2.2.1] heptane of the General formula (1)
Figure 00000001
Figure 00000001
 характеризующийся тем, что фуллерен С60 взаимодействует с тиофаном в присутствии катализатора гафнацендихлорида в мольном соотношении С60: тиофан: Cp2HfCl2=0,01:(0,045-0,055):(0,0015-0,0025) в среде толуола при температуре 140-160°С в течение 5-7 ч.characterized in that the fullerene C 60 interacts with thiophan in the presence of a hafnacenedichloride catalyst in a molar ratio of C 60 : thiophan: Cp 2 HfCl 2 = 0.01: (0.045-0.055) :( 0.0015-0.0025) in toluene at a temperature of 140-160 ° C for 5-7 hours
RU2007121961/04A 2007-06-13 2007-06-13 Method of producing 2,3-fullero-7-thiabicyclo [2,2,1]heptane RU2349593C1 (en)

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RU2007121961/04A RU2349593C1 (en) 2007-06-13 2007-06-13 Method of producing 2,3-fullero-7-thiabicyclo [2,2,1]heptane

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