RU2007104485A - METHOD FOR PRODUCING 3,4-FULLERO [60] TETRAHYDROTHYOPHENE - Google Patents

METHOD FOR PRODUCING 3,4-FULLERO [60] TETRAHYDROTHYOPHENE Download PDF

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Publication number
RU2007104485A
RU2007104485A RU2007104485/04A RU2007104485A RU2007104485A RU 2007104485 A RU2007104485 A RU 2007104485A RU 2007104485/04 A RU2007104485/04 A RU 2007104485/04A RU 2007104485 A RU2007104485 A RU 2007104485A RU 2007104485 A RU2007104485 A RU 2007104485A
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RU
Russia
Prior art keywords
fullero
tetrahydrothyophene
producing
dimethyl sulfide
tetrahydrothiophene
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RU2007104485/04A
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Russian (ru)
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RU2342378C2 (en
Inventor
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Айрат Рамилевич Туктаров (RU)
Айрат Рамилевич Туктаров
Арслан Рифхатович Ахметов (RU)
Арслан Рифхатович Ахметов
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Марко Пудас (FI)
Марко Пудас
Райхана Валиулловна Кунакова (RU)
Райхана Валиулловна Кунакова
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Priority to RU2007104485/04A priority Critical patent/RU2342378C2/en
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Способ получения 3,4-фуллеро[60]тетрагидротиофена (1)The method of obtaining 3,4-fullero [60] tetrahydrothiophene (1)
Figure 00000001
Figure 00000001
 отличающийся тем, что фуллерен С60 подвергают взаимодействию с диметилсульфидом в присутствии катализатора титанацендихлорида при мольном соотношении С60 : диметилсульфид : Ср2TiCl2 = 0,01:(0,045-0,055):(0,0015-0,0025), в среде толуола, при комнатной температуре (~20°С) в течение 66-78 ч.characterized in that the fullerene C 60 is reacted with dimethyl sulfide in the presence of a titanocene dichloride catalyst at a molar ratio of C 60 : dimethyl sulfide: Cp 2 TiCl 2 = 0.01: (0.045-0.055) :( 0.0015-0.0025), in medium toluene, at room temperature (~ 20 ° C) for 66-78 hours
RU2007104485/04A 2007-02-05 2007-02-05 Method of obtaining 3,4-fullero [60]tetrahydrothiophene RU2342378C2 (en)

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RU2007104485/04A RU2342378C2 (en) 2007-02-05 2007-02-05 Method of obtaining 3,4-fullero [60]tetrahydrothiophene

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RU2007104485/04A RU2342378C2 (en) 2007-02-05 2007-02-05 Method of obtaining 3,4-fullero [60]tetrahydrothiophene

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RU2342378C2 RU2342378C2 (en) 2008-12-27

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RU2565782C1 (en) * 2014-05-08 2015-10-20 Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук Method of obtaining 6-alkyl(aryl)-2,3-(c60-ih)[5,6]fullero-2,3,4,5-tetrahydropyridines

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