RU2010100055A - METHOD FOR PRODUCING BIS-2,4-DIALKYL-1,5,3-DITIAZEPAN-3-ILOV - Google Patents

METHOD FOR PRODUCING BIS-2,4-DIALKYL-1,5,3-DITIAZEPAN-3-ILOV Download PDF

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RU2010100055A
RU2010100055A RU2010100055/04A RU2010100055A RU2010100055A RU 2010100055 A RU2010100055 A RU 2010100055A RU 2010100055/04 A RU2010100055/04 A RU 2010100055/04A RU 2010100055 A RU2010100055 A RU 2010100055A RU 2010100055 A RU2010100055 A RU 2010100055A
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Russia
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dialkyl
ethanedithiol
aldehyde
ditiazepan
ilov
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RU2010100055/04A
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Russian (ru)
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RU2455303C2 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Наталия Наильевна Мурзакова (RU)
Наталия Наильевна Мурзакова
Гузель Ражаповна Хабибуллина (RU)
Гузель Ражаповна Хабибуллина
Внира Рахимовна Ахметова (RU)
Внира Рахимовна Ахметова
Татьяна Викторовна Тюмкина (RU)
Татьяна Викторовна Тюмкина
Райхана Валиулловна Кунакова (RU)
Райхана Валиулловна Кунакова
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
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Учреждение Российской академии наук ИНСТИТУТ НЕФТЕХИМИИ И КАТАЛИЗА РАН (RU)
Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран
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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen- Or Sulfur-Containing Heterocyclic Ring Compounds With Rings Of Six Or More Members (AREA)

Abstract

Способ получения бис-2,4-диалкил-1,5,3-дитиазепан-3-илов общей формулы (1): ! R=Me, Et, nPr, nBu ! отличающийся тем, что предварительно приготовленную смесь при 0°С этандитиола и альдегида (уксусный или пропионовый, или масляный, или валериановый) подвергают взаимодействию с гидразингидратом (60%) при мольном соотношении альдегид : этандитиол : гидразин = 40:20:10 при температуре 0°С и атмосферном давлении в течение 2-4 ч. The method of obtaining bis-2,4-dialkyl-1,5,3-dithiazepan-3-yls of the general formula (1):! R = Me, Et, nPr, nBu! characterized in that the previously prepared mixture at 0 ° C of ethanedithiol and aldehyde (acetic or propionic, or butyric, or valerianic) is reacted with hydrazine hydrate (60%) at a molar ratio of aldehyde: ethanedithiol: hydrazine = 40:20:10 at a temperature of 0 ° C and atmospheric pressure for 2-4 hours

Claims (1)

Способ получения бис-2,4-диалкил-1,5,3-дитиазепан-3-илов общей формулы (1):The method of obtaining bis-2,4-dialkyl-1,5,3-dithiazepan-3-yls of the General formula (1):
Figure 00000001
R=Me, Et, nPr, nBu
Figure 00000001
R = Me, Et, n Pr, n Bu отличающийся тем, что предварительно приготовленную смесь при 0°С этандитиола и альдегида (уксусный или пропионовый, или масляный, или валериановый) подвергают взаимодействию с гидразингидратом (60%) при мольном соотношении альдегид : этандитиол : гидразин = 40:20:10 при температуре 0°С и атмосферном давлении в течение 2-4 ч. characterized in that the previously prepared mixture at 0 ° C of ethanedithiol and aldehyde (acetic or propionic, or butyric, or valerianic) is reacted with hydrazine hydrate (60%) at a molar ratio of aldehyde: ethanedithiol: hydrazine = 40:20:10 at a temperature of 0 ° C and atmospheric pressure for 2-4 hours
RU2010100055/04A 2010-01-11 2010-01-11 Method of producing bis-2,4-dialkyl-1,5,3-dithiazepan-3-yls RU2455303C2 (en)

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RU2547266C2 (en) * 2013-01-29 2015-04-10 Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук Method of obtaining 1,6-bis-(1,5,3-dithiazepan-3-yl)-2,5-disulphanylhexane, possessing fungicidal activity
RU2601310C2 (en) * 2014-12-31 2016-11-10 Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук Method of producing n-(1, 5, 3-dithiazepan-3-yl) carboxylic acids

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