RU2004129342A - METHOD FOR PRODUCING 2,6-DIETHYL-5,7-DIPHENYL-1,2,3,3A, 4,6,8,8A-OCTAHYDROALUMUMACYCLOPENT-DIENO [3,4-F] ISOALUMUMINDOL - Google Patents

METHOD FOR PRODUCING 2,6-DIETHYL-5,7-DIPHENYL-1,2,3,3A, 4,6,8,8A-OCTAHYDROALUMUMACYCLOPENT-DIENO [3,4-F] ISOALUMUMINDOL Download PDF

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RU2004129342A
RU2004129342A RU2004129342/04A RU2004129342A RU2004129342A RU 2004129342 A RU2004129342 A RU 2004129342A RU 2004129342/04 A RU2004129342/04 A RU 2004129342/04A RU 2004129342 A RU2004129342 A RU 2004129342A RU 2004129342 A RU2004129342 A RU 2004129342A
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Russia
Prior art keywords
diphenyl
diethyl
octahydroalumumacyclopent
isoalumumindol
dieno
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RU2004129342/04A
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Russian (ru)
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RU2280037C2 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Лейла Османовна Хафизова (RU)
Лейла Османовна Хафизова
Руслан Васильевич Шайкин (RU)
Руслан Васильевич Шайкин
Лили Рафиковна Якупова (RU)
Лилия Рафиковна Якупова
Тать на Петровна Саламатина (RU)
Татьяна Петровна Саламатина
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ГУ Институт нефтехимии и катализа АН РБ и УНЦ РАН (RU)
ГУ Институт нефтехимии и катализа АН РБ и УНЦ РАН
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Priority to RU2004129342/04A priority Critical patent/RU2280037C2/en
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Claims (1)

Способ получения 2,6-диэтил-5,7-дифенил-1,2,3,3а,4,6,8,8а-октагидроалюмациклопентадиено[3,4-f]изоалюмаиндола общей формулы (1)The method of obtaining 2,6-diethyl-5,7-diphenyl-1,2,3,3a, 4,6,8,8a-octahydroalumacyclopentadiene [3,4-f] isoaluminindole of the general formula (1)
Figure 00000001
Figure 00000001
Figure 00000002
Figure 00000002
 характеризующийся тем, что фенилаллилацетилен общей формулы взаимодействует с этилалюминийдихлоридом (EtAlCl2) в присутствии катализатора цирконацендихлорида (Cp2ZrCl2) в мольном соотношении
Figure 00000003
:EtAlCl2:Mg:Cp2ZrCl2=10:(10÷14):(10÷14):(0.8÷1.2) в атмосфере аргона при нормальном давлении в тетрагидрофуране в течение 8-12 ч.characterized in that the phenylallylacetylene of the general formula is reacted with ethyl aluminum dichloride (EtAlCl 2 ) in the presence of a catalyst of zirconacenedichloride (Cp 2 ZrCl 2 ) in a molar ratio
Figure 00000003
: EtAlCl 2 : Mg: Cp 2 ZrCl 2 = 10: (10 ÷ 14) :( 10 ÷ 14) :( 0.8 ÷ 1.2) in an argon atmosphere at normal pressure in tetrahydrofuran for 8-12 hours.
RU2004129342/04A 2004-10-05 2004-10-05 METHOD FOR PREPARING 2,6-DIETHYL-5,7-DIPHENYL-1,2,3,3a,4,6,8,8a-OCTAHYDROALUMACYCLOPENTADIENO[3,4-f]-ISOALUMAINDOLE RU2280037C2 (en)

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RU2004129342/04A RU2280037C2 (en) 2004-10-05 2004-10-05 METHOD FOR PREPARING 2,6-DIETHYL-5,7-DIPHENYL-1,2,3,3a,4,6,8,8a-OCTAHYDROALUMACYCLOPENTADIENO[3,4-f]-ISOALUMAINDOLE

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