RU2007103634A - METHOD FOR PRODUCING 7-CHLORO-1,2,3,4,5,6,7,8,9,10,11,12,13-DODECACHYDRODicycloOOCTA- [b, d] -ALUMINACYCLOPENTADIENE - Google Patents

METHOD FOR PRODUCING 7-CHLORO-1,2,3,4,5,6,7,8,9,10,11,12,13-DODECACHYDRODicycloOOCTA- [b, d] -ALUMINACYCLOPENTADIENE Download PDF

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Publication number
RU2007103634A
RU2007103634A RU2007103634/04A RU2007103634A RU2007103634A RU 2007103634 A RU2007103634 A RU 2007103634A RU 2007103634/04 A RU2007103634/04 A RU 2007103634/04A RU 2007103634 A RU2007103634 A RU 2007103634A RU 2007103634 A RU2007103634 A RU 2007103634A
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Russia
Prior art keywords
aluminacyclopentadiene
chloro
dodecachydrodicyclooocta
producing
cyclooctin
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RU2007103634/04A
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Russian (ru)
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RU2342394C2 (en
Inventor
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
конов Владимир Анатольевич Дь (RU)
Владимир Анатольевич Дьяконов
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Регина Адиковна Зиннурова (RU)
Регина Адиковна Зиннурова
Галина Аркадьевна Джемилева (RU)
Галина Аркадьевна Джемилева
Лили Фанисовна Галимова (RU)
Лилия Фанисовна Галимова
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Priority to RU2007103634/04A priority Critical patent/RU2342394C2/en
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Claims (1)

Способ получения 7-хлор-1,2,3,4,5,6,7,8,9,10,11,12,13-додекагидродициклоокта-[b,d]-алюминациклопентадиена (1),The method of obtaining 7-chloro-1,2,3,4,5,6,7,8,9,10,11,12,13-dodecahydrodicycloocta- [b, d] -aluminacyclopentadiene (1),
Figure 00000001
Figure 00000001
 характеризующийся тем, что циклооктин подвергают взаимодействию с трихлоралюминием AlCl3 в присутствии порошкообразного магния и катализатора цирконацендихлорида Cp2ZrCl2 при мольном соотношении циклооктин:AlCl3:Mg:Cp2ZrCl2=20:(10-14):(10-14):(0.4-0.6) в атмосфере аргона при нормальном давлении и комнатной температуре, в тетрагидрофуране, в течение 8-12 ч.characterized in that cyclooctin is reacted with trichloroaluminium AlCl 3 in the presence of powdered magnesium and a catalyst of zirconacene dichloride Cp 2 ZrCl 2 at a molar ratio of cyclooctin: AlCl 3 : Mg: Cp 2 ZrCl 2 = 20: (10-14) :( 10-14) : (0.4-0.6) in an argon atmosphere at normal pressure and room temperature, in tetrahydrofuran, for 8-12 hours
RU2007103634/04A 2007-01-30 2007-01-30 METHOD OF OBTAINING 7-CHLORO-1,2,3,4,5,6,7,8,9,10,11,12,13-DODECAHYDRODICYCLO-OCTA-[b,d]-ALUMINACYCLOPENTADIENE RU2342394C2 (en)

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RU2007103634/04A RU2342394C2 (en) 2007-01-30 2007-01-30 METHOD OF OBTAINING 7-CHLORO-1,2,3,4,5,6,7,8,9,10,11,12,13-DODECAHYDRODICYCLO-OCTA-[b,d]-ALUMINACYCLOPENTADIENE

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RU2007103634/04A RU2342394C2 (en) 2007-01-30 2007-01-30 METHOD OF OBTAINING 7-CHLORO-1,2,3,4,5,6,7,8,9,10,11,12,13-DODECAHYDRODICYCLO-OCTA-[b,d]-ALUMINACYCLOPENTADIENE

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RU2342394C2 RU2342394C2 (en) 2008-12-27

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