RU2007126099A - METHOD FOR PRODUCING (9-Ethyl-1-Cyclononenyl) Magnesium Halogenides - Google Patents

METHOD FOR PRODUCING (9-Ethyl-1-Cyclononenyl) Magnesium Halogenides Download PDF

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RU2007126099A
RU2007126099A RU2007126099/04A RU2007126099A RU2007126099A RU 2007126099 A RU2007126099 A RU 2007126099A RU 2007126099/04 A RU2007126099/04 A RU 2007126099/04A RU 2007126099 A RU2007126099 A RU 2007126099A RU 2007126099 A RU2007126099 A RU 2007126099A
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cyclononenyl
ethyl
producing
magnesium
etmgx
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RU2007126099/04A
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RU2355696C2 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
конов Владимир Анатольевич Дь (RU)
Владимир Анатольевич Дьяконов
Алексей Александрович Макаров (RU)
Алексей Александрович Макаров
Галина Аркадьевна Джемилева (RU)
Галина Аркадьевна Джемилева
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Priority to RU2007126099/04A priority Critical patent/RU2355696C2/en
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Claims (1)

Способ получения (9-этил-1-циклононенил)магнийгалогенидов общей формулы (1)The method of obtaining (9-ethyl-1-cyclononenyl) magnesium halides of the General formula (1)
Figure 00000001
Figure 00000001
 характеризующийся тем, что 1,2-нонадиен подвергают взаимодействию с этилмагнийгалогенидом EtMgX в присутствии катализатора цирконацендихлорида Cp2ZrCl2 при мольном соотношении 1,2-нонадиен:EtMgX:Cp2ZrCl2=10:(15-25):(0.4-0.6) в атмосфере аргона при нормальном давлении и комнатной температуре в ТГФ в течение 6-10 ч. characterized in that 1,2-nonadiene is reacted with ethylmagnesium halide EtMgX in the presence of a catalyst of zirconacene dichloride Cp 2 ZrCl 2 at a molar ratio of 1,2-nonadiene: EtMgX: Cp 2 ZrCl 2 = 10: (15-25) :( 0.4-0.6 ) in an argon atmosphere at normal pressure and room temperature in THF for 6-10 hours
RU2007126099/04A 2007-07-09 2007-07-09 Method of (9-ethyl-1-cyclononenyl)magnesium halogenide obtainment RU2355696C2 (en)

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