RU2007103616A - METHOD FOR PRODUCING 1,2,3,4,5,6,8,9,10,11,12,13-DODECAGIDRODICYCLOOCT- [b, d] -MAGNESACYCLOPENTADIENE - Google Patents

METHOD FOR PRODUCING 1,2,3,4,5,6,8,9,10,11,12,13-DODECAGIDRODICYCLOOCT- [b, d] -MAGNESACYCLOPENTADIENE Download PDF

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RU2007103616A
RU2007103616A RU2007103616/04A RU2007103616A RU2007103616A RU 2007103616 A RU2007103616 A RU 2007103616A RU 2007103616/04 A RU2007103616/04 A RU 2007103616/04A RU 2007103616 A RU2007103616 A RU 2007103616A RU 2007103616 A RU2007103616 A RU 2007103616A
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Russia
Prior art keywords
magnesacyclopentadiene
dodecagidrodicyclooct
producing
cyclooctin
bumgcl
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RU2007103616/04A
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Russian (ru)
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RU2342391C2 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
конов Владимир Анатольевич Дь (RU)
Владимир Анатольевич Дьяконов
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Регина Адиковна Зиннурова (RU)
Регина Адиковна Зиннурова
Галина Аркадьевна Джемилева (RU)
Галина Аркадьевна Джемилева
Алексей Александрович Макаров (RU)
Алексей Александрович Макаров
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Priority to RU2007103616/04A priority Critical patent/RU2342391C2/en
Publication of RU2007103616A publication Critical patent/RU2007103616A/en
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Claims (1)

Способ получения 1,2,3,4,5,6,8,9,10,11,12,13-додекагидродициклоокта[b,d]магнезациклопентадиена общей формулы (1)The method of obtaining 1,2,3,4,5,6,8,9,10,11,12,13-dodecahydrodicyclooct [b, d] magnesacyclopentadiene of the general formula (1)
Figure 00000001
Figure 00000001
 характеризующийся тем, что циклооктин взаимодействует с бутилмагнийхлоридом н-BuMgCl в присутствии катализатора цирконацендихлорида Cp2ZrCl2 в мольном соотношении циклооктин: н-BuMgCl:Cp2ZrCl2=10:(22-26):(1.0-1.4) в атмосфере аргона при нормальном давлении и комнатной температуре, в диэтиловом эфире, в течение 4-6 ч.characterized by the fact that cyclooctin interacts with n-BuMgCl butyl magnesium chloride in the presence of a catalyst of zirconacene dichloride Cp 2 ZrCl 2 in a molar ratio cyclooctin: n-BuMgCl: Cp 2 ZrCl 2 = 10: (22-26) :( 1.0-1.4) in argon atmosphere under normal pressure and room temperature, in diethyl ether, for 4-6 hours
RU2007103616/04A 2007-01-30 2007-01-30 METHOD OF 1, 2, 3, 4, 5, 6, 8, 9, 10, 11, 12, 13-DODECAHYDRO-DICYCLOOCTA-[b, d]-MAGNESACYCLOPENTADIENE PRODUCTION RU2342391C2 (en)

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RU2007103616/04A RU2342391C2 (en) 2007-01-30 2007-01-30 METHOD OF 1, 2, 3, 4, 5, 6, 8, 9, 10, 11, 12, 13-DODECAHYDRO-DICYCLOOCTA-[b, d]-MAGNESACYCLOPENTADIENE PRODUCTION

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RU2007103616/04A RU2342391C2 (en) 2007-01-30 2007-01-30 METHOD OF 1, 2, 3, 4, 5, 6, 8, 9, 10, 11, 12, 13-DODECAHYDRO-DICYCLOOCTA-[b, d]-MAGNESACYCLOPENTADIENE PRODUCTION

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RU2342391C2 RU2342391C2 (en) 2008-12-27

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