RU2005110567A - METHOD FOR PRODUCING 1- (1-METHYL-2- (3,4-FULLEROPYRROLIDINYL)) - 1H-1,2,3-BENZOTRIAZOLE - Google Patents

METHOD FOR PRODUCING 1- (1-METHYL-2- (3,4-FULLEROPYRROLIDINYL)) - 1H-1,2,3-BENZOTRIAZOLE Download PDF

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RU2005110567A
RU2005110567A RU2005110567/04A RU2005110567A RU2005110567A RU 2005110567 A RU2005110567 A RU 2005110567A RU 2005110567/04 A RU2005110567/04 A RU 2005110567/04A RU 2005110567 A RU2005110567 A RU 2005110567A RU 2005110567 A RU2005110567 A RU 2005110567A
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Prior art keywords
benzotriazole
methyl
fulleropyrrolidinyl
producing
fullerene
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RU2005110567/04A
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Russian (ru)
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RU2291153C1 (en
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Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
конов Владимир Анатольевич Дь (RU)
Владимир Анатольевич Дьяконов
Айрат Рамилевич Туктаров (RU)
Айрат Рамилевич Туктаров
Нина Егоровна Додонова (RU)
Нина Егоровна Додонова
Ирина Анатольевна Ковтуненко (RU)
Ирина Анатольевна Ковтуненко
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
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Claims (1)

Способ получения 1-(1-метил-2-(3,4-фуллеро-пирролидинил))-1Н-1,2,3-бензотриазола общей формулы (1)The method of obtaining 1- (1-methyl-2- (3,4-fullero-pyrrolidinyl)) - 1H-1,2,3-benzotriazole of the general formula (1)
Figure 00000001
Figure 00000001
 отличающийся тем, что фуллерен[60] взаимодействует с 1Н-1,2,3-бензотриазол-1-N,N-диметилметанамином общей формулы (R-CH2-N-(СН2)2), где R=
Figure 00000002
в мольном соотношении С60:Р-СН2-N-(СН2)2 равном 0.01:(0.01-0.011), в присутствии катализатора Cp2TiCl2 в количестве 15-25 мол.% по отношению к фуллерену[60], в атмосфере аргона в среде толуола в качестве растворителя при температуре 140-160°С в течение 2-4 ч.characterized in that fullerene [60] interacts with 1H-1,2,3-benzotriazole-1-N, N-dimethylmethanamine of the general formula (R-CH 2 -N- (CH 2 ) 2 ), where R =
Figure 00000002
in a molar ratio of C 60 : P-CH 2 -N- (CH 2 ) 2 equal to 0.01: (0.01-0.011), in the presence of a catalyst Cp 2 TiCl 2 in an amount of 15-25 mol.% with respect to fullerene [60], in an argon atmosphere in toluene as a solvent at a temperature of 140-160 ° C for 2-4 hours
RU2005110567/04A 2005-04-11 2005-04-11 Method for preparing 1-[1-(methyl-2-(3,4-fulleropyrrolidinyl)]-1h-1,2,3-benzotriazole RU2291153C1 (en)

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RU2005110567/04A RU2291153C1 (en) 2005-04-11 2005-04-11 Method for preparing 1-[1-(methyl-2-(3,4-fulleropyrrolidinyl)]-1h-1,2,3-benzotriazole

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2669782C2 (en) * 2014-02-07 2018-10-16 Федеральное государственное бюджетное учреждение науки Институт проблем химической физики Российской академии наук (ИПХФ РАН) 1',2',5'-trisubstituted fulleropyrrolidines, methods for production and use thereof in photovoltaic cell

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2669782C2 (en) * 2014-02-07 2018-10-16 Федеральное государственное бюджетное учреждение науки Институт проблем химической физики Российской академии наук (ИПХФ РАН) 1',2',5'-trisubstituted fulleropyrrolidines, methods for production and use thereof in photovoltaic cell

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