RO85397B1 - Procedeu de obtinere a clorhidratului hidrat de 2-dietilamino-n-2', 6'-dimetilfenil-acetamida - Google Patents
Procedeu de obtinere a clorhidratului hidrat de 2-dietilamino-n-2', 6'-dimetilfenil-acetamidaInfo
- Publication number
- RO85397B1 RO85397B1 RO109666A RO10966683A RO85397B1 RO 85397 B1 RO85397 B1 RO 85397B1 RO 109666 A RO109666 A RO 109666A RO 10966683 A RO10966683 A RO 10966683A RO 85397 B1 RO85397 B1 RO 85397B1
- Authority
- RO
- Romania
- Prior art keywords
- dimethylphenyle
- chlorohydrate
- diethylamino
- preparing
- xylene
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 239000008096 xylene Substances 0.000 abstract 2
- 230000001476 alcoholic effect Effects 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 239000012458 free base Substances 0.000 abstract 1
- DKAGJZJALZXOOV-UHFFFAOYSA-N hydrate;hydrochloride Chemical compound O.Cl DKAGJZJALZXOOV-UHFFFAOYSA-N 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000009331 sowing Methods 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Inventia se refera la un procedeu de obtinere a xilinei clorhidrat, hidrat în care se neutralizeaza baza libera cu acid clorhidric solutia apoasa sau alcoolica de concentratie 20...40% la pH 2...4, într-un solvent organic ales dintre toluen, xilen, benzen, care permite îndepartarea azeotropa a apei, racite la 30...35 degree C, adaugarea cantitatii de apa de 1...2 mol de xilina, însamîntare si cristalizare la aceasta temperatura.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO109666A RO85397B1 (ro) | 1983-01-11 | 1983-01-11 | Procedeu de obtinere a clorhidratului hidrat de 2-dietilamino-n-2', 6'-dimetilfenil-acetamida |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO109666A RO85397B1 (ro) | 1983-01-11 | 1983-01-11 | Procedeu de obtinere a clorhidratului hidrat de 2-dietilamino-n-2', 6'-dimetilfenil-acetamida |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RO85397A2 RO85397A2 (ro) | 1984-10-31 |
| RO85397B1 true RO85397B1 (ro) | 1984-11-30 |
Family
ID=20112522
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO109666A RO85397B1 (ro) | 1983-01-11 | 1983-01-11 | Procedeu de obtinere a clorhidratului hidrat de 2-dietilamino-n-2', 6'-dimetilfenil-acetamida |
Country Status (1)
| Country | Link |
|---|---|
| RO (1) | RO85397B1 (ro) |
-
1983
- 1983-01-11 RO RO109666A patent/RO85397B1/ro unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RO85397A2 (ro) | 1984-10-31 |
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