RO78872B - PROCEDEU SI INSTALATIE DE PREPARARE A UNUI COPOLIMER SOLUBIL îN APA - Google Patents

PROCEDEU SI INSTALATIE DE PREPARARE A UNUI COPOLIMER SOLUBIL îN APA

Info

Publication number
RO78872B
RO78872B RO98241A RO9824179A RO78872B RO 78872 B RO78872 B RO 78872B RO 98241 A RO98241 A RO 98241A RO 9824179 A RO9824179 A RO 9824179A RO 78872 B RO78872 B RO 78872B
Authority
RO
Romania
Prior art keywords
column
solution
manomer
subjected
aqueous solution
Prior art date
Application number
RO98241A
Other languages
English (en)
Other versions
RO78872A (ro
Inventor
Jean Boutin
Bernard Guenot
Bruno Jamet
Original Assignee
Societe Rhone Poulenc Industries
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Societe Rhone Poulenc Industries filed Critical Societe Rhone Poulenc Industries
Publication of RO78872A publication Critical patent/RO78872A/ro
Publication of RO78872B publication Critical patent/RO78872B/ro

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/232Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles
    • B01F23/2321Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles by moving liquid and gas in counter current
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/232Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles
    • B01F23/2322Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles using columns, e.g. multi-staged columns
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/237Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media
    • B01F23/2376Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media characterised by the gas being introduced
    • B01F23/23761Aerating, i.e. introducing oxygen containing gas in liquids
    • B01F23/237612Oxygen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/237Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media
    • B01F23/2376Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media characterised by the gas being introduced
    • B01F23/23765Nitrogen
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/20Positioning, supporting, modifying or maintaining the physical state of objects being observed or treated
    • H01J2237/2001Maintaining constant desired temperature
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/20Positioning, supporting, modifying or maintaining the physical state of objects being observed or treated
    • H01J2237/2002Controlling environment of sample
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/26Electron or ion microscopes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymerisation Methods In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Of Suspended Particles By Flocculating Agents (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

Procedeul de preparare a unui copolimer solubil în apa cu proprietati de floculant, caracterizat prin aceea ca, o solutie apoasa de acilamida, metacrilamida, acid acrilic, acid metacrilic, sarurile si esterii acestora, acrilatii si metacrilati, cuaternati de aminoalchil si glicerina cu concentratiea în manomer cuprinsa între 30....90% în greutate, saturata cu aoxigen, este adusa în contact cu o solutie apoasa de hidroxid de sodiu, de potasiu, de amoniu sau sarurile alcaline si un initiator de polimerizare, astfel încît sa rezulte o solutie cu cuntinut de fotoinitiator de 0,005...1% în greutate cu pH de 4...13 si un continut de oxigen sub 0,01%, la o temperatura cuprinsa între temperatura camerei si 75 degree C, anestecarea fiind realizata prin introducerea de gaz inert pe la baza coloanei, apoi solutia de manomer rezultata în partea inferioara a coloanei este evacuata în strat subtire si este supusa iradierii cu raze ultraviolete, apoi produsul rezultat este supus uscarii si macinarii în mod cunoscut. Instalatia pentru realizarea procedeului, este alcatuita dintr-o coloana cu diametrul de 14 cm, avînd pereti opaci cu gauri de vizitare, care contin doua straturi de umplutura, cu elemente de umplutura din sticla sustinute de cîte o grila cu diametrul de peste 0,5 mm si care este prevazuta la partea superioara cu o conducra de alimentare..........
RO98241A 1978-07-24 1979-07-21 PROCEDEU SI INSTALATIE DE PREPARARE A UNUI COPOLIMER SOLUBIL îN APA RO78872B (ro)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7822883A FR2431876A2 (fr) 1978-07-24 1978-07-24 Procede de preparation de solutions aqueuses de monomeres olefiniques en vue d'une photopolymerisation

Publications (2)

Publication Number Publication Date
RO78872A RO78872A (ro) 1983-02-15
RO78872B true RO78872B (ro) 1983-02-28

Family

ID=9211509

Family Applications (1)

Application Number Title Priority Date Filing Date
RO98241A RO78872B (ro) 1978-07-24 1979-07-21 PROCEDEU SI INSTALATIE DE PREPARARE A UNUI COPOLIMER SOLUBIL îN APA

Country Status (14)

Country Link
US (1) US4294676A (ro)
EP (1) EP0008246A1 (ro)
JP (1) JPS584687B2 (ro)
AT (1) AT369391B (ro)
AU (1) AU532382B2 (ro)
BR (1) BR7904697A (ro)
CA (1) CA1123375A (ro)
DK (1) DK309279A (ro)
ES (1) ES482758A1 (ro)
FI (1) FI65267C (ro)
FR (1) FR2431876A2 (ro)
HU (1) HU182660B (ro)
NO (1) NO792432L (ro)
RO (1) RO78872B (ro)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4508687A (en) * 1983-06-20 1985-04-02 Houghton Richard W Degassing/brine tank for pool chlorinating system
US5358611A (en) * 1993-05-17 1994-10-25 Rohm And Haas Company Method of reducing impurities in aqueous monomer solutions
US6423235B1 (en) * 1999-08-18 2002-07-23 Nittetu Chemical Engineering Ltd. Column gas-liquid contacting apparatus and its use thereof
US7879267B2 (en) 2001-08-02 2011-02-01 J&J Vision Care, Inc. Method for coating articles by mold transfer
US7485672B2 (en) * 2001-08-02 2009-02-03 Johnson & Johnson Vision Care, Inc. Process for the synthesis of soluble, high molecular weight polymers
GB0202990D0 (en) * 2002-02-08 2002-03-27 Ciba Spec Chem Water Treat Ltd Apparatus and method for degassing liquids
DE10235643A1 (de) * 2002-08-02 2004-02-19 Cognis Deutschland Gmbh & Co. Kg Überwachung der Stabilität von vinylogen Verbindungen
JP4713167B2 (ja) * 2005-01-21 2011-06-29 株式会社日本触媒 吸水性樹脂の製造方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3912607A (en) * 1969-10-22 1975-10-14 Rhone Progil Process for obtaining high molecular weight water-soluble acrylic polymers and copolymers using radiation
DE2545290A1 (de) * 1975-10-09 1977-04-21 Roehm Gmbh Verfahren zum polymerisieren mittels uv-licht
DE2546279A1 (de) * 1975-10-16 1977-04-21 Bayer Ag Verfahren und vorrichtung zum loesen von feststoffen in loesungsmitteln
FR2348227A1 (fr) * 1976-04-14 1977-11-10 Rhone Poulenc Ind Perfectionnement aux procedes de preparation de polymeres acryliques hydrosolubles par photopolymerisation

Also Published As

Publication number Publication date
HU182660B (en) 1984-02-28
AT369391B (de) 1982-12-27
US4294676A (en) 1981-10-13
FR2431876A2 (fr) 1980-02-22
FI65267C (fi) 1984-04-10
EP0008246A1 (fr) 1980-02-20
FI65267B (fi) 1983-12-30
JPS584687B2 (ja) 1983-01-27
BR7904697A (pt) 1980-05-27
FI792298A7 (fi) 1980-01-25
AU4905979A (en) 1980-01-31
RO78872A (ro) 1983-02-15
NO792432L (no) 1980-01-25
CA1123375A (fr) 1982-05-11
DK309279A (da) 1980-01-25
FR2431876B2 (ro) 1982-02-12
JPS5562903A (en) 1980-05-12
ATA507079A (de) 1982-05-15
AU532382B2 (en) 1983-09-29
ES482758A1 (es) 1980-07-01

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