RO72486B - Procedeu de preparare a triesterului n-fosfonometilglicinei - Google Patents
Procedeu de preparare a triesterului n-fosfonometilglicineiInfo
- Publication number
- RO72486B RO72486B RO80441A RO8044174A RO72486B RO 72486 B RO72486 B RO 72486B RO 80441 A RO80441 A RO 80441A RO 8044174 A RO8044174 A RO 8044174A RO 72486 B RO72486 B RO 72486B
- Authority
- RO
- Romania
- Prior art keywords
- phosphonomethylglycine
- triester
- preparing
- amperage
- phosphono
- Prior art date
Links
- -1 n-phosphonomethylglycine triester Chemical class 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 abstract 3
- AZIHIQIVLANVKD-UHFFFAOYSA-N N-(phosphonomethyl)iminodiacetic acid Chemical compound OC(=O)CN(CC(O)=O)CP(O)(O)=O AZIHIQIVLANVKD-UHFFFAOYSA-N 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical class Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 abstract 1
- 238000005868 electrolysis reaction Methods 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B3/00—Electrolytic production of organic compounds
- C25B3/20—Processes
- C25B3/23—Oxidation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/40—Esters thereof
- C07F9/4003—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
- C07F9/4006—Esters of acyclic acids which can have further substituents on alkyl
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Procedeul de preparare a triesterului N-fosfonometilglicinei, caracterizat prin aceea ca tetraetilesterul de acid N-fosfono-metiliminodiacetic este supus electrolizei la un voltaj de circa +1,6 V fata de electrodul de calomel saturat si amperaj cuprins între 3 si 30 mA timp de 5 h în prezenta de hexafluorofosfat de amoniu, în mediu de acetonitril, la temperatura camerei si presiune normala, apoi amestecul de reactie este supus concentrarii, iar rezidul este prelucrat în vederea separarii produsului de reactie în mod cunoscut.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US413476A US3859183A (en) | 1973-11-07 | 1973-11-07 | Process for producing n-phosphonomethyl glycine triesters |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RO72486A RO72486A (ro) | 1983-04-29 |
| RO72486B true RO72486B (ro) | 1983-04-30 |
Family
ID=23637369
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO80441A RO72486B (ro) | 1973-11-07 | 1974-11-06 | Procedeu de preparare a triesterului n-fosfonometilglicinei |
Country Status (29)
| Country | Link |
|---|---|
| US (1) | US3859183A (ro) |
| JP (1) | JPS5441573B2 (ro) |
| AR (1) | AR216279A1 (ro) |
| AT (1) | AT337206B (ro) |
| BE (1) | BE821891A (ro) |
| BG (1) | BG27092A3 (ro) |
| BR (1) | BR7409282A (ro) |
| CA (1) | CA1030900A (ro) |
| CH (1) | CH615932A5 (ro) |
| CS (1) | CS177191B2 (ro) |
| DD (1) | DD116237A5 (ro) |
| DK (1) | DK140897B (ro) |
| EG (1) | EG11633A (ro) |
| ES (1) | ES431642A1 (ro) |
| FR (1) | FR2249974B1 (ro) |
| GB (1) | GB1452644A (ro) |
| HU (1) | HU171934B (ro) |
| IE (1) | IE40538B1 (ro) |
| IL (1) | IL45990A (ro) |
| IN (1) | IN140891B (ro) |
| IT (1) | IT1025475B (ro) |
| MY (1) | MY7800041A (ro) |
| NL (1) | NL173773C (ro) |
| PH (1) | PH10866A (ro) |
| PL (1) | PL92408B1 (ro) |
| RO (1) | RO72486B (ro) |
| SE (1) | SE401926B (ro) |
| YU (1) | YU39930B (ro) |
| ZA (1) | ZA747144B (ro) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX3898E (es) * | 1975-12-29 | 1981-09-10 | Monsanto Co | Procedimiento mejorado para la preparacion de triesteres de n-fosfonometilglicina |
| DE2635802C2 (de) * | 1976-08-09 | 1984-03-01 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von symmetrischen Carotinoiden |
| CN104313636B (zh) * | 2014-07-08 | 2016-08-24 | 重庆紫光化工股份有限公司 | 一种高纯度EDTA-2Na的环保清洁生产工艺 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2978392A (en) * | 1957-08-12 | 1961-04-04 | Celanese Corp | Electrolytic process |
| US3137705A (en) * | 1960-04-08 | 1964-06-16 | Ciba Geigy Corp | Hydroxylamino compounds |
| US3649484A (en) * | 1969-04-09 | 1972-03-14 | Uniroyal Inc | Electrolytic process for the manufacture of azo compounds |
-
1973
- 1973-11-07 US US413476A patent/US3859183A/en not_active Expired - Lifetime
-
1974
- 1974-11-04 IL IL45990A patent/IL45990A/en unknown
- 1974-11-05 EG EG493/74A patent/EG11633A/xx active
- 1974-11-05 NL NLAANVRAGE7414397,A patent/NL173773C/xx not_active IP Right Cessation
- 1974-11-05 ES ES431642A patent/ES431642A1/es not_active Expired
- 1974-11-06 GB GB4791574A patent/GB1452644A/en not_active Expired
- 1974-11-06 PH PH16491A patent/PH10866A/en unknown
- 1974-11-06 SE SE7413908A patent/SE401926B/xx unknown
- 1974-11-06 DD DD182198A patent/DD116237A5/xx unknown
- 1974-11-06 BR BR9282/74A patent/BR7409282A/pt unknown
- 1974-11-06 IT IT29168/74A patent/IT1025475B/it active
- 1974-11-06 BG BG7428135A patent/BG27092A3/xx unknown
- 1974-11-06 YU YU2974/74A patent/YU39930B/xx unknown
- 1974-11-06 IN IN2439/CAL/1974A patent/IN140891B/en unknown
- 1974-11-06 JP JP12724074A patent/JPS5441573B2/ja not_active Expired
- 1974-11-06 DK DK577674AA patent/DK140897B/da unknown
- 1974-11-06 AR AR256425A patent/AR216279A1/es active
- 1974-11-06 HU HU74MO00000922A patent/HU171934B/hu unknown
- 1974-11-06 PL PL1974175374A patent/PL92408B1/pl unknown
- 1974-11-06 IE IE2284/74A patent/IE40538B1/xx unknown
- 1974-11-06 CS CS7559A patent/CS177191B2/cs unknown
- 1974-11-06 AT AT889074A patent/AT337206B/de not_active IP Right Cessation
- 1974-11-06 CH CH1483874A patent/CH615932A5/de not_active IP Right Cessation
- 1974-11-06 FR FR7436868A patent/FR2249974B1/fr not_active Expired
- 1974-11-06 CA CA213,144A patent/CA1030900A/en not_active Expired
- 1974-11-06 RO RO80441A patent/RO72486B/ro unknown
- 1974-11-06 BE BE150245A patent/BE821891A/xx not_active IP Right Cessation
- 1974-11-06 ZA ZA00747144A patent/ZA747144B/xx unknown
-
1978
- 1978-12-30 MY MY41/78A patent/MY7800041A/xx unknown
Also Published As
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