PT1577334E - Acidificação de um fluxo de alimentação de um iniciador num processo catalisado por dmc para a produção de polióis de poliéter - Google Patents

Acidificação de um fluxo de alimentação de um iniciador num processo catalisado por dmc para a produção de polióis de poliéter Download PDF

Info

Publication number
PT1577334E
PT1577334E PT05005699T PT05005699T PT1577334E PT 1577334 E PT1577334 E PT 1577334E PT 05005699 T PT05005699 T PT 05005699T PT 05005699 T PT05005699 T PT 05005699T PT 1577334 E PT1577334 E PT 1577334E
Authority
PT
Portugal
Prior art keywords
feed stream
dmc
starter
polyether polyols
production
Prior art date
Application number
PT05005699T
Other languages
English (en)
Inventor
Edward P Browne
Original Assignee
Bayer Materialscience Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Materialscience Llc filed Critical Bayer Materialscience Llc
Publication of PT1577334E publication Critical patent/PT1577334E/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F8/00Chemical modification by after-treatment
    • C08F8/02Alkylation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2696Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2/00Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
    • C08G2/30Chemical modification by after-treatment
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645Metals or compounds thereof, e.g. salts
    • C08G65/2663Metal cyanide catalysts, i.e. DMC's
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24Nitrogen compounds
    • B01J27/26Cyanides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polyethers (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Sealing Material Composition (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
PT05005699T 2004-03-19 2005-03-16 Acidificação de um fluxo de alimentação de um iniciador num processo catalisado por dmc para a produção de polióis de poliéter PT1577334E (pt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10/804,894 US20050209438A1 (en) 2004-03-19 2004-03-19 Starter feed stream acidification in DMC-catalyzed process

Publications (1)

Publication Number Publication Date
PT1577334E true PT1577334E (pt) 2008-04-28

Family

ID=34838948

Family Applications (1)

Application Number Title Priority Date Filing Date
PT05005699T PT1577334E (pt) 2004-03-19 2005-03-16 Acidificação de um fluxo de alimentação de um iniciador num processo catalisado por dmc para a produção de polióis de poliéter

Country Status (15)

Country Link
US (2) US20050209438A1 (pt)
EP (1) EP1577334B1 (pt)
JP (1) JP4912602B2 (pt)
KR (1) KR101156415B1 (pt)
CN (2) CN1670007A (pt)
AT (1) ATE386766T1 (pt)
BR (1) BRPI0500969B1 (pt)
CA (1) CA2500905C (pt)
DE (1) DE602005004821T2 (pt)
ES (1) ES2300889T3 (pt)
MX (1) MXPA05003008A (pt)
PL (1) PL1577334T3 (pt)
PT (1) PT1577334E (pt)
RU (1) RU2005107562A (pt)
SG (1) SG115771A1 (pt)

Families Citing this family (49)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050209438A1 (en) * 2004-03-19 2005-09-22 Browne Edward P Starter feed stream acidification in DMC-catalyzed process
US7323605B2 (en) * 2005-11-09 2008-01-29 Bayer Materialscience Llc Double metal cyanide-catalyzed, low unsaturation polyethers from boron-containing starters
US20080021191A1 (en) * 2006-07-20 2008-01-24 Reese Jack R High water content tolerant process for the production of polyethers
DE102007057147A1 (de) 2007-11-28 2009-06-04 Evonik Goldschmidt Gmbh Verfahren zur Alkoxylierung mit DMC-Katalysatoren im Schlaufenreaktor mit Strahlsauger
WO2009077517A1 (de) * 2007-12-19 2009-06-25 Basf Se Verfahren zur herstellung von polyetheralkoholen
US20100324340A1 (en) * 2009-06-23 2010-12-23 Bayer Materialscience Llc Short chain polyether polyols prepared from ultra-low water-content starters via dmc catalysis
EP2475700B2 (en) * 2009-09-07 2022-12-21 Shell Internationale Research Maatschappij B.V. Process for preparing a polyurethane foam
CN102753603B (zh) * 2009-12-14 2015-01-14 陶氏环球技术有限责任公司 使用双金属氰化物催化剂连续制备低当量多元醇的方法
US20140206787A1 (en) * 2010-02-25 2014-07-24 Dow Global Technologies Llc Polyfunctional Polyglycerine Initiated Polyether Polyols and High Resilience Polyurethane Slabstock Therefrom
GB2482176A (en) * 2010-07-23 2012-01-25 Christopher Wickham Noakes Production of polyols for use in low ball rebound polyurethane foams
SG190803A1 (en) 2010-12-20 2013-07-31 Bayer Ip Gmbh Method for producing polyether polyols
SG191340A1 (en) 2010-12-27 2013-08-30 Dow Global Technologies Llc Alkylene oxide polymerization using a double metal cyanide catalyst complex and a magnesium, group 3-group 15 metal or lanthanide series metal compound
ES2539235T3 (es) * 2011-03-31 2015-06-29 Dow Global Technologies Llc Método para producir polioles de poliéter polifuncionales de cadena corta usando catálisis de superácido y cianuro de metal doble
PT2543689T (pt) * 2011-07-04 2016-09-22 Repsol Sa Método contínuo para a síntese de polióis
US20130289150A1 (en) 2012-04-26 2013-10-31 Bayer Materialscience Ag Viscoelastic polyurethane foams
EP2671893A1 (de) 2012-06-06 2013-12-11 Bayer MaterialScience AG Verfahren zur Herstellung von Omega-Hydroxy-Aminopolymeren
US10358404B2 (en) 2012-06-21 2019-07-23 Covestro Llc Process for the production of low molecular weight impact polyethers
CN103525353B (zh) * 2012-07-01 2015-04-22 万华化学(北京)有限公司 一种聚氨酯复膜胶及其制备方法
US9051412B2 (en) * 2013-03-14 2015-06-09 Bayer Materialscience Llc Base-catalyzed, long chain, active polyethers from short chain DMC-catalyzed starters
US9890100B2 (en) 2013-03-14 2018-02-13 Covestro Llc Continuous process for the production of low molecular weight polyethers with a DMC catalyst
US10669368B2 (en) * 2013-03-15 2020-06-02 Covestro Llc Method to increase the resistance of double metal cyanide catalysts to deactivation
US9708448B2 (en) 2013-09-27 2017-07-18 Dow Global Technologies Llc Method for making poly(butylene oxide) polyols
EP2865700A1 (de) * 2013-10-23 2015-04-29 Bayer MaterialScience AG Verfahren zur Herstellung von Polyethercarbonatpolyolen
EP2876121A1 (de) 2013-11-22 2015-05-27 Bayer MaterialScience AG Einsatz von Urethan-Alkoholen zur Herstellung von Polyetherpolyolen
PL3277740T3 (pl) 2015-03-31 2021-06-28 Dow Global Technologies Llc Formulacje pianki półelastycznej
CN107428901B (zh) 2015-03-31 2020-10-27 陶氏环球技术有限责任公司 聚醚多元醇组合物
EP3098251A1 (de) 2015-05-26 2016-11-30 Covestro Deutschland AG Einsatz von alkoholen, die mindestens zwei urethangruppen enthalten, zur herstellung von polyetherpolyolen
AR104981A1 (es) 2015-06-20 2017-08-30 Dow Global Technologies Llc Proceso continuo para producir polioles de poliéter que tienen un elevado contenido de óxido de etileno polimerizado, mediante el uso de un complejo catalizador de cianuro de metal doble y un compuesto metálico de la serie de lantanida o metal del grupo 3 - grupo 15, magnesio
CN107709405B (zh) * 2015-07-02 2020-02-07 科思创有限公司 使用dmc催化剂和连续加入起始剂制备聚醚多元醇的方法
US10626212B2 (en) 2015-07-06 2020-04-21 Dow Global Technologies Llc Polyurethane prepolymers
US9879114B2 (en) 2015-12-22 2018-01-30 Covestro Llc Process for the production of low molecular weight polyoxyalkylene polyols
CN107200837B (zh) * 2016-03-18 2019-10-18 淮安巴德聚氨酯科技有限公司 一种利用dmc催化剂循环制备聚醚多元醇的方法
US9994506B2 (en) * 2016-04-20 2018-06-12 Covestro Llc Process for transitioning reactors from base-catalyzed polyol production to DMC-catalyzed polyol production
JP6931362B2 (ja) 2016-05-13 2021-09-01 コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag ポリオキシアルキレンポリオールの製造方法
US10258953B2 (en) 2016-08-05 2019-04-16 Covestro Llc Systems and processes for producing polyether polyols
CN110869416B (zh) 2017-05-10 2023-04-04 陶氏环球技术有限责任公司 催化剂络合物
KR101950930B1 (ko) * 2017-05-26 2019-02-22 한국화학연구원 아연 산화물 및 알루미늄 산화물을 포함하는 히드록실기 알킬화용 다공성 촉매, 이의 비이온성 계면활성제를 사용한 제조방법 및 이를 이용한 폴리알킬렌 글리콜의 히드록실기의 알킬화 방법
CN111225936B (zh) 2017-09-15 2023-05-12 陶氏环球技术有限责任公司 制造聚醚多元醇的连续工艺
CN109762123A (zh) * 2017-11-09 2019-05-17 山东蓝星东大有限公司 聚酯醚二醇及制法和由其制备的聚氨酯弹性体及制法
JP6510098B1 (ja) * 2018-02-14 2019-05-08 Agc株式会社 ポリウレタンフォーム製造用組成物、ポリオールシステム液及びポリウレタンフォームの製造方法
CN110964191B (zh) * 2018-09-29 2021-02-02 杭州普力材料科技有限公司 一种混合酸改性的锌钴双金属氰化物催化剂及其制备方法
WO2020062816A1 (zh) 2018-09-29 2020-04-02 杭州普力材料科技有限公司 一种混合酸改性的锌钴双金属氰化物催化剂及其制备方法
CN110964192B (zh) * 2018-09-29 2022-05-17 杭州普力材料科技有限公司 一种用于制备二氧化碳基聚碳酸酯的混合酸改性双金属氰化物催化剂及其制备方法
US10723829B2 (en) 2018-12-19 2020-07-28 Covestro Llc Product-to-product process for preparation of low viscosity polyoxyalkylene polyols
US10738155B2 (en) 2018-12-19 2020-08-11 Covestro Llc Product-to-product process for preparation of low viscosity polyoxyalkylene polyols
US10961347B2 (en) 2018-12-19 2021-03-30 Covestro Llc Process for preparing polyoxyalkylene polyols by the continuous addition of starter
US11820861B2 (en) 2018-12-21 2023-11-21 Dow Global Technologies Llc Polyether polymerization process
ES2961155T3 (es) 2019-02-28 2024-03-08 Dow Global Technologies Llc Proceso de polimerización de poliéter
US10723830B1 (en) 2019-03-28 2020-07-28 Covestro Llc Product-to-product process for preparation of low viscosity polyoxyalkylene polyether polyols

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3427256A (en) * 1963-02-14 1969-02-11 Gen Tire & Rubber Co Double metal cyanide complex compounds
GB1063525A (en) * 1963-02-14 1967-03-30 Gen Tire & Rubber Co Organic cyclic oxide polymers, their preparation and tires prepared therefrom
US3427335A (en) * 1963-02-14 1969-02-11 Gen Tire & Rubber Co Double metal cyanides complexed with an acyclic aliphatic saturated monoether,an ester and a cyclic ether and methods for making the same
US3427334A (en) * 1963-02-14 1969-02-11 Gen Tire & Rubber Co Double metal cyanides complexed with an alcohol aldehyde or ketone to increase catalytic activity
GB1225803A (pt) * 1967-06-02 1971-03-24
US3829505A (en) * 1970-02-24 1974-08-13 Gen Tire & Rubber Co Polyethers and method for making the same
US3829500A (en) * 1972-05-24 1974-08-13 R Crowley Oxybis(benzenesulfonylpolyalkoxyalkanols)and their use as surfactants
AU551979B2 (en) * 1982-03-31 1986-05-15 Shell Internationale Research Maatschappij B.V. Epoxy polymerisation catalysts
AU552988B2 (en) * 1982-03-31 1986-06-26 Shell Internationale Research Maatschappij B.V. Polymerizing epoxides and catalyst suspensions for this
JP3097854B2 (ja) * 1989-05-12 2000-10-10 旭硝子株式会社 ポリウレタン類の製造方法
US5158922A (en) * 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
JPH05331278A (ja) * 1992-05-29 1993-12-14 Asahi Glass Co Ltd 高分子量ポリエーテル類の製造方法
US5470813A (en) * 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5482908A (en) * 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5545601A (en) * 1995-08-22 1996-08-13 Arco Chemical Technology, L.P. Polyether-containing double metal cyanide catalysts
US5777177A (en) * 1996-02-07 1998-07-07 Arco Chemical Technology, L.P. Preparation of double metal cyanide-catalyzed polyols by continuous addition of starter
US5689012A (en) * 1996-07-18 1997-11-18 Arco Chemical Technology, L.P. Continuous preparation of low unsaturation polyoxyalkylene polyether polyols with continuous additon of starter
US6077978A (en) * 1997-09-17 2000-06-20 Arco Chemical Technology L.P. Direct polyoxyalkylation of glycerine with double metal cyanide catalysis
US6063897A (en) * 1998-05-05 2000-05-16 Arco Chemical Technology, L.P. Acid-treated double metal cyanide complex catalysts
US6028230A (en) * 1998-06-05 2000-02-22 Arco Chemical Technology, L.P. Epoxide polymerization process
US6359101B1 (en) * 1999-12-15 2002-03-19 Synuthane International, Inc. Preparing polyether polyols with DMC catalysts
DE10001779A1 (de) * 2000-01-18 2001-07-19 Basf Ag Verfahren zur Herstellung von Polyetheralkoholen
KR100697749B1 (ko) * 2000-02-29 2007-03-22 바스프 악티엔게젤샤프트 다금속 시아나이드 화합물의 제조 방법
EP1318985A2 (en) * 2000-09-20 2003-06-18 MERCK PATENT GmbH 4-amino-quinazolines
DE10122020A1 (de) * 2001-05-07 2002-11-14 Bayer Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
US6764978B2 (en) * 2002-08-28 2004-07-20 Basf Aktiengesellschaft Multimetal cyanide compounds
US20050209438A1 (en) * 2004-03-19 2005-09-22 Browne Edward P Starter feed stream acidification in DMC-catalyzed process
US20080021191A1 (en) * 2006-07-20 2008-01-24 Reese Jack R High water content tolerant process for the production of polyethers

Also Published As

Publication number Publication date
SG115771A1 (en) 2005-10-28
KR101156415B1 (ko) 2012-06-13
EP1577334A1 (en) 2005-09-21
BRPI0500969A (pt) 2005-11-08
CA2500905C (en) 2012-11-20
US7919575B2 (en) 2011-04-05
RU2005107562A (ru) 2006-08-27
DE602005004821D1 (de) 2008-04-03
US20050209438A1 (en) 2005-09-22
BRPI0500969B1 (pt) 2015-08-11
US20100234647A1 (en) 2010-09-16
EP1577334B1 (en) 2008-02-20
CN101851329A (zh) 2010-10-06
KR20060044413A (ko) 2006-05-16
ES2300889T3 (es) 2008-06-16
DE602005004821T2 (de) 2009-03-26
CN1670007A (zh) 2005-09-21
JP2005272838A (ja) 2005-10-06
CA2500905A1 (en) 2005-09-19
MXPA05003008A (es) 2005-09-22
ATE386766T1 (de) 2008-03-15
PL1577334T3 (pl) 2008-06-30
JP4912602B2 (ja) 2012-04-11

Similar Documents

Publication Publication Date Title
PL1577334T3 (pl) Zakwaszanie zasilającego strumienia startera w procesie wytwarzania polieteropolioli katalizowanym DMC
HK1079537A1 (en) Polyurethane prepolymers with reduced functionality comprising alkoxysilyl and oh terminal groups, amethod for production and use thereof
DE60204461D1 (de) Verfahren zur herstellung von polyol-mischungen
TW200728337A (en) Process for making moisture-curable silylated resin composition, the resulting composition and moisture-curable products containing the composition
SI1928927T1 (sl) Gelske mase na poliuretanski osnovi, njihova priprava in uporaba
ATE493457T1 (de) Verfahren zur herstellung von polyethercarbonatpolyolen
MXPA05005620A (es) Formulaciones de poliuretano con tiempo de crema extendido/demoldeado rapido.
MX2013000273A (es) Espuma de poliuretano rigida.
MX2012011531A (es) Composiciones de recubrimiento poliasparticas de dos componentes.
DE502006003088D1 (de) Verfahren zur kontinuierlichen herstellung thermoplastisch verarbeitbarer polyurethan-elastomere
MX2016006983A (es) Sistema de poliuretano con vida en crisol prolongada y rapido endurecimiento.
GB0613638D0 (en) Polyurethane elastomers
TW200714670A (en) Process for the continuous production of silylated resin
WO2003014013A3 (en) Calcium hypochlorite of reduced reactivity
TW200639228A (en) Wood adhesives
GB2466895A (en) Polyurethane coating
MX2011013699A (es) Procedimiento para la preparacion de polieterpolioles con grupos terminales hidroxilo primarios.
MX2017015295A (es) Compuesto de poliuretano-poliisocianurato que comprende excelentes propiedades mecanicas.
MY156301A (en) Polymerizable liquid composition and process for the production of organic glass starting from polymerizable liquid compositions of the polyurethane type
MX2019000365A (es) Composiciones adhesivas a base de solvente, con alto contenido de sólidos y métodos para fabricar las mismas.
SA516370740B1 (ar) بوليولات بولي إيثير كربونات متفرعة وعملية لتحضيرها
SG130109A1 (en) A process for the production of polyurethane products
MX354457B (es) Resinas de poliamidoamina-epihalohidrina, método de fabricación y usos de las mismas.
TW200631937A (en) Polyaspartimides
WO2012130673A3 (de) Härtbare zusammensetzung mit bei der härtung alkohol freisetzenden bestandteilen