PL3105176T3 - Sposób wytwarzania grafenu przez erozję elektrochemiczną elektrod grafitowych - Google Patents

Sposób wytwarzania grafenu przez erozję elektrochemiczną elektrod grafitowych

Info

Publication number
PL3105176T3
PL3105176T3 PL15702556T PL15702556T PL3105176T3 PL 3105176 T3 PL3105176 T3 PL 3105176T3 PL 15702556 T PL15702556 T PL 15702556T PL 15702556 T PL15702556 T PL 15702556T PL 3105176 T3 PL3105176 T3 PL 3105176T3
Authority
PL
Poland
Prior art keywords
graphite electrodes
producing graphene
electrochemical erosion
erosion
electrochemical
Prior art date
Application number
PL15702556T
Other languages
English (en)
Inventor
Derek Fray
Ali KAMALI
Original Assignee
Cambridge Enterprise Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cambridge Enterprise Limited filed Critical Cambridge Enterprise Limited
Publication of PL3105176T3 publication Critical patent/PL3105176T3/pl

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/184—Preparation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/184—Preparation
    • C01B32/19—Preparation by exfoliation
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/042—Electrodes formed of a single material
    • C25B11/043—Carbon, e.g. diamond or graphene
    • C25B11/044—Impregnation of carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2204/00—Structure or properties of graphene
    • C01B2204/20—Graphene characterized by its properties
    • C01B2204/32—Size or surface area
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/70—Nanostructure
    • Y10S977/734—Fullerenes, i.e. graphene-based structures, such as nanohorns, nanococoons, nanoscrolls or fullerene-like structures, e.g. WS2 or MoS2 chalcogenide nanotubes, planar C3N4, etc.
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/84—Manufacture, treatment, or detection of nanostructure
    • Y10S977/842—Manufacture, treatment, or detection of nanostructure for carbon nanotubes or fullerenes
    • Y10S977/845—Purification or separation of fullerenes or nanotubes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Metallurgy (AREA)
  • Nanotechnology (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Electric Double-Layer Capacitors Or The Like (AREA)
PL15702556T 2014-02-14 2015-01-28 Sposób wytwarzania grafenu przez erozję elektrochemiczną elektrod grafitowych PL3105176T3 (pl)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB1402650.4A GB2523154B (en) 2014-02-14 2014-02-14 Method of producing graphene
EP15702556.0A EP3105176B1 (en) 2014-02-14 2015-01-28 Method of producing graphene by electrochemical erosion of graphite electrodes
PCT/GB2015/050194 WO2015121613A1 (en) 2014-02-14 2015-01-28 Method of producing graphene

Publications (1)

Publication Number Publication Date
PL3105176T3 true PL3105176T3 (pl) 2020-12-28

Family

ID=50440188

Family Applications (1)

Application Number Title Priority Date Filing Date
PL15702556T PL3105176T3 (pl) 2014-02-14 2015-01-28 Sposób wytwarzania grafenu przez erozję elektrochemiczną elektrod grafitowych

Country Status (9)

Country Link
US (2) US10458026B2 (pl)
EP (1) EP3105176B1 (pl)
JP (1) JP6609562B2 (pl)
CN (2) CN111498837B (pl)
ES (1) ES2812780T3 (pl)
GB (1) GB2523154B (pl)
HU (1) HUE051069T2 (pl)
PL (1) PL3105176T3 (pl)
WO (1) WO2015121613A1 (pl)

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GB2523154B (en) 2014-02-14 2016-04-27 Cambridge Entpr Ltd Method of producing graphene
KR102250190B1 (ko) * 2014-10-31 2021-05-10 삼성전자주식회사 나노버블을 가진 그래핀 구조체 및 그 제조방법
JP6827699B2 (ja) * 2016-02-17 2021-02-10 株式会社キャタラー キャパシタ用炭素材料及びキャパシタ
US10081550B2 (en) 2016-06-26 2018-09-25 Nanotek Instruments, Inc. Direct ultrasonication production of graphene sheets from coke or coal
US10435797B2 (en) * 2016-06-26 2019-10-08 Global Graphene Group, Inc. Electrochemical production of graphene sheets from coke or coal
US11121360B2 (en) 2016-07-15 2021-09-14 Nanotek Instruments Group, Llc Supercritical fluid production of graphene-based supercapacitor electrode from coke or coal
US10081551B2 (en) 2016-07-15 2018-09-25 Nanotek Instruments, Inc. Supercritical fluid process for producing graphene from coke or coal
CN106044762B (zh) * 2016-08-08 2017-12-15 江西理工大学 一种熔盐电解精炼石墨的方法
CN107055515B (zh) * 2016-11-03 2019-04-23 孙旭阳 一种雾化熔融介质制备石墨烯的方法
CN107032333B (zh) * 2017-06-15 2018-03-27 成都新柯力化工科技有限公司 一种基于激光剥离制备石墨烯的方法
CN109663524B (zh) * 2017-10-13 2022-07-15 分散技术有限责任公司 用于热动力学熔体共混批次的热敏部分的速度改变的直接进样探头感测温度方法
US20210061654A1 (en) * 2018-05-21 2021-03-04 The Regents Of The University Of California Natural gas conversion to chemicals and power with molten salts
CN112941567B (zh) * 2018-07-10 2024-02-23 东北大学 潮湿气氛的高温熔盐电解的电化学方法和装置
CN108675287A (zh) * 2018-07-12 2018-10-19 西安交通大学 一种在低温熔盐中电化学阳极剥离制备石墨烯的方法
CA3118079A1 (en) * 2018-10-29 2020-05-07 Stuart Licht Sustainable, facile separation of the molten carbonate electrolysis cathode product
DE102018132896A1 (de) * 2018-12-19 2020-06-25 Universität Duisburg-Essen Verfahren zur Herstellung eines Graphen-Komposits
CN110203904B (zh) * 2019-06-06 2021-07-09 东北大学 用于制备纳米结构碳材料的前体材料及方法
CN111252759B (zh) * 2019-11-20 2021-03-09 厦门大学 一种光照制备氧化石墨烯的方法及产品
CN112591737A (zh) * 2020-12-16 2021-04-02 昆明理工大学 一种回收废旧锂离子电池负极石墨制备碳纳米角的方法
EP4313595A1 (en) 2021-03-26 2024-02-07 Carbon Holdings Intellectual Properties, LLC Methods and apparatus for production of electrochemical graphite
CN113479868A (zh) * 2021-08-02 2021-10-08 中国科学院苏州纳米技术与纳米仿生研究所 一种有机酸铵熔盐双极电化学剥离制备石墨烯的方法
CN113620283B (zh) * 2021-09-03 2023-01-31 陕西六元碳晶股份有限公司 一种石墨烯及其处理方法和应用
CN115417401A (zh) * 2022-05-12 2022-12-02 太原理工大学 一种可回收低温熔融盐制备石墨烯的方法

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JP2002317287A (ja) 2001-04-18 2002-10-31 Permelec Electrode Ltd 過酸化水素製造用電解槽及び過酸化水素製造方法
WO2008143829A2 (en) * 2007-05-14 2008-11-27 Northwestern University Graphene oxide sheet laminate and method
US8114375B2 (en) * 2008-09-03 2012-02-14 Nanotek Instruments, Inc. Process for producing dispersible nano graphene platelets from oxidized graphite
US8226801B2 (en) 2009-07-27 2012-07-24 Nanotek Instruments, Inc. Mass production of pristine nano graphene materials
WO2011019095A1 (en) 2009-08-10 2011-02-17 N-Baro Tech Co., Ltd A method of producing nano-size graphene-based material and an equipment for producing the same
KR100988577B1 (ko) 2010-01-08 2010-10-18 전남대학교산학협력단 터보스트래틱 구조를 갖는 흑연성구조체부터의 그라핀시트 제조방법 및 상기 방법으로 제조된 그라핀시트
KR100996883B1 (ko) 2010-01-08 2010-11-26 전남대학교산학협력단 그라핀시트 제조방법 및 상기 방법으로 제조된 그라핀시트
US8834701B2 (en) 2010-09-14 2014-09-16 Council Of Scientific & Industrial Research Electrochemical process for synthesis of graphene
CN102465309A (zh) * 2010-11-10 2012-05-23 海洋王照明科技股份有限公司 一种石墨烯制备方法
GB2488825A (en) * 2011-03-10 2012-09-12 Morganite Elect Carbon Electrolytic exfoliation of graphite
US9713650B2 (en) 2011-05-06 2017-07-25 The Research Foundation For The State University Of New York Magnetic graphene-like nanoparticles or graphitic nano- or microparticles and method of production and uses thereof
US9922744B2 (en) * 2011-11-14 2018-03-20 John S. Lettow Graphene-sulfur compositions and electrodes made therefrom
TWI522314B (zh) 2011-12-23 2016-02-21 中央研究院 規模化量產製造石墨烯及石墨烯氧化物之設備及其方法
TW201326036A (zh) 2011-12-27 2013-07-01 Ind Tech Res Inst 石墨烯的形成方法
GB201204279D0 (en) * 2012-03-09 2012-04-25 Univ Manchester Production of graphene
CN104540778B (zh) 2012-04-09 2016-10-26 俄亥俄州立大学 生产石墨烯的方法
JP6097908B2 (ja) * 2012-05-25 2017-03-22 国立研究開発法人物質・材料研究機構 剥離グラフェン膜の製造方法
CN103132100B (zh) 2013-03-22 2015-06-17 上海交通大学 一种从煤生产纯净氢气和二氧化碳的工艺方法
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GB2523154B (en) 2014-02-14 2016-04-27 Cambridge Entpr Ltd Method of producing graphene

Also Published As

Publication number Publication date
HUE051069T2 (hu) 2021-01-28
GB2523154B (en) 2016-04-27
EP3105176B1 (en) 2020-07-29
GB2523154A (en) 2015-08-19
CN106414323A (zh) 2017-02-15
GB201402650D0 (en) 2014-04-02
EP3105176A1 (en) 2016-12-21
CN106414323B (zh) 2020-03-24
US10865488B2 (en) 2020-12-15
JP2017512736A (ja) 2017-05-25
CN111498837B (zh) 2023-10-24
JP6609562B2 (ja) 2019-11-20
US10458026B2 (en) 2019-10-29
US20170050853A1 (en) 2017-02-23
ES2812780T3 (es) 2021-03-18
CN111498837A (zh) 2020-08-07
US20200095694A1 (en) 2020-03-26
WO2015121613A1 (en) 2015-08-20

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