NO315709B1 - Fremgangsmåte for reduksjon av organiske syrer i petroleumsinnmatinger - Google Patents
Fremgangsmåte for reduksjon av organiske syrer i petroleumsinnmatinger Download PDFInfo
- Publication number
- NO315709B1 NO315709B1 NO20010599A NO20010599A NO315709B1 NO 315709 B1 NO315709 B1 NO 315709B1 NO 20010599 A NO20010599 A NO 20010599A NO 20010599 A NO20010599 A NO 20010599A NO 315709 B1 NO315709 B1 NO 315709B1
- Authority
- NO
- Norway
- Prior art keywords
- volatile hydrocarbon
- hydrocarbon fraction
- organic acids
- volatile
- reactor
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 34
- 150000007524 organic acids Chemical class 0.000 title claims description 25
- 235000005985 organic acids Nutrition 0.000 title claims description 24
- 239000003208 petroleum Substances 0.000 title claims description 19
- 239000004215 Carbon black (E152) Substances 0.000 claims description 56
- 229930195733 hydrocarbon Natural products 0.000 claims description 56
- 150000002430 hydrocarbons Chemical class 0.000 claims description 56
- 239000002253 acid Substances 0.000 claims description 25
- 150000001447 alkali salts Chemical class 0.000 claims description 25
- 238000006243 chemical reaction Methods 0.000 claims description 18
- 238000007669 thermal treatment Methods 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000000354 decomposition reaction Methods 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 9
- 238000010926 purge Methods 0.000 claims description 8
- 238000011282 treatment Methods 0.000 claims description 8
- 230000002378 acidificating effect Effects 0.000 claims description 6
- 239000011261 inert gas Substances 0.000 claims description 5
- 150000003839 salts Chemical group 0.000 claims description 5
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000011010 flushing procedure Methods 0.000 claims description 2
- 150000002739 metals Chemical class 0.000 claims 1
- 239000010779 crude oil Substances 0.000 description 23
- 239000007788 liquid Substances 0.000 description 20
- 239000003921 oil Substances 0.000 description 20
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 12
- 125000005608 naphthenic acid group Chemical group 0.000 description 12
- 150000007513 acids Chemical class 0.000 description 9
- 238000004064 recycling Methods 0.000 description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 8
- 239000011575 calcium Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical class [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 6
- 229910052791 calcium Inorganic materials 0.000 description 6
- 229910002092 carbon dioxide Inorganic materials 0.000 description 6
- 239000012263 liquid product Substances 0.000 description 6
- 239000001569 carbon dioxide Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 4
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 4
- 239000000920 calcium hydroxide Substances 0.000 description 4
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 239000012530 fluid Substances 0.000 description 4
- 238000006386 neutralization reaction Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- -1 carboxylic acids Chemical class 0.000 description 3
- 150000001735 carboxylic acids Chemical class 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 230000035484 reaction time Effects 0.000 description 3
- 239000000341 volatile oil Substances 0.000 description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 159000000007 calcium salts Chemical class 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000002737 fuel gas Substances 0.000 description 2
- 239000000295 fuel oil Substances 0.000 description 2
- 238000005984 hydrogenation reaction Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
- 150000004679 hydroxides Chemical class 0.000 description 2
- 239000003112 inhibitor Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- HNNQYHFROJDYHQ-UHFFFAOYSA-N 3-(4-ethylcyclohexyl)propanoic acid 3-(3-ethylcyclopentyl)propanoic acid Chemical compound CCC1CCC(CCC(O)=O)C1.CCC1CCC(CCC(O)=O)CC1 HNNQYHFROJDYHQ-UHFFFAOYSA-N 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical class [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 229910019440 Mg(OH) Inorganic materials 0.000 description 1
- 229910003296 Ni-Mo Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000007701 flash-distillation Methods 0.000 description 1
- 159000000012 group IIA salts Chemical class 0.000 description 1
- 229940097789 heavy mineral oil Drugs 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000011777 magnesium Chemical class 0.000 description 1
- 229910052749 magnesium Chemical class 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- DDTIGTPWGISMKL-UHFFFAOYSA-N molybdenum nickel Chemical compound [Ni].[Mo] DDTIGTPWGISMKL-UHFFFAOYSA-N 0.000 description 1
- 229910000476 molybdenum oxide Inorganic materials 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- PQQKPALAQIIWST-UHFFFAOYSA-N oxomolybdenum Chemical compound [Mo]=O PQQKPALAQIIWST-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 238000005504 petroleum refining Methods 0.000 description 1
- 238000011027 product recovery Methods 0.000 description 1
- 239000002683 reaction inhibitor Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G17/00—Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G31/00—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
- C10G31/06—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for by heating, cooling, or pressure treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/132,295 US5891325A (en) | 1998-08-11 | 1998-08-11 | Process for reducing total acid number of crude oil |
| PCT/US1999/016058 WO2000009631A1 (en) | 1998-08-11 | 1999-07-16 | Process for reducing total acid number of crude oil |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO20010599D0 NO20010599D0 (no) | 2001-02-05 |
| NO20010599L NO20010599L (no) | 2001-02-05 |
| NO315709B1 true NO315709B1 (no) | 2003-10-13 |
Family
ID=22453355
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20010599A NO315709B1 (no) | 1998-08-11 | 2001-02-05 | Fremgangsmåte for reduksjon av organiske syrer i petroleumsinnmatinger |
Country Status (20)
| Country | Link |
|---|---|
| US (1) | US5891325A (id) |
| EP (1) | EP1109879B1 (id) |
| JP (1) | JP2003534391A (id) |
| KR (1) | KR20010088788A (id) |
| CN (1) | CN1312849A (id) |
| AR (1) | AR022360A1 (id) |
| AT (1) | ATE236235T1 (id) |
| AU (1) | AU750406B2 (id) |
| BR (1) | BR9912882A (id) |
| CA (1) | CA2338623A1 (id) |
| DE (1) | DE69906549T2 (id) |
| DK (1) | DK1109879T3 (id) |
| ES (1) | ES2194485T3 (id) |
| HK (1) | HK1039144A1 (id) |
| ID (1) | ID28396A (id) |
| MY (1) | MY115922A (id) |
| NO (1) | NO315709B1 (id) |
| RU (1) | RU2207366C2 (id) |
| TW (1) | TW500796B (id) |
| WO (1) | WO2000009631A1 (id) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9912842D0 (en) * | 1999-06-02 | 1999-08-04 | Bp Exploration Operating | Process for reducing the acidity of oil |
| EP1678278A4 (en) * | 2003-10-17 | 2011-08-24 | Fluor Tech Corp | COMPOSITIONS, CONFIGURATIONS, AND METHODS FOR REDUCING NAPHTHIC ACID CORROSIVITY |
| US7602369B2 (en) * | 2004-05-04 | 2009-10-13 | Sharp Laboratories Of America, Inc. | Liquid crystal display with colored backlight |
| WO2006014486A1 (en) * | 2004-07-07 | 2006-02-09 | California Institute Of Technology | Process to upgrade oil using metal oxides |
| US8277639B2 (en) * | 2005-09-20 | 2012-10-02 | Exxonmobil Chemical Patents Inc. | Steam cracking of high TAN crudes |
| JP5506139B2 (ja) * | 2007-01-18 | 2014-05-28 | Ｊｘ日鉱日石エネルギー株式会社 | 化学装置に対する腐食を低減する方法 |
| KR101540680B1 (ko) * | 2008-01-09 | 2015-07-30 | 차이나 페트로리움 앤드 케미컬 코포레이션 | 저급의 산 함유 원유를 변환하기 위한 촉매, 그의 제조 및 이용 방법 |
| US9259711B2 (en) * | 2008-05-20 | 2016-02-16 | China Petroleum & Chemical Corporation | Catalyst for upgrading inferior acid-containing crude oil, process for manufacturing the same, and application thereof |
| CN102041034B (zh) * | 2009-10-23 | 2013-08-21 | 中国石油化工股份有限公司 | 降低基础油中和值的方法 |
| JP5421794B2 (ja) | 2010-01-12 | 2014-02-19 | 日揮株式会社 | 原油処理システム |
| US8840778B2 (en) * | 2010-03-29 | 2014-09-23 | Lyondell Chemical Technology, L.P. | Processing of acid containing hydrocarbons |
| JP6072790B2 (ja) | 2011-07-29 | 2017-02-01 | サウジ アラビアン オイル カンパニー | 石油精製原料中の全酸価を減少させる方法 |
| CN102643664B (zh) * | 2012-04-27 | 2015-02-18 | 山东金诚重油化工技术研究院 | 淤固床焦化生产工艺 |
| CN104122321A (zh) * | 2013-04-28 | 2014-10-29 | 威尔资源有限公司 | 石油中酸性化合物的测定方法 |
| US20150065766A1 (en) | 2013-08-09 | 2015-03-05 | Soumaine Dehkissia | Heavy Oils Having Reduced Total Acid Number and Olefin Content |
| EP4112702A1 (en) | 2021-06-29 | 2023-01-04 | Indian Oil Corporation Limited | Pre-treatment process for conversion of residual oils in a delayed coker unit |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA612730A (en) * | 1961-01-17 | Sun Oil Company | Obtaining neutral distillates from petroleum | |
| US1236230A (en) * | 1916-11-01 | 1917-08-07 | Aaron E Suter | Elevator. |
| US1953353A (en) * | 1930-08-19 | 1934-04-03 | Associated Oil Company | Process of treating hydrocarbon oils |
| US2770580A (en) * | 1953-09-17 | 1956-11-13 | Sun Oil Co | Alkaline treatment of petroleum vapors |
| US2795532A (en) * | 1954-10-04 | 1957-06-11 | Sun Oil Co | Refining heavy mineral oil fractions with an anhydrous mixture of sodium hydroxide and potassium hydroxide |
| US2921023A (en) * | 1957-05-14 | 1960-01-12 | Pure Oil Co | Removal of naphthenic acids by hydrogenation with a molybdenum oxidesilica alumina catalyst |
| US3617501A (en) * | 1968-09-06 | 1971-11-02 | Exxon Research Engineering Co | Integrated process for refining whole crude oil |
| US3761534A (en) * | 1971-12-29 | 1973-09-25 | Dow Chemical Co | Removal of acidic contaminants from process streams |
| US3806437A (en) * | 1973-03-22 | 1974-04-23 | Petrolite Corp | Treatment of petroleum distillates containing naphthenic acids |
| US3847774A (en) * | 1973-06-22 | 1974-11-12 | Petrolite Corp | Purification of petroleum distillates containing naphthenic acids |
| US4033860A (en) * | 1975-09-10 | 1977-07-05 | Uop Inc. | Mercaptan conversion process |
| US4199440A (en) * | 1977-05-05 | 1980-04-22 | Uop Inc. | Trace acid removal in the pretreatment of petroleum distillate |
| US4300995A (en) * | 1980-06-30 | 1981-11-17 | Exxon Research & Engineering Co. | Oxygen-alkylation of carbonous material and products thereof |
| US5011579A (en) * | 1990-01-16 | 1991-04-30 | Merichem Company | Neutral oil recovery process for the production of naphthenic acids |
| NO303837B1 (no) * | 1994-08-29 | 1998-09-07 | Norske Stats Oljeselskap | FremgangsmÕte for Õ fjerne hovedsakelig naftensyrer fra en hydrokarbonolje |
| DK0809683T3 (da) * | 1995-02-17 | 2002-03-04 | Exxonmobil Res & Eng Co | Termisk dekomponering af naphtensyrer |
-
1998
- 1998-08-11 US US09/132,295 patent/US5891325A/en not_active Expired - Fee Related
-
1999
- 1999-07-08 MY MYPI99002873A patent/MY115922A/en unknown
- 1999-07-16 JP JP2000565068A patent/JP2003534391A/ja active Pending
- 1999-07-16 CN CN99809440A patent/CN1312849A/zh active Pending
- 1999-07-16 AT AT99934076T patent/ATE236235T1/de not_active IP Right Cessation
- 1999-07-16 RU RU2001103893/04A patent/RU2207366C2/ru not_active IP Right Cessation
- 1999-07-16 EP EP99934076A patent/EP1109879B1/en not_active Expired - Lifetime
- 1999-07-16 CA CA002338623A patent/CA2338623A1/en not_active Abandoned
- 1999-07-16 ES ES99934076T patent/ES2194485T3/es not_active Expired - Lifetime
- 1999-07-16 BR BR9912882-9A patent/BR9912882A/pt not_active Application Discontinuation
- 1999-07-16 ID IDW20010560A patent/ID28396A/id unknown
- 1999-07-16 DK DK99934076T patent/DK1109879T3/da active
- 1999-07-16 DE DE69906549T patent/DE69906549T2/de not_active Expired - Fee Related
- 1999-07-16 WO PCT/US1999/016058 patent/WO2000009631A1/en not_active Application Discontinuation
- 1999-07-16 KR KR1020017001702A patent/KR20010088788A/ko not_active Application Discontinuation
- 1999-07-16 AU AU49991/99A patent/AU750406B2/en not_active Ceased
- 1999-08-02 AR ARP990103842A patent/AR022360A1/es active IP Right Grant
- 1999-08-17 TW TW088113759A patent/TW500796B/zh not_active IP Right Cessation
-
2001
- 2001-02-05 NO NO20010599A patent/NO315709B1/no not_active IP Right Cessation
-
2002
- 2002-01-16 HK HK02100333.4A patent/HK1039144A1/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN1312849A (zh) | 2001-09-12 |
| BR9912882A (pt) | 2001-05-08 |
| DK1109879T3 (da) | 2003-04-22 |
| CA2338623A1 (en) | 2000-02-24 |
| EP1109879B1 (en) | 2003-04-02 |
| RU2207366C2 (ru) | 2003-06-27 |
| AR022360A1 (es) | 2002-09-04 |
| DE69906549D1 (de) | 2003-05-08 |
| AU750406B2 (en) | 2002-07-18 |
| ID28396A (id) | 2001-05-17 |
| TW500796B (en) | 2002-09-01 |
| US5891325A (en) | 1999-04-06 |
| ATE236235T1 (de) | 2003-04-15 |
| JP2003534391A (ja) | 2003-11-18 |
| KR20010088788A (ko) | 2001-09-28 |
| ES2194485T3 (es) | 2003-11-16 |
| MY115922A (en) | 2003-09-30 |
| HK1039144A1 (zh) | 2002-04-12 |
| NO20010599D0 (no) | 2001-02-05 |
| EP1109879A1 (en) | 2001-06-27 |
| DE69906549T2 (de) | 2004-01-15 |
| AU4999199A (en) | 2000-03-06 |
| NO20010599L (no) | 2001-02-05 |
| WO2000009631A1 (en) | 2000-02-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM1K | Lapsed by not paying the annual fees |