NO20053893L - Fremgangsmate for a oppna fettsyrealkyleestere, kolofoniumsyrer og steroler fra ratallolje - Google Patents

Fremgangsmate for a oppna fettsyrealkyleestere, kolofoniumsyrer og steroler fra ratallolje

Info

Publication number
NO20053893L
NO20053893L NO20053893A NO20053893A NO20053893L NO 20053893 L NO20053893 L NO 20053893L NO 20053893 A NO20053893 A NO 20053893A NO 20053893 A NO20053893 A NO 20053893A NO 20053893 L NO20053893 L NO 20053893L
Authority
NO
Norway
Prior art keywords
sterols
fatty acid
alkyl esters
rosin acids
acid alkyl
Prior art date
Application number
NO20053893A
Other languages
English (en)
Inventor
Ulrich Schorken
Setsuo Sato
Henrique Jorge Sousa Sales
Hercules Peloggia
Peter Kempers
Sabine Both
Thomas Wolf
Original Assignee
Cognis Brasil Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cognis Brasil Ltd filed Critical Cognis Brasil Ltd
Publication of NO20053893L publication Critical patent/NO20053893L/no

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07JSTEROIDS
    • C07J51/00Normal steroids with unmodified cyclopenta(a)hydrophenanthrene skeleton not provided for in groups C07J1/00 - C07J43/00
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07JSTEROIDS
    • C07J75/00Processes for the preparation of steroids in general
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07JSTEROIDS
    • C07J9/00Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00Recovery of fats, fatty oils or fatty acids from waste materials
    • C11B13/005Recovery of fats, fatty oils or fatty acids from waste materials of residues of the fabrication of wood-cellulose (in particular tall-oil)
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08Refining
    • C11C1/10Refining by distillation
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/62Carboxylic acid esters
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/64Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436Fatty acid esters
    • C12P7/6445Glycerides
    • C12P7/6458Glycerides by transesterification, e.g. interesterification, ester interchange, alcoholysis or acidolysis
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/64Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436Fatty acid esters
    • C12P7/649Biodiesel, i.e. fatty acid alkyl esters
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/74Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Genetics & Genomics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Steroid Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Fats And Perfumes (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Det er beskrevet en fremgangsmåte for å oppnå fettsyrealkylestere, kolofoniumsyrer og steroler fra råtallolje (CTO), som er kjennetegnet ved følgende trinn: (a) omsetning av de frie fettsyrene til stede i CTO med lavere alkoholer; (b) forestring av sterolene i CTO med borsyre eller ttansforestring med katalysator; (c) separering av fettsyrelaverealkylesteme og kolofoniumsyrene fra de gjenværende sterolboratesteme eller sterolesteme av fettsyrer for å fremstille en sttøm av sterolestere; (d) separering av fettsyrealkylesteme fra kolofoniumsyrene for å danne en første strøm av fettsyrealkylestere og en andre sttøm av kolofoniumsyrer; og (e) omdanning av nevnte sterolestere til de fiie steroler for å frembringe en ttedje sttøm av fiie steroler.
NO20053893A 2003-02-21 2005-08-19 Fremgangsmate for a oppna fettsyrealkyleestere, kolofoniumsyrer og steroler fra ratallolje NO20053893L (no)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PCT/BR2003/000024 WO2004074233A1 (en) 2003-02-21 2003-02-21 Process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil
PCT/BR2004/000016 WO2004080942A1 (en) 2003-02-21 2004-02-20 Process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil

Publications (1)

Publication Number Publication Date
NO20053893L true NO20053893L (no) 2005-08-19

Family

ID=32873322

Family Applications (2)

Application Number Title Priority Date Filing Date
NO20053894A NO20053894L (no) 2003-02-21 2005-08-19 Fremgangsmate for a oppna fettsyrealkylestere, kolofoniumsyrer og steroler fra ratallolje
NO20053893A NO20053893L (no) 2003-02-21 2005-08-19 Fremgangsmate for a oppna fettsyrealkyleestere, kolofoniumsyrer og steroler fra ratallolje

Family Applications Before (1)

Application Number Title Priority Date Filing Date
NO20053894A NO20053894L (no) 2003-02-21 2005-08-19 Fremgangsmate for a oppna fettsyrealkylestere, kolofoniumsyrer og steroler fra ratallolje

Country Status (11)

Country Link
US (2) US20070015904A1 (no)
EP (2) EP1594834B1 (no)
JP (2) JP2006518335A (no)
AT (2) ATE463477T1 (no)
AU (1) AU2003303929A1 (no)
BR (2) BRPI0318115B8 (no)
CA (2) CA2514700A1 (no)
DE (2) DE60332053D1 (no)
ES (2) ES2342936T3 (no)
NO (2) NO20053894L (no)
WO (2) WO2004074233A1 (no)

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JP2009513771A (ja) * 2005-10-26 2009-04-02 サンパイン・アクチボラゲット 粗トールオイルから得られる自動車燃料およびファインケミカル
US7695532B2 (en) * 2005-11-16 2010-04-13 The Research Foundation Of State University Of New York Process for making biodiesel from crude tall oil
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US7540889B2 (en) * 2006-07-11 2009-06-02 Bluekey Energy Inc. Production of a refinery feedstock from soaps produced during a chemical pulping process
JP5238147B2 (ja) * 2006-07-31 2013-07-17 ハリマ化成株式会社 トール脂肪酸エステル、その製造方法およびその用途
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WO2008112910A1 (en) 2007-03-14 2008-09-18 Endicott Biofuels Ii, Llc Methods for producing triol ethers by reactive distillation
EP2134819A4 (en) 2007-03-14 2016-11-16 Endicott Biofuels Ii Llc PREPARATION OF BIODIESEL FUELS WITH LOW GLYCEROL AND SULFUR CONTENT
WO2009017958A1 (en) 2007-07-31 2009-02-05 Endicott Biofuels Ii, Llc Production of renewable diesel by pyrolysis and esterification
WO2009029344A1 (en) * 2007-08-27 2009-03-05 Endicott Biofuels Ii, Llc Production of ester-based fuels such as biodiesel from renewable starting materials
US9221869B2 (en) 2008-03-10 2015-12-29 Sunpine Ab Recovery of phytosterols from residual vegetable oil streams
FI125590B (en) 2008-04-10 2015-12-15 Neste Oyj A process for the preparation of a composition for the preparation of pinosylvine and its compounds, a composition for the preparation of stilbene compounds, a process for the recovery of stilbene compounds, and fatty acid and resin acid esters of pinosylvine and its monomethyl ether
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FI126337B (fi) 2010-03-26 2016-10-14 Forchem Oy Menetelmä mäntyöljypien hyödyntämiseksi
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Also Published As

Publication number Publication date
BR0318115B1 (pt) 2013-11-12
BRPI0407689B1 (pt) 2013-07-02
CA2514700A1 (en) 2004-09-02
ES2342936T3 (es) 2010-07-19
JP2006518335A (ja) 2006-08-10
WO2004074233A1 (en) 2004-09-02
WO2004080942B1 (en) 2004-10-28
ATE463477T1 (de) 2010-04-15
EP1613581A1 (en) 2006-01-11
US20060235198A1 (en) 2006-10-19
US20070015904A1 (en) 2007-01-18
EP1613581B1 (en) 2008-10-29
EP1594834B1 (en) 2010-04-07
ATE412626T1 (de) 2008-11-15
DE602004017442D1 (de) 2008-12-11
ES2315639T3 (es) 2009-04-01
CA2516598A1 (en) 2004-09-23
BRPI0407689A (pt) 2006-03-01
WO2004080942A1 (en) 2004-09-23
NO20053894L (no) 2005-08-19
CA2516598C (en) 2012-08-07
BRPI0318115B8 (pt) 2016-05-17
US9079845B2 (en) 2015-07-14
AU2003303929A1 (en) 2004-09-09
JP4484865B2 (ja) 2010-06-16
BR0318115A (pt) 2006-02-07
JP2006518768A (ja) 2006-08-17
DE60332053D1 (de) 2010-05-20
EP1594834A1 (en) 2005-11-16

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