DE602004017442D1 - Verfahren zur gewinnung von fettsäurealkylestern, harzsäuren und sterinen aus rohtallöl - Google Patents

Verfahren zur gewinnung von fettsäurealkylestern, harzsäuren und sterinen aus rohtallöl

Info

Publication number
DE602004017442D1
DE602004017442D1 DE200460017442 DE602004017442T DE602004017442D1 DE 602004017442 D1 DE602004017442 D1 DE 602004017442D1 DE 200460017442 DE200460017442 DE 200460017442 DE 602004017442 T DE602004017442 T DE 602004017442T DE 602004017442 D1 DE602004017442 D1 DE 602004017442D1
Authority
DE
Germany
Prior art keywords
fatty acid
esters
sterols
stream
acid alkyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE200460017442
Other languages
English (en)
Inventor
Setsuo Sato
Sales Henrique Jorge Sousa
Hercules Peloggia
Peter Kempers
Sabine Both
Ulrich Schoerken
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cognis IP Management GmbH
Original Assignee
Cognis IP Management GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cognis IP Management GmbH filed Critical Cognis IP Management GmbH
Publication of DE602004017442D1 publication Critical patent/DE602004017442D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07JSTEROIDS
    • C07J51/00Normal steroids with unmodified cyclopenta(a)hydrophenanthrene skeleton not provided for in groups C07J1/00 - C07J43/00
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07JSTEROIDS
    • C07J75/00Processes for the preparation of steroids in general
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07JSTEROIDS
    • C07J9/00Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00Recovery of fats, fatty oils or fatty acids from waste materials
    • C11B13/005Recovery of fats, fatty oils or fatty acids from waste materials of residues of the fabrication of wood-cellulose (in particular tall-oil)
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08Refining
    • C11C1/10Refining by distillation
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/62Carboxylic acid esters
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/64Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436Fatty acid esters
    • C12P7/6445Glycerides
    • C12P7/6458Glycerides by transesterification, e.g. interesterification, ester interchange, alcoholysis or acidolysis
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/64Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436Fatty acid esters
    • C12P7/649Biodiesel, i.e. fatty acid alkyl esters
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/74Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • Genetics & Genomics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Steroid Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Fats And Perfumes (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE200460017442 2003-02-21 2004-02-20 Verfahren zur gewinnung von fettsäurealkylestern, harzsäuren und sterinen aus rohtallöl Expired - Lifetime DE602004017442D1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PCT/BR2003/000024 WO2004074233A1 (en) 2003-02-21 2003-02-21 Process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil
PCT/BR2004/000016 WO2004080942A1 (en) 2003-02-21 2004-02-20 Process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil

Publications (1)

Publication Number Publication Date
DE602004017442D1 true DE602004017442D1 (de) 2008-12-11

Family

ID=32873322

Family Applications (2)

Application Number Title Priority Date Filing Date
DE60332053T Expired - Lifetime DE60332053D1 (de) 2003-02-21 2003-02-21 Verfahren zur gewinnung von fettsäurealkylestern, harzsäuren und sterinen aus rohtallöl
DE200460017442 Expired - Lifetime DE602004017442D1 (de) 2003-02-21 2004-02-20 Verfahren zur gewinnung von fettsäurealkylestern, harzsäuren und sterinen aus rohtallöl

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DE60332053T Expired - Lifetime DE60332053D1 (de) 2003-02-21 2003-02-21 Verfahren zur gewinnung von fettsäurealkylestern, harzsäuren und sterinen aus rohtallöl

Country Status (11)

Country Link
US (2) US20070015904A1 (de)
EP (2) EP1594834B1 (de)
JP (2) JP2006518335A (de)
AT (2) ATE463477T1 (de)
AU (1) AU2003303929A1 (de)
BR (2) BRPI0318115B8 (de)
CA (2) CA2514700A1 (de)
DE (2) DE60332053D1 (de)
ES (2) ES2342936T3 (de)
NO (2) NO20053894L (de)
WO (2) WO2004074233A1 (de)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
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ES2342936T3 (es) * 2003-02-21 2010-07-19 Cognis Ip Management Gmbh Procedimiento para obtener esteres alquilicos de acido graso, acidos de resina de trementina y esteroles a partir de taloil en bruto.
EP1951852B1 (de) * 2005-10-26 2016-04-13 SunPine AB Kraftfahrzeug-brennstoff und feinchemikalien aus rohtallöl
US7695532B2 (en) * 2005-11-16 2010-04-13 The Research Foundation Of State University Of New York Process for making biodiesel from crude tall oil
JP4914113B2 (ja) * 2006-05-11 2012-04-11 ハリマ化成株式会社 ステロール類の製造方法
US7540889B2 (en) * 2006-07-11 2009-06-02 Bluekey Energy Inc. Production of a refinery feedstock from soaps produced during a chemical pulping process
JP5238147B2 (ja) * 2006-07-31 2013-07-17 ハリマ化成株式会社 トール脂肪酸エステル、その製造方法およびその用途
FI20070137A0 (fi) 2007-02-15 2007-02-15 Raisio Benecol Oy Menetelmä rasvahappojen, hartsihappojen ja sterolien eristämiseksi mäntyöljypiestä
CN103540412A (zh) 2007-03-14 2014-01-29 恩迪科特生物燃料Ii有限责任公司 低甘油低硫生物柴油燃料的生产
AU2008224996B2 (en) 2007-03-14 2011-12-15 Endicott Biofuels Ii, Llc Production of biodiesel fuels which are low in glycerin and sulfur
US8105399B2 (en) 2007-07-31 2012-01-31 Endicott Biofuels Ii, Llc Production of renewable diesel by pyrolysis and esterification
US8105398B2 (en) * 2007-08-27 2012-01-31 Endicott Biofuels Ii, Llc Production of ester-based fuels such as biodiesel from renewable starting materials
EP2252626B1 (de) 2008-03-10 2014-07-23 SunPine AB Rückgewinnung von phytosterolen aus restpflanzenölströmen
FI125590B (en) * 2008-04-10 2015-12-15 Neste Oyj A process for the preparation of a composition for the preparation of pinosylvine and its compounds, a composition for the preparation of stilbene compounds, a process for the recovery of stilbene compounds, and fatty acid and resin acid esters of pinosylvine and its monomethyl ether
FI120737B (fi) * 2008-06-18 2010-02-15 Forchem Oy Menetelmä ja laitteistosovitelma moottoripolttoaineen valmistamiseksi
FI126337B (fi) 2010-03-26 2016-10-14 Forchem Oy Menetelmä mäntyöljypien hyödyntämiseksi
FI20106252A0 (fi) 2010-11-26 2010-11-26 Upm Kymmene Corp Menetelmä ja systeemi polttoainekomponenttien valmistamiseksi
FI126958B (en) 2015-05-25 2017-08-31 Forchem Oyj Production of sterols
SE542797C2 (en) * 2018-12-11 2020-07-07 Stora Enso Oyj Fractionation of crude tall oil
CN109825359B (zh) * 2019-04-04 2021-05-25 南京林业大学 一种利用造纸黑液制备生物基润滑油的方法及专用生产装置

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US2415301A (en) * 1944-04-03 1947-02-04 Benjamin Clayton Refining of glyceride oils and recovery of by-products
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US3496159A (en) * 1967-03-27 1970-02-17 Spence & Green Chem Co Esterification of fatty acids of tall oil in a horizontal distillation column and condenser
US3691211A (en) * 1970-12-07 1972-09-12 Procter & Gamble Process for preparing sterols from tall oil pitch
US3804819A (en) * 1972-05-03 1974-04-16 Scm Corp Recovery of fatty acids from tall oil heads
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GB1532177A (en) * 1976-06-08 1978-11-15 Kuraray Co Isomerisation of alkenols
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WO2001029060A2 (en) * 1999-10-21 2001-04-26 The Board Of Regents For Oklahoma State University Sterol esters of conjugated linoleic acids and process for their production
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DE10050403A1 (de) * 2000-10-12 2002-04-25 Goldschmidt Ag Th Enzymatische Herstellung von bei Raumtemperatur festen Hydroxyfettsäureestern mehrwertiger Alkohole
ATE391135T1 (de) * 2001-09-07 2008-04-15 Raisio Staest Oy Verfahren zur isolierung von sterinen und/oder wachsalkoholen aus talölprodukten
ES2342936T3 (es) * 2003-02-21 2010-07-19 Cognis Ip Management Gmbh Procedimiento para obtener esteres alquilicos de acido graso, acidos de resina de trementina y esteroles a partir de taloil en bruto.

Also Published As

Publication number Publication date
CA2516598C (en) 2012-08-07
BRPI0407689B1 (pt) 2013-07-02
WO2004080942A1 (en) 2004-09-23
AU2003303929A1 (en) 2004-09-09
EP1594834A1 (de) 2005-11-16
JP2006518768A (ja) 2006-08-17
EP1594834B1 (de) 2010-04-07
JP4484865B2 (ja) 2010-06-16
ATE412626T1 (de) 2008-11-15
NO20053894L (no) 2005-08-19
BR0318115B1 (pt) 2013-11-12
US9079845B2 (en) 2015-07-14
BRPI0407689A (pt) 2006-03-01
JP2006518335A (ja) 2006-08-10
DE60332053D1 (de) 2010-05-20
NO20053893L (no) 2005-08-19
ATE463477T1 (de) 2010-04-15
EP1613581B1 (de) 2008-10-29
CA2516598A1 (en) 2004-09-23
WO2004074233A1 (en) 2004-09-02
ES2315639T3 (es) 2009-04-01
BRPI0318115B8 (pt) 2016-05-17
CA2514700A1 (en) 2004-09-02
EP1613581A1 (de) 2006-01-11
ES2342936T3 (es) 2010-07-19
US20070015904A1 (en) 2007-01-18
WO2004080942B1 (en) 2004-10-28
US20060235198A1 (en) 2006-10-19
BR0318115A (pt) 2006-02-07

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