NO20053894L - Fremgangsmate for a oppna fettsyrealkylestere, kolofoniumsyrer og steroler fra ratallolje - Google Patents

Fremgangsmate for a oppna fettsyrealkylestere, kolofoniumsyrer og steroler fra ratallolje

Info

Publication number
NO20053894L
NO20053894L NO20053894A NO20053894A NO20053894L NO 20053894 L NO20053894 L NO 20053894L NO 20053894 A NO20053894 A NO 20053894A NO 20053894 A NO20053894 A NO 20053894A NO 20053894 L NO20053894 L NO 20053894L
Authority
NO
Norway
Prior art keywords
fatty acid
sterols
rosin acids
alkyl esters
cto
Prior art date
Application number
NO20053894A
Other languages
English (en)
Inventor
Ulrich Schorken
Setsuo Sato
Henrique Jorge Sousa Sales
Hercules Peloggia
Peter Kempers
Sabine Both
Thomas Wolf
Original Assignee
Cognis Brasil Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cognis Brasil Ltd filed Critical Cognis Brasil Ltd
Publication of NO20053894L publication Critical patent/NO20053894L/no

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J51/00—Normal steroids with unmodified cyclopenta(a)hydrophenanthrene skeleton not provided for in groups C07J1/00 - C07J43/00
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J75/00—Processes for the preparation of steroids in general
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J9/00—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
    • C11B13/005—Recovery of fats, fatty oils or fatty acids from waste materials of residues of the fabrication of wood-cellulose (in particular tall-oil)
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C11C1/10—Refining by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/62—Carboxylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436—Fatty acid esters
    • C12P7/6445—Glycerides
    • C12P7/6458—Glycerides by transesterification, e.g. interesterification, ester interchange, alcoholysis or acidolysis
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436—Fatty acid esters
    • C12P7/649—Biodiesel, i.e. fatty acid alkyl esters
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • Genetics & Genomics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Steroid Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Fats And Perfumes (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Det er beskrevet en fremgangsmåte for å oppnå fettsyrealkylestere, kolofoniumsyrer og steroler fra råtallolje (CTO), som er kjennetegnet ved følgende trinn: (b) omsetning av den fiie fettsyren til stede i CTO med lavere alkoholer; (c) separering av fettsyrelaverealkylesteme som derved oppnås fra gjenværende CTO for å fremstille en første sttøm av fettsyreestere; (d) forestring av sterolene i det gjenværende CTO med borsyre; (e) separering av de gjenværende kolofoniumsyrene fra sterolboratene på forhånd oppnådd for å fremstille en andre sttøm av kolofoniumsyrer; og (f) omdanning av nevnte sterolborater til de frie sterolene for å fremstille en ttedje sttøm av fiie steroler.
NO20053894A 2003-02-21 2005-08-19 Fremgangsmate for a oppna fettsyrealkylestere, kolofoniumsyrer og steroler fra ratallolje NO20053894L (no)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/BR2003/000024 WO2004074233A1 (en) 2003-02-21 2003-02-21 Process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil

Publications (1)

Publication Number Publication Date
NO20053894L true NO20053894L (no) 2005-08-19

Family

ID=32873322

Family Applications (2)

Application Number Title Priority Date Filing Date
NO20053894A NO20053894L (no) 2003-02-21 2005-08-19 Fremgangsmate for a oppna fettsyrealkylestere, kolofoniumsyrer og steroler fra ratallolje
NO20053893A NO20053893L (no) 2003-02-21 2005-08-19 Fremgangsmate for a oppna fettsyrealkyleestere, kolofoniumsyrer og steroler fra ratallolje

Family Applications After (1)

Application Number Title Priority Date Filing Date
NO20053893A NO20053893L (no) 2003-02-21 2005-08-19 Fremgangsmate for a oppna fettsyrealkyleestere, kolofoniumsyrer og steroler fra ratallolje

Country Status (11)

Country Link
US (2) US20070015904A1 (no)
EP (2) EP1594834B1 (no)
JP (2) JP2006518335A (no)
AT (2) ATE463477T1 (no)
AU (1) AU2003303929A1 (no)
BR (2) BRPI0318115B8 (no)
CA (2) CA2514700A1 (no)
DE (2) DE60332053D1 (no)
ES (2) ES2342936T3 (no)
NO (2) NO20053894L (no)
WO (2) WO2004074233A1 (no)

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US7695532B2 (en) * 2005-11-16 2010-04-13 The Research Foundation Of State University Of New York Process for making biodiesel from crude tall oil
JP4914113B2 (ja) * 2006-05-11 2012-04-11 ハリマ化成株式会社 ステロール類の製造方法
US7540889B2 (en) * 2006-07-11 2009-06-02 Bluekey Energy Inc. Production of a refinery feedstock from soaps produced during a chemical pulping process
JP5238147B2 (ja) * 2006-07-31 2013-07-17 ハリマ化成株式会社 トール脂肪酸エステル、その製造方法およびその用途
FI20070137A0 (fi) 2007-02-15 2007-02-15 Raisio Benecol Oy Menetelmä rasvahappojen, hartsihappojen ja sterolien eristämiseksi mäntyöljypiestä
CN101641429B (zh) 2007-03-14 2013-07-17 恩迪科特生物燃料Ⅱ有限责任公司 低甘油低硫生物柴油燃料的生产
US20080228011A1 (en) 2007-03-14 2008-09-18 Endicott Biofuels Ii, Llc Methods for Producing Triol Ethers by Reactive Distillation
US8105399B2 (en) 2007-07-31 2012-01-31 Endicott Biofuels Ii, Llc Production of renewable diesel by pyrolysis and esterification
US8105398B2 (en) * 2007-08-27 2012-01-31 Endicott Biofuels Ii, Llc Production of ester-based fuels such as biodiesel from renewable starting materials
CA2717956C (en) 2008-03-10 2017-01-10 Sunpine Ab Recovery of phytosterols from residual vegetable oil streams
FI125590B (en) * 2008-04-10 2015-12-15 Neste Oyj A process for the preparation of a composition for the preparation of pinosylvine and its compounds, a composition for the preparation of stilbene compounds, a process for the recovery of stilbene compounds, and fatty acid and resin acid esters of pinosylvine and its monomethyl ether
FI120737B (fi) * 2008-06-18 2010-02-15 Forchem Oy Menetelmä ja laitteistosovitelma moottoripolttoaineen valmistamiseksi
FI126337B (fi) 2010-03-26 2016-10-14 Forchem Oy Menetelmä mäntyöljypien hyödyntämiseksi
FI20106252A0 (fi) 2010-11-26 2010-11-26 Upm Kymmene Corp Menetelmä ja systeemi polttoainekomponenttien valmistamiseksi
FI126958B (en) * 2015-05-25 2017-08-31 Forchem Oyj Production of sterols
SE542797C2 (en) * 2018-12-11 2020-07-07 Stora Enso Oyj Fractionation of crude tall oil
CN109825359B (zh) * 2019-04-04 2021-05-25 南京林业大学 一种利用造纸黑液制备生物基润滑油的方法及专用生产装置

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CA2514700A1 (en) * 2003-02-21 2004-09-02 Setsuo Sato Process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil

Also Published As

Publication number Publication date
DE60332053D1 (de) 2010-05-20
ES2342936T3 (es) 2010-07-19
EP1594834A1 (en) 2005-11-16
CA2514700A1 (en) 2004-09-02
EP1613581B1 (en) 2008-10-29
WO2004080942A1 (en) 2004-09-23
WO2004074233A1 (en) 2004-09-02
CA2516598A1 (en) 2004-09-23
BRPI0407689B1 (pt) 2013-07-02
US20060235198A1 (en) 2006-10-19
EP1613581A1 (en) 2006-01-11
BR0318115B1 (pt) 2013-11-12
JP2006518335A (ja) 2006-08-10
EP1594834B1 (en) 2010-04-07
US9079845B2 (en) 2015-07-14
NO20053893L (no) 2005-08-19
JP2006518768A (ja) 2006-08-17
ATE463477T1 (de) 2010-04-15
BR0318115A (pt) 2006-02-07
DE602004017442D1 (de) 2008-12-11
AU2003303929A1 (en) 2004-09-09
CA2516598C (en) 2012-08-07
US20070015904A1 (en) 2007-01-18
ATE412626T1 (de) 2008-11-15
JP4484865B2 (ja) 2010-06-16
WO2004080942B1 (en) 2004-10-28
BRPI0318115B8 (pt) 2016-05-17
BRPI0407689A (pt) 2006-03-01
ES2315639T3 (es) 2009-04-01

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