NO150302B - DISPENSES FOR PHEROMONS - Google Patents
DISPENSES FOR PHEROMONS Download PDFInfo
- Publication number
- NO150302B NO150302B NO792405A NO792405A NO150302B NO 150302 B NO150302 B NO 150302B NO 792405 A NO792405 A NO 792405A NO 792405 A NO792405 A NO 792405A NO 150302 B NO150302 B NO 150302B
- Authority
- NO
- Norway
- Prior art keywords
- verbenol
- cis
- pheromone
- dispenser
- methylbutenol
- Prior art date
Links
- 239000003016 pheromone Substances 0.000 claims description 15
- HNVRRHSXBLFLIG-UHFFFAOYSA-N 3-hydroxy-3-methylbut-1-ene Chemical compound CC(C)(O)C=C HNVRRHSXBLFLIG-UHFFFAOYSA-N 0.000 claims description 14
- WONIGEXYPVIKFS-UHFFFAOYSA-N (+)-cis-Verbenol Natural products CC1=CC(O)C2C(C)(C)C1C2 WONIGEXYPVIKFS-UHFFFAOYSA-N 0.000 claims description 9
- WONIGEXYPVIKFS-YIZRAAEISA-N (1s,2s,5s)-4,6,6-trimethylbicyclo[3.1.1]hept-3-en-2-ol Chemical compound CC1=C[C@H](O)[C@@H]2C(C)(C)[C@H]1C2 WONIGEXYPVIKFS-YIZRAAEISA-N 0.000 claims description 9
- 241000545593 Scolytinae Species 0.000 claims description 7
- 239000004698 Polyethylene Substances 0.000 claims description 5
- 239000011888 foil Substances 0.000 claims description 5
- -1 polyethylene Polymers 0.000 claims description 5
- 229920000573 polyethylene Polymers 0.000 claims description 5
- BZAZNULYLRVMSW-UHFFFAOYSA-N 2-Methyl-2-buten-3-ol Natural products CC(C)=C(C)O BZAZNULYLRVMSW-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 2
- VBPSVYDSYVJIPX-UHFFFAOYSA-N methylbutenol Natural products CCC=C(C)O VBPSVYDSYVJIPX-UHFFFAOYSA-N 0.000 description 6
- 241000218657 Picea Species 0.000 description 3
- 239000002775 capsule Substances 0.000 description 3
- 238000003466 welding Methods 0.000 description 3
- 241000254173 Coleoptera Species 0.000 description 2
- 241000546120 Ips typographus Species 0.000 description 2
- ATFPTLNYZBJXFD-UHFFFAOYSA-N 2-methylbut-3-en-2-ol pent-2-en-2-ol Chemical compound CC(=CCC)O.CC(C)(C=C)O ATFPTLNYZBJXFD-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- JLYXXMFPNIAWKQ-GNIYUCBRSA-N gamma-hexachlorocyclohexane Chemical compound Cl[C@H]1[C@H](Cl)[C@@H](Cl)[C@@H](Cl)[C@H](Cl)[C@H]1Cl JLYXXMFPNIAWKQ-GNIYUCBRSA-N 0.000 description 1
- JLYXXMFPNIAWKQ-UHFFFAOYSA-N gamma-hexachlorocyclohexane Natural products ClC1C(Cl)C(Cl)C(Cl)C(Cl)C1Cl JLYXXMFPNIAWKQ-UHFFFAOYSA-N 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 229960002809 lindane Drugs 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 229920006255 plastic film Polymers 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N29/00—Biocides, pest repellants or attractants, or plant growth regulators containing halogenated hydrocarbons
- A01N29/04—Halogen directly attached to a carbocyclic ring system
- A01N29/06—Hexachlorocyclohexane
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/18—Vapour or smoke emitting compositions with delayed or sustained release
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/06—Oxygen or sulfur directly attached to a cycloaliphatic ring system
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)
Description
Gjenstanden for foreliggende oppfinnelse er definert i kravet. The object of the present invention is defined in the claim.
Det er kjent at forbindelsene (S)-cis-verbenol med formelen It is known that the compounds (S)-cis-verbenol with the formula
og metylbutenol (2-metyl-3-buten-2-ol) i kombinasjon virker som lokke sto f f (feromon) for barkbiller (stor granbarkbille, Ips typographus). and methylbutenol (2-methyl-3-buten-2-ol) in combination acts as a lure sto f f (pheromone) for bark beetles (large spruce bark beetle, Ips typographus).
For anvendelse som feromon må blandingen av de aktive stoffer tilberedes slik at feromonet avgis fra preparatet jevnt over et tidsrom på minst 4 uker. Dessuten bør mengden av og mengdeforholdet mellom de to komponenter ligge mest mulig konstant i-det området hvor den gunstigste lokkevirkning oppnås. Det har vist seg fordelaktig når 0,01-0,1 mg. (3)-cis-verbenol og 0,5-2 mg. metylbutenol avgis pr. time. For use as a pheromone, the mixture of the active substances must be prepared so that the pheromone is released from the preparation evenly over a period of at least 4 weeks. Moreover, the quantity of and the quantity ratio between the two components should remain as constant as possible in the area where the most favorable luring effect is achieved. It has proven beneficial when 0.01-0.1 mg. (3)-cis-verbenol and 0.5-2 mg. methylbutenol is released per hour.
For å spre feromoner har man hittil enten benyttet polyetylenkapsler forsynt med hull eller glasskapillarrør inne-holdende en oppløsning av (S)-cis-verbenol i metylbutenol. Denne anvendeIsesform har den ulempe at feromonet avgis i for stor mengde og ukontrollerbart ujevnt. Dessuten kreves mye arbeid, ef-tersom feromonoppløsningen må efterfylles idet man ellers ikke oppnår den nødvendige varighet av utspredningen. To spread pheromones, either polyethylene capsules with holes or glass capillary tubes containing a solution of (S)-cis-verbenol in methylbutenol have been used. This form of application has the disadvantage that the pheromone is released in too large an amount and uncontrollably unevenly. In addition, a lot of work is required, as the pheromone solution must be refilled, otherwise the required duration of the spread will not be achieved.
Det er nu funnet at feromoner overraskende kan spres ut It has now been found that pheromones can be spread surprisingly
i den ønskede mengde og over et tilstrekkelig langt tidsrom hvis man inneslutter det i plastfolier av egnet art og tykkelse. in the desired amount and over a sufficiently long period of time if it is enclosed in plastic films of a suitable type and thickness.
Det kunne ikke forutsees at det på denne måte var mulig å få It could not be foreseen that in this way it was possible to get
spredd feromonet med hell, da det mellom komponentene består betydelige forskjeller med hensyn til damptrykk ((S)-cis-verbenol: k'P-20mmHg 12°°C; ^tylbutenol: k.p.76Q ^ 9<9>°C) og også med hensyn til molekylstruktur. spread the pheromone successfully, as there are significant differences between the components in terms of vapor pressure ((S)-cis-verbenol: k'P-20mmHg 12°°C; ^tylbutenol: b.p.76Q ^ 9<9>°C) and also with respect to molecular structure.
Oppfinnelsen angår således en dispenser for utspredning The invention thus relates to a dispenser for spreading
av barkbille-feromonene (S)-cis-verbenol og 2-metyl-3-buten-2-ol, hvilken dispenser er kjennetegnet ved at den omfatter en svamp impregnert med (S)-cis-verbenol og 2-metyl-3-buten-2-ol i vekt-forholdet 1:10 til 1:3.0, omhyllet av en polyetylenfolie med tykkelse 20 - lOO^um. of the bark beetle pheromones (S)-cis-verbenol and 2-methyl-3-buten-2-ol, which dispenser is characterized in that it comprises a sponge impregnated with (S)-cis-verbenol and 2-methyl-3- buten-2-ol in the weight ratio 1:10 to 1:3.0, enveloped by a polyethylene foil with a thickness of 20 - 100 µm.
En applikasjonsenhet ifølge oppfinnelsen (dispenser) kan fremstilles ved at man i et ca. 9 cm langt stykke av en slange av høytrykkpolyetylen (veggtykkelse ca. 50 ym, diameter ca. 5,5 cm) inneslutter ved sveising et 6 x 4 cm 2 stort, flere mm tykt svampstykke som er gjennombløtt med feromonoppløsning. Den ene sveisesømmen befinner seg ved enden av slangen, mens den andre er ca. 1,5 cm fra den andre enden av slangen, slik at man får et belte som kan anvendes til å feste dispenseren, f.eks. på fangsttreet. Som feromon anvendes oppløsningen av 100 mg (S)-cis-verbenol i 1900 mg metylbutenol pr. dispenser. Den biologiske virkning varer i minst 8 uker,- og avgivningshastighéten ligger ved ca. 0,025-0,04 mg/time; for (S)-cis-verbenol og ca. 1,0-2,2 mg/time for metylbutenol ved eh konstant temperatur på 25°C. An application unit according to the invention (dispenser) can be produced by using in an approx. A 9 cm long piece of high-pressure polyethylene hose (wall thickness approx. 50 ym, diameter approx. 5.5 cm) encloses, by welding, a 6 x 4 cm 2 large, several mm thick piece of sponge soaked with pheromone solution. One welding seam is located at the end of the hose, while the other is approx. 1.5 cm from the other end of the hose, so that you get a belt that can be used to attach the dispenser, e.g. on the catch tree. As a pheromone, the solution of 100 mg of (S)-cis-verbenol in 1900 mg of methylbutenol per dispenser. The biological effect lasts for at least 8 weeks, and the release rate is approx. 0.025-0.04 mg/hour; for (S)-cis-verbenol and approx. 1.0-2.2 mg/hour for methylbutenol at a constant temperature of 25°C.
Istedenfor det her anvendte mengdeforhold på 1:19, kan Instead of the quantity ratio of 1:19 used here, can
de to komponenter anvendes i andre forhold mellom 1:10 og 1:30. the two components are used in other ratios between 1:10 and 1:30.
Bestanddelene i den aktive kombinasjon kan på samme måte også innesluttes adskilt ved sveising. Ved anvendelse av forskjellige folietyper og folier av forskjellige tykkelser kan avgivningshastigheten og avgivningsforholdet eventuelt endres. The components of the active combination can in the same way also be contained separately by welding. When using different foil types and foils of different thicknesses, the dispensing speed and the dispensing ratio can possibly be changed.
For lagring holdes dispenseren hensiktsmessig i et For storage, the dispenser is conveniently kept in a
aluminiumetui for å unngå uønsket tap av feromon. aluminum case to avoid unwanted loss of pheromone.
Det nye middel anvendes slik at én eller flere dispensere festes på en granstamme i et granskogområde ved begynnelsen av billenes svermningstid. Istedenfor granstammer kan man som fangsttre også anvende ca. 2 m lange trestokker og også trær som har rødråte eller som har fått barken fjernet av vilt. Også inn-retninger som tjener som feller, kan anvendes som bærere for dispenserne. The new agent is used so that one or more dispensers are attached to a spruce trunk in a spruce forest area at the beginning of the beetles' swarming season. Instead of fir trunks, you can also use approx. 2 m long logs and also trees that have red rot or that have had their bark removed by game. Devices that serve as traps can also be used as carriers for the dispensers.
For å avlive barkbillene kan fangsttrærne hensiktsmessig behandles med et insekticid som er aktivt mot billene, f.eks. med lindan. To kill the bark beetles, the catch trees can be appropriately treated with an insecticide that is active against the beetles, e.g. with lindane.
Ved et sammenlignings forsøk i grankulturer viste det seg at over en periode på 8 uker og under like betingelser ble det med dispenserne ifølge oppfinnelsen tiltrukket like mange barkbiller som med de kjente kapsler med feromonoppløsning. Imidlertid måtte kapslene fylles påny med feromonoppløsning i den 5. uke. In a comparison test in spruce cultures, it turned out that over a period of 8 weeks and under the same conditions, the dispensers according to the invention attracted the same number of bark beetles as with the known capsules with pheromone solution. However, the capsules had to be refilled with pheromone solution in the 5th week.
Ved et forsøk med en dispenser som beskrevet ovenfor (1900 mg metylbutenol/100 mg S-cis-verbenol) ble i løpet av observasjonstiden 6 729 barkbiller tiltrukket og fanget. In an experiment with a dispenser as described above (1900 mg methylbutenol/100 mg S-cis-verbenol) during the observation period 6,729 bark beetles were attracted and caught.
Ved adskilt inneslutning av 2000 mg metylbutenol og By separately containing 2000 mg of methylbutenol and
50 mg krystallinsk S-cis-verbenol i 50 ym tykk polyetylenfolie 50 mg of crystalline S-cis-verbenol in 50 µm thick polyethylene foil
(avgivning ved konstant temperatur på 25°C: 18-35 yg/time) (release at a constant temperature of 25°C: 18-35 yg/hour)
utgjorde i det samme tidsrom antall fangede barkbiller 5220. in the same period, the number of bark beetles caught amounted to 5,220.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19782832248 DE2832248A1 (en) | 1978-07-22 | 1978-07-22 | DISPENSER FOR THE APPLICATION OF PHEROMONES |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO792405L NO792405L (en) | 1980-01-23 |
| NO150302B true NO150302B (en) | 1984-06-18 |
| NO150302C NO150302C (en) | 1984-09-26 |
Family
ID=6045090
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO792405A NO150302C (en) | 1978-07-22 | 1979-07-20 | DISPENSES FOR PHEROMONS |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS5519276A (en) |
| AT (1) | AT370584B (en) |
| CH (1) | CH642230A5 (en) |
| CS (1) | CS213311B2 (en) |
| DD (1) | DD144856A5 (en) |
| DE (1) | DE2832248A1 (en) |
| FI (1) | FI64492C (en) |
| FR (1) | FR2431254A1 (en) |
| NO (1) | NO150302C (en) |
| PL (1) | PL120659B1 (en) |
| SE (1) | SE446936B (en) |
| SU (1) | SU984393A3 (en) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2945655A1 (en) * | 1979-11-12 | 1981-05-21 | Celamerck Gmbh & Co Kg, 6507 Ingelheim | DEVICE FOR THE DELIVERY OF PHERMONES |
| IT1194595B (en) * | 1979-11-29 | 1988-09-22 | Montedison Spa | SOLID FORMULATIONS CONTAINING FERORMONES |
| IT1129711B (en) * | 1980-01-23 | 1986-06-11 | Montedison Spa | SOLID FORMULATIONS CONTAINING FERORMONES |
| JPS5991174A (en) * | 1982-11-15 | 1984-05-25 | Nitto Electric Ind Co Ltd | Preparation of tape with double-faced adhesive piece |
| NZ206613A (en) * | 1982-12-20 | 1987-01-23 | B J Morrison | Making pesticidal sheets |
| GB2150834B (en) * | 1983-10-08 | 1988-03-23 | Fumakilla Ltd | Pest control sheet and device for indicating the termination of its effectiveness |
| DE3430211A1 (en) * | 1984-08-17 | 1986-02-27 | Celamerck Gmbh & Co Kg, 6507 Ingelheim | INSECT LURE |
| DE3543297C2 (en) * | 1984-12-10 | 1994-10-27 | Shell Int Research | Process for controlling bark beetles |
| DE3541467A1 (en) * | 1985-11-23 | 1987-05-27 | Celamerck Gmbh & Co Kg | Insect attractant |
| JPS62181203A (en) * | 1986-02-05 | 1987-08-08 | Shin Etsu Chem Co Ltd | Simultaneous release controlling of sex pheromone of different insect pest |
| DE3628091A1 (en) * | 1986-08-19 | 1988-02-25 | Basf Ag | AGENTS, ESPECIALLY FOR THE DISTRIBUTION OF PHEROMONES |
| GB8906382D0 (en) * | 1989-03-20 | 1989-05-04 | Univ Southampton | Pheromone baits for social insects |
| DE3927243A1 (en) * | 1989-08-18 | 1991-02-21 | Basf Ag | DEVICE FOR COMBATING BORK BEETLES, IN PARTICULAR THE BOOK PRINTER |
| DE4343337A1 (en) * | 1993-12-18 | 1995-06-22 | Ulrich Wilhelm | Device for retaining bait for bark beetles |
| DE102004048579A1 (en) | 2004-10-04 | 2006-04-13 | Contitech Elastomer-Beschichtungen Gmbh | Material as a pheromone dispenser for attracting in particular spruce bark beetles using a carrier material |
| JP4719851B2 (en) * | 2005-02-18 | 2011-07-06 | 独立行政法人森林総合研究所 | Oak oyster beetle assemblage pheromone, Oak moth beetle attractant and pheromone trap containing the pheromone |
| KR101121365B1 (en) | 2007-04-26 | 2012-03-09 | 히다치 가세고교 가부시끼가이샤 | Process for production of multilayer film |
| WO2010076316A1 (en) | 2008-12-30 | 2010-07-08 | Basf Se | Pheromone dispenser |
| US9173389B2 (en) | 2010-11-18 | 2015-11-03 | Auburn University | Systems and methods to deliver and maintain volatile compounds |
| US20120126024A1 (en) | 2010-11-18 | 2012-05-24 | Boyd Maurice M | Methods and systems to deliver volatile compounds |
| US9185897B2 (en) | 2010-11-18 | 2015-11-17 | Auburn University | Methods to deliver and maintain volatile compounds |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AR220507A1 (en) * | 1975-09-26 | 1980-11-14 | Albany Int Corp | DEVICE TO SPREAD A VAPORIZABLE MATERIAL BY DIFFUSION OF STEAM, IN A DEFAULT PROPORTION |
| NO138235C (en) * | 1977-01-13 | 1978-08-02 | Borregaard Ind | PREPARATION FOR ATTRACTION OF SPRINE BARKET BEETLES |
-
1978
- 1978-07-22 DE DE19782832248 patent/DE2832248A1/en not_active Ceased
-
1979
- 1979-07-09 AT AT0475779A patent/AT370584B/en active
- 1979-07-17 CS CS795002A patent/CS213311B2/en unknown
- 1979-07-18 FR FR7918642A patent/FR2431254A1/en not_active Withdrawn
- 1979-07-19 CH CH673779A patent/CH642230A5/en not_active IP Right Cessation
- 1979-07-19 DD DD79214472A patent/DD144856A5/en not_active IP Right Cessation
- 1979-07-20 NO NO792405A patent/NO150302C/en unknown
- 1979-07-20 PL PL1979217278A patent/PL120659B1/en unknown
- 1979-07-20 SU SU792789507A patent/SU984393A3/en active
- 1979-07-20 FI FI792274A patent/FI64492C/en not_active IP Right Cessation
- 1979-07-20 JP JP9314679A patent/JPS5519276A/en active Pending
- 1979-07-20 SE SE7906258A patent/SE446936B/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE2832248A1 (en) | 1980-01-31 |
| CH642230A5 (en) | 1984-04-13 |
| SE446936B (en) | 1986-10-20 |
| FI792274A (en) | 1980-01-23 |
| PL217278A1 (en) | 1980-05-05 |
| CS213311B2 (en) | 1982-04-09 |
| FR2431254A1 (en) | 1980-02-15 |
| FI64492B (en) | 1983-08-31 |
| NO150302C (en) | 1984-09-26 |
| AT370584B (en) | 1983-04-11 |
| ATA475779A (en) | 1982-09-15 |
| FI64492C (en) | 1983-12-12 |
| SE7906258L (en) | 1980-01-23 |
| PL120659B1 (en) | 1982-03-31 |
| DD144856A5 (en) | 1980-11-12 |
| SU984393A3 (en) | 1982-12-23 |
| NO792405L (en) | 1980-01-23 |
| JPS5519276A (en) | 1980-02-09 |
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