NO136489B - - Google Patents
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- Publication number
- NO136489B NO136489B NO3191/72A NO319172A NO136489B NO 136489 B NO136489 B NO 136489B NO 3191/72 A NO3191/72 A NO 3191/72A NO 319172 A NO319172 A NO 319172A NO 136489 B NO136489 B NO 136489B
- Authority
- NO
- Norway
- Prior art keywords
- mercury
- washing liquid
- sulfuric acid
- acid
- gas
- Prior art date
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 256
- 238000000034 method Methods 0.000 claims abstract description 68
- 238000004519 manufacturing process Methods 0.000 claims abstract description 32
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 223
- 229910052753 mercury Inorganic materials 0.000 claims description 189
- 239000007789 gas Substances 0.000 claims description 127
- 238000010521 absorption reaction Methods 0.000 claims description 115
- 238000005406 washing Methods 0.000 claims description 70
- 229910052751 metal Inorganic materials 0.000 claims description 18
- 239000002184 metal Substances 0.000 claims description 18
- 239000000463 material Substances 0.000 claims description 13
- 239000003595 mist Substances 0.000 claims description 13
- QXKXDIKCIPXUPL-UHFFFAOYSA-N sulfanylidenemercury Chemical compound [Hg]=S QXKXDIKCIPXUPL-UHFFFAOYSA-N 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 239000010949 copper Substances 0.000 claims description 11
- 229910052725 zinc Inorganic materials 0.000 claims description 10
- 239000011701 zinc Substances 0.000 claims description 10
- 239000011669 selenium Substances 0.000 claims description 9
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 8
- 229910052802 copper Inorganic materials 0.000 claims description 8
- 229910052711 selenium Inorganic materials 0.000 claims description 8
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 7
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 7
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 7
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 238000001556 precipitation Methods 0.000 claims description 6
- -1 silver ions Chemical class 0.000 claims description 6
- 229910052783 alkali metal Inorganic materials 0.000 claims description 5
- 150000001340 alkali metals Chemical class 0.000 claims description 5
- 239000003344 environmental pollutant Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 231100000719 pollutant Toxicity 0.000 claims description 5
- 239000002244 precipitate Substances 0.000 claims description 5
- YQMLDSWXEQOSPP-UHFFFAOYSA-N selanylidenemercury Chemical compound [Hg]=[Se] YQMLDSWXEQOSPP-UHFFFAOYSA-N 0.000 claims description 5
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 claims description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 4
- 239000004411 aluminium Substances 0.000 claims description 4
- 229910001431 copper ion Inorganic materials 0.000 claims description 4
- 239000000428 dust Substances 0.000 claims description 4
- 229940008718 metallic mercury Drugs 0.000 claims description 4
- 229920001021 polysulfide Polymers 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- 229910052717 sulfur Inorganic materials 0.000 claims description 4
- 239000011593 sulfur Substances 0.000 claims description 4
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims description 3
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 230000006835 compression Effects 0.000 claims description 3
- 238000007906 compression Methods 0.000 claims description 3
- 229910000037 hydrogen sulfide Inorganic materials 0.000 claims description 3
- 229910052976 metal sulfide Inorganic materials 0.000 claims description 3
- 150000002739 metals Chemical class 0.000 claims description 3
- 239000005077 polysulfide Substances 0.000 claims description 3
- 150000008117 polysulfides Polymers 0.000 claims description 3
- 229940065287 selenium compound Drugs 0.000 claims description 3
- 150000003343 selenium compounds Chemical class 0.000 claims description 3
- 150000003346 selenoethers Chemical class 0.000 claims description 3
- 229910052709 silver Inorganic materials 0.000 claims description 3
- 239000004332 silver Substances 0.000 claims description 3
- 150000004763 sulfides Chemical class 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims 38
- 150000001342 alkaline earth metals Chemical class 0.000 claims 2
- 239000003599 detergent Substances 0.000 claims 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 description 158
- 238000001035 drying Methods 0.000 description 53
- 239000003153 chemical reaction reagent Substances 0.000 description 35
- 150000002500 ions Chemical class 0.000 description 22
- 238000001914 filtration Methods 0.000 description 16
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 16
- 229910001385 heavy metal Inorganic materials 0.000 description 14
- 239000012535 impurity Substances 0.000 description 13
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 13
- 229910052979 sodium sulfide Inorganic materials 0.000 description 12
- 238000000746 purification Methods 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 238000000926 separation method Methods 0.000 description 7
- 238000003860 storage Methods 0.000 description 7
- 230000001105 regulatory effect Effects 0.000 description 6
- DOBUSJIVSSJEDA-UHFFFAOYSA-L 1,3-dioxa-2$l^{6}-thia-4-mercuracyclobutane 2,2-dioxide Chemical compound [Hg+2].[O-]S([O-])(=O)=O DOBUSJIVSSJEDA-UHFFFAOYSA-L 0.000 description 5
- 239000000356 contaminant Substances 0.000 description 5
- 229910000370 mercury sulfate Inorganic materials 0.000 description 5
- 238000005201 scrubbing Methods 0.000 description 5
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 229910000497 Amalgam Inorganic materials 0.000 description 3
- 239000005909 Kieselgur Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 239000005083 Zinc sulfide Substances 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 description 3
- 229910052785 arsenic Inorganic materials 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 239000011133 lead Substances 0.000 description 2
- XCAUINMIESBTBL-UHFFFAOYSA-N lead(ii) sulfide Chemical compound [Pb]=S XCAUINMIESBTBL-UHFFFAOYSA-N 0.000 description 2
- VPCVQOUFBWWQSL-UHFFFAOYSA-L mercury(2+);selenate Chemical compound [Hg+2].[O-][Se]([O-])(=O)=O VPCVQOUFBWWQSL-UHFFFAOYSA-L 0.000 description 2
- 150000002736 metal compounds Chemical class 0.000 description 2
- 239000012255 powdered metal Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 101150013030 FAN1 gene Proteins 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- 229910020275 Na2Sx Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 229910052946 acanthite Inorganic materials 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000004035 construction material Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical class [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- 150000002730 mercury Chemical class 0.000 description 1
- 229940100892 mercury compound Drugs 0.000 description 1
- 150000002731 mercury compounds Chemical class 0.000 description 1
- CBBVHSHLSCZIHD-UHFFFAOYSA-N mercury silver Chemical compound [Ag].[Hg] CBBVHSHLSCZIHD-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical class [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 1
- 239000012716 precipitator Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- FSJWWSXPIWGYKC-UHFFFAOYSA-M silver;silver;sulfanide Chemical compound [SH-].[Ag].[Ag+] FSJWWSXPIWGYKC-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000012453 solvate Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical class [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 235000009529 zinc sulphate Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/48—Sulfur dioxide; Sulfurous acid
- C01B17/50—Preparation of sulfur dioxide
- C01B17/56—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Treating Waste Gases (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7062571A JPS4836092A (sv) | 1971-09-10 | 1971-09-10 | |
| JP2082072A JPS5229272B2 (sv) | 1972-02-28 | 1972-02-28 | |
| JP2138472A JPS5027478B2 (sv) | 1972-02-29 | 1972-02-29 | |
| JP4163372A JPS5139197B2 (sv) | 1972-04-24 | 1972-04-24 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO136489B true NO136489B (sv) | 1977-06-06 |
| NO136489C NO136489C (no) | 1977-09-14 |
Family
ID=27457464
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO3191/72A NO136489C (no) | 1971-09-10 | 1972-09-08 | Fremgangsm}te ved fremstilling av kvikks¦lvfri svovelsyre |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US3954451A (sv) |
| AU (1) | AU477154B2 (sv) |
| BE (1) | BE788615A (sv) |
| CA (1) | CA986685A (sv) |
| DE (1) | DE2243577C3 (sv) |
| FI (1) | FI60850C (sv) |
| FR (1) | FR2152807B1 (sv) |
| GB (1) | GB1410032A (sv) |
| IT (1) | IT968320B (sv) |
| NL (1) | NL7212277A (sv) |
| NO (1) | NO136489C (sv) |
| SE (1) | SE394659C (sv) |
| ZM (1) | ZM14572A1 (sv) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4057423A (en) * | 1971-09-10 | 1977-11-08 | Mitsui Mining & Smelting Co., Ltd. | Method for the manufacture of mercury free sulfuric acid |
| US4044098A (en) * | 1976-05-18 | 1977-08-23 | Phillips Petroleum Company | Removal of mercury from gas streams using hydrogen sulfide and amines |
| FI62002C (fi) * | 1981-04-15 | 1982-11-10 | Outokumpu Oy | Foerfarande och anordning foer separering av kvicksilver ur svveldioxidhaltiga heta och fuktiga gaser |
| LU83715A1 (fr) * | 1981-10-26 | 1983-06-07 | Metallurgie Hoboken | Procede pour fabriquer de l'acide sulfurique |
| SE439154B (sv) * | 1982-12-03 | 1985-06-03 | Boliden Ab | Forfarande vid produktion av svavelsyra ur svaveldioxidhaltig gas |
| SE439153B (sv) * | 1982-12-03 | 1985-06-03 | Boliden Ab | Forfarande vid produktion av svavelsyra ur svaveldioxidhaltig gas herrorande fran behandling av kvicksilverinnehallande ravaror och mellanprodukter |
| US5711929A (en) * | 1989-05-06 | 1998-01-27 | 698638 Alberta Ltd. | Purification of elemental sulphur |
| GB8912861D0 (en) * | 1989-06-05 | 1989-07-26 | Sherritt Gordon Ltd | Purification of elemental sulphur |
| DE4436019C2 (de) * | 1994-10-08 | 1999-04-22 | Metallgesellschaft Ag | Verfahren zur Herstellung von schwermetallfreier Schwefelsäure aus SO¶2¶-haltigen Gasen |
| ES2097699B1 (es) * | 1994-10-26 | 1997-12-16 | Asturiana De Zinc Sa | Procedimiento continuo para la captacion y precipitacion simultanea de mercurio en gases que lo contienen. |
| FI117617B (sv) * | 2000-12-08 | 2006-12-29 | Outokumpu Oy | Förfarande för att avlägsna kvicksilver ur gas |
| US20050207955A1 (en) * | 2004-03-17 | 2005-09-22 | Bo Wang | Mercury adsorbent composition, process of making same and method of separating mercury from fluids |
| CN112174098B (zh) * | 2020-09-29 | 2022-05-03 | 安徽华铂再生资源科技有限公司 | 一种低温制冷机组在低气浓制酸系统中的应用方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US940595A (en) * | 1906-02-10 | 1909-11-16 | Gen Chemical Corp | Purification of burner-gases. |
| US935337A (en) * | 1908-07-08 | 1909-09-28 | John Herbert Thwaites | Wet method of separating metallic compounds. |
| US1915270A (en) * | 1930-03-21 | 1933-06-27 | Catalytic Process Corp | Process of making contact sulphuric acid |
| GB742052A (en) * | 1951-04-05 | 1955-12-21 | Alfons Zieren | Improvements relating to the washing and cooling of gases containing sulphur dioxide |
| US2846305A (en) * | 1954-04-05 | 1958-08-05 | American Cyanamid Co | Separation and recovery of mercury |
| DE1054972B (de) * | 1957-05-08 | 1959-04-16 | Goldschmidt Ag Th | Verfahren zur Herstellung von weitgehend quecksilberfreier Schwefelsaeure |
| US2958572A (en) * | 1957-05-20 | 1960-11-01 | Monsanto Chemicals | Separation of selenium compounds from sulfur trioxide |
| US3145080A (en) * | 1960-11-15 | 1964-08-18 | Basf Ag | Purification of dilute commercial sulfuric acid |
| US3147074A (en) * | 1961-09-18 | 1964-09-01 | Chemical Construction Corp | Sulfuric acid process |
| DE1216263B (de) * | 1964-05-23 | 1966-05-12 | Vni Gorno Metall I Zwetnych Me | Verfahren zur Abtrennung des Quecksilbers aus konzentrierter Schwefelsaeure |
| SE334598B (sv) * | 1969-09-01 | 1971-05-03 | Boliden Ab | |
| DE1954828B2 (de) * | 1969-10-31 | 1974-07-18 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Verringerung der Quecksilber-Verluste bei der Chlor-Alkali-Elektrolyse nach dem Amalgam-Verfahren |
| US3701651A (en) * | 1970-02-06 | 1972-10-31 | Al Hack & Associates Inc | Process for production of mercury |
| US3689217A (en) * | 1970-06-15 | 1972-09-05 | Inventa Ag | Process for freeing 55-85% sulphuric acid from its impurities due to metals and/or semi-metals |
| FI45767C (sv) * | 1970-07-03 | 1972-09-11 | Outokumpu Oy | Förfarande för avskiljande och utvinning av kvicksilver och/eller sele n ur kvicksilver- och/eller selenhaltiga gaser. |
| US3826819A (en) * | 1972-04-21 | 1974-07-30 | Bunker Hill Co | Sulfuric acid purification process |
-
0
- BE BE788615D patent/BE788615A/xx unknown
-
1972
- 1972-09-04 AU AU46265/72A patent/AU477154B2/en not_active Expired
- 1972-09-05 DE DE2243577A patent/DE2243577C3/de not_active Expired
- 1972-09-05 FI FI2443/72A patent/FI60850C/fi active
- 1972-09-06 CA CA151,082A patent/CA986685A/en not_active Expired
- 1972-09-06 US US05/286,712 patent/US3954451A/en not_active Expired - Lifetime
- 1972-09-06 SE SE7211517A patent/SE394659C/sv unknown
- 1972-09-08 FR FR7231993A patent/FR2152807B1/fr not_active Expired
- 1972-09-08 IT IT69845/72A patent/IT968320B/it active
- 1972-09-08 NL NL7212277A patent/NL7212277A/xx unknown
- 1972-09-08 NO NO3191/72A patent/NO136489C/no unknown
- 1972-09-11 ZM ZM145/72*UA patent/ZM14572A1/xx unknown
- 1972-09-11 GB GB4202072A patent/GB1410032A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| SE394659B (sv) | 1977-07-04 |
| AU477154B2 (en) | 1976-10-14 |
| NO136489C (no) | 1977-09-14 |
| FI60850B (fi) | 1981-12-31 |
| ZM14572A1 (en) | 1973-06-21 |
| DE2243577C3 (de) | 1980-02-14 |
| IT968320B (it) | 1974-03-20 |
| BE788615A (fr) | 1973-01-02 |
| GB1410032A (en) | 1975-10-15 |
| SE394659C (sv) | 1979-06-05 |
| DE2243577B2 (de) | 1979-06-21 |
| AU4626572A (en) | 1974-03-14 |
| CA986685A (en) | 1976-04-06 |
| FR2152807B1 (sv) | 1975-01-03 |
| FR2152807A1 (sv) | 1973-04-27 |
| FI60850C (fi) | 1982-04-13 |
| NL7212277A (sv) | 1973-03-13 |
| DE2243577A1 (de) | 1973-03-15 |
| US3954451A (en) | 1976-05-04 |
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