NO120189B - - Google Patents
Download PDFInfo
- Publication number
- NO120189B NO120189B NO312968A NO312968A NO120189B NO 120189 B NO120189 B NO 120189B NO 312968 A NO312968 A NO 312968A NO 312968 A NO312968 A NO 312968A NO 120189 B NO120189 B NO 120189B
- Authority
- NO
- Norway
- Prior art keywords
- rare earth
- picolyl
- amide
- solution
- earth metal
- Prior art date
Links
- 238000000034 method Methods 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- -1 rare earth metal ions Chemical class 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 229910052761 rare earth metal Inorganic materials 0.000 claims 5
- 238000000605 extraction Methods 0.000 claims 3
- 150000002910 rare earth metals Chemical class 0.000 claims 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- 239000004215 Carbon black (E152) Substances 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- 229930195733 hydrocarbon Natural products 0.000 claims 1
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- 239000006193 liquid solution Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 229910052727 yttrium Inorganic materials 0.000 claims 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims 1
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 12
- INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 description 10
- 238000002844 melting Methods 0.000 description 10
- 230000008018 melting Effects 0.000 description 10
- 229910052799 carbon Inorganic materials 0.000 description 6
- 239000013078 crystal Substances 0.000 description 5
- GZUXJHMPEANEGY-UHFFFAOYSA-N bromomethane Chemical compound BrC GZUXJHMPEANEGY-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 150000003839 salts Chemical group 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 150000001408 amides Chemical class 0.000 description 3
- 229940073608 benzyl chloride Drugs 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- VBSTXRUAXCTZBQ-UHFFFAOYSA-N 1-hexyl-4-phenylpiperazine Chemical compound C1CN(CCCCCC)CCN1C1=CC=CC=C1 VBSTXRUAXCTZBQ-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- JACRWUWPXAESPB-QMMMGPOBSA-N Tropic acid Natural products OC[C@H](C(O)=O)C1=CC=CC=C1 JACRWUWPXAESPB-QMMMGPOBSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- BHELZAPQIKSEDF-UHFFFAOYSA-N allyl bromide Chemical compound BrCC=C BHELZAPQIKSEDF-UHFFFAOYSA-N 0.000 description 2
- KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical compound ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 description 2
- VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229940102396 methyl bromide Drugs 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 2
- MPPPKRYCTPRNTB-UHFFFAOYSA-N 1-bromobutane Chemical compound CCCCBr MPPPKRYCTPRNTB-UHFFFAOYSA-N 0.000 description 1
- WMXURTHCVUXSGD-UHFFFAOYSA-N 2-(hydroxymethyl)-3-oxo-2-phenylbutanoyl chloride Chemical compound CC(=O)C(CO)(C(Cl)=O)C1=CC=CC=C1 WMXURTHCVUXSGD-UHFFFAOYSA-N 0.000 description 1
- WOXFMYVTSLAQMO-UHFFFAOYSA-N 2-Pyridinemethanamine Chemical compound NCC1=CC=CC=N1 WOXFMYVTSLAQMO-UHFFFAOYSA-N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241000294754 Macroptilium atropurpureum Species 0.000 description 1
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 1
- 125000003342 alkenyl group Chemical group 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 125000000304 alkynyl group Chemical group 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- AGEZXYOZHKGVCM-UHFFFAOYSA-N benzyl bromide Chemical compound BrCC1=CC=CC=C1 AGEZXYOZHKGVCM-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- DENRZWYUOJLTMF-UHFFFAOYSA-N diethyl sulfate Chemical compound CCOS(=O)(=O)OCC DENRZWYUOJLTMF-UHFFFAOYSA-N 0.000 description 1
- 229940008406 diethyl sulfate Drugs 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- HVTICUPFWKNHNG-UHFFFAOYSA-N iodoethane Chemical compound CCI HVTICUPFWKNHNG-UHFFFAOYSA-N 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- ZBAMQLFFVBPAOX-UHFFFAOYSA-N n-(pyridin-4-ylmethyl)ethanamine Chemical compound CCNCC1=CC=NC=C1 ZBAMQLFFVBPAOX-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000002568 propynyl group Chemical group [*]C#CC([H])([H])[H] 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000003381 solubilizing effect Effects 0.000 description 1
- 230000002048 spasmolytic effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Landscapes
- Pyridine Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO312968A NO120189B (enrdf_load_stackoverflow) | 1966-02-04 | 1968-08-08 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB495266A GB1180921A (en) | 1966-02-04 | 1966-02-04 | Improvements in Separation Procedures. |
| NO166696A NO119633B (enrdf_load_stackoverflow) | 1966-02-04 | 1967-02-03 | |
| NO312968A NO120189B (enrdf_load_stackoverflow) | 1966-02-04 | 1968-08-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO120189B true NO120189B (enrdf_load_stackoverflow) | 1970-09-14 |
Family
ID=27254534
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO312968A NO120189B (enrdf_load_stackoverflow) | 1966-02-04 | 1968-08-08 |
Country Status (1)
| Country | Link |
|---|---|
| NO (1) | NO120189B (enrdf_load_stackoverflow) |
-
1968
- 1968-08-08 NO NO312968A patent/NO120189B/no unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| SU422151A3 (ru) | Способ получения n-трифенилметилимидазолов | |
| US5382685A (en) | Preparation of O-substituted hydroxylammonium salts | |
| CH432519A (de) | Verfahren zur Herstellung neuer Alkoxypiperidin-Derivate und ihrer Salze | |
| CA3043613A1 (en) | Method for making n-(fluorosulfonyl) dimethylamine | |
| NO120189B (enrdf_load_stackoverflow) | ||
| US3963768A (en) | Process for the preparation of thiocarbamic acid O-esters | |
| US3294842A (en) | Alpha-hydroxy oximes containing alkenyl radicals | |
| JPS6251651A (ja) | ３−アミノアクリル酸エステルの製造法 | |
| CN107337628B (zh) | 一种制备左乙拉西坦的方法 | |
| JPS6015622B2 (ja) | アミノラクタム化合物の同時分割及びラセミ化 | |
| WO2000002848A1 (en) | Novel salts of n-tert-butylhydroxylamine | |
| US3415836A (en) | Salicylic acid esters of beta-pyridyl carbinol | |
| Lyman et al. | The Identification of Acids. Ii. | |
| DE194748C (enrdf_load_stackoverflow) | ||
| CA2000184C (en) | Trihydrates of sodium l- and d-2-pyrrolidone-5-carboxylate | |
| JPH0256354B2 (enrdf_load_stackoverflow) | ||
| US12398091B2 (en) | Process for the purification of a mixture comprising N-alkyl-hydroxylammonium salts | |
| US4409386A (en) | Separation of 3,4-dichloroaniline | |
| US2798075A (en) | Heterocyclic quaternary salts | |
| DE1909741A1 (de) | Alkylester von alpha-(1-substituierter 3-Pyrrolidinyl)-alpha-phenylessigsaeure und Verfahren zu seiner Herstellung | |
| US2437833A (en) | Nu-benzyl-nu-myristyl morpholinium halides | |
| US3383389A (en) | Process for synthesis of vinyltetrazole monomers | |
| US3997611A (en) | Production of tertiary phosphine oxides | |
| CH411901A (de) | Verfahren zur Herstellung von heterocyclischen Verbindungen | |
| US2937200A (en) | Resolution of dl-glutamic acid |