MX9703727A - Preparacion de caprolactama. - Google Patents

Preparacion de caprolactama.

Info

Publication number
MX9703727A
MX9703727A MX9703727A MX9703727A MX9703727A MX 9703727 A MX9703727 A MX 9703727A MX 9703727 A MX9703727 A MX 9703727A MX 9703727 A MX9703727 A MX 9703727A MX 9703727 A MX9703727 A MX 9703727A
Authority
MX
Mexico
Prior art keywords
caprolactam
boiling compounds
give
mixture
stage
Prior art date
Application number
MX9703727A
Other languages
English (en)
Other versions
MXPA97003727A (es
Inventor
Gunther Achhammer
Eberhard Fuchs
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of MXPA97003727A publication Critical patent/MXPA97003727A/es
Publication of MX9703727A publication Critical patent/MX9703727A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Audible-Bandwidth Dynamoelectric Transducers Other Than Pickups (AREA)
  • Polyamides (AREA)
  • Mounting Of Bearings Or Others (AREA)

Abstract

La presente invencion se refiere a la caprolactama que se prepara haciendo reaccionar una solucion de 6-aminocapronitrilo con agua en la fase líquida a temperaturas elavadas mediante un proceso en el cual, (a) una solucion de 6-aminocapronitrilo en fase líquida se calienta sin la adicion de un catalizador en un reactor A para dar una mezcla I que cosiste esencialmente en agua, caprolactama y una fraccion de elevado punto de ebullicion (ebullidor elevado), luego (b) el agua se retira de la mezcla resultante I para dar una mezcla II que consiste esencialmente en caprolactama y los ebullidores elevados, después (c) la caprolactama y los ebullidores elevados de la mezcla II se separan por destilacion, y luego (D1) los ebullidores elevados de la etapa (c) se alimentan al reactor A de la etapa (a), o (d2) los ebullidores elevados se calientan de la misma manera que en la etapa (a) en otro reactor B y luego se procesan de la misma manera que etapas (b) y (c) para producir más caprolactama, o (d3) los ebullidores elevados se calientan a presion reducida en presencia de una base en un reactor C y la mezcla que reacciono se trabaja por destilacion para dar caprolactama.
MX9703727A 1994-11-25 1995-11-14 Preparacion de caprolactama. MX9703727A (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE4441962A DE4441962A1 (de) 1994-11-25 1994-11-25 Verfahren zur Herstellung von Caprolactam
DEP4441962.7 1994-11-25
PCT/EP1995/004464 WO1996016936A1 (de) 1994-11-25 1995-11-14 Verfahren zur herstellung von caprolactam

Publications (2)

Publication Number Publication Date
MXPA97003727A MXPA97003727A (es) 1998-02-01
MX9703727A true MX9703727A (es) 1998-02-28

Family

ID=6534115

Family Applications (1)

Application Number Title Priority Date Filing Date
MX9703727A MX9703727A (es) 1994-11-25 1995-11-14 Preparacion de caprolactama.

Country Status (15)

Country Link
US (1) US5495016A (es)
EP (1) EP0793650B1 (es)
JP (1) JPH10509963A (es)
KR (1) KR100403093B1 (es)
CN (1) CN1070182C (es)
AT (1) ATE220061T1 (es)
AU (1) AU3928795A (es)
CZ (1) CZ291034B6 (es)
DE (2) DE4441962A1 (es)
ES (1) ES2179888T3 (es)
MX (1) MX9703727A (es)
MY (1) MY112192A (es)
PL (1) PL320367A1 (es)
RU (1) RU2153492C2 (es)
WO (1) WO1996016936A1 (es)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4443125A1 (de) * 1994-12-03 1996-06-05 Basf Ag Verfahren zur Herstellung von Caprolactam
DE19500041A1 (de) * 1995-01-03 1996-07-04 Basf Ag Verfahren zur kontinuierlichen Reinigung von aus 6-Aminocapronitril hergestelltem Roh-Caprolactam
DE19517823A1 (de) * 1995-05-18 1996-11-21 Basf Ag Verfahren zur Herstellung von Caprolactam
TW420662B (en) † 1996-02-17 2001-02-01 Du Pont Recovery of <epsilon>-caprolactam
DE19628805A1 (de) * 1996-07-17 1998-01-22 Basf Ag Verfahren zur Herstellung von Caprolactam aus 6-Aminocapronitril
JP2001502688A (ja) 1996-10-21 2001-02-27 ディーエスエム エヌ．ブイ． ６―アミノカプロアミド及び６―アミノカプロアミドオリゴマーからε―カプロラクタムを分離するための方法
EP0860431A1 (en) 1997-02-19 1998-08-26 Dsm N.V. Process to prepare e-caprolactam
DE19718706A1 (de) * 1997-05-02 1998-11-05 Basf Ag Verfahren zur Herstellung cyclischer Lactame
DE19738463C2 (de) 1997-09-03 1999-09-23 Basf Ag Verfahren zur Herstellung von Caprolactam
DE19811880A1 (de) * 1998-03-18 1999-09-23 Basf Ag Verfahren zur Herstellung von Lactamen
FR2781796B1 (fr) * 1998-07-28 2000-09-22 Rhone Poulenc Fibres Procede de deshydratation de lactame
JP3667140B2 (ja) * 1999-03-04 2005-07-06 パイオニア株式会社 ディスクチェンジャ装置
US6627046B1 (en) 2000-01-21 2003-09-30 E. I. Du Pont De Nemours And Company Separation of the products of polyamide ammonolysis
US6686465B2 (en) 2000-05-03 2004-02-03 Basf Aktiengesellschaft Preparation of cyclic lactams
DE10021193A1 (de) * 2000-05-03 2001-11-08 Basf Ag Verfahren zur Herstellung cyclischer Lactame
JP4182273B2 (ja) 2000-06-27 2008-11-19 住友化学株式会社 ε−カプロラクタムの製造方法
EP1405846A1 (en) * 2002-10-01 2004-04-07 DSM IP Assets B.V. Process for the preparation of epsilon-caprolactam from a mixture comprising 6-aminocaproamide and/or oligomers
DE10253095A1 (de) * 2002-11-13 2004-06-17 Basf Ag Verfahren zur Reinigung von Caprolactam
DE10253094A1 (de) * 2002-11-13 2004-05-27 Basf Ag Verfahren zur Reinigung von Caprolactam
US6858728B2 (en) * 2003-06-17 2005-02-22 Invista North America S.A.R.L. Method for making caprolactam from impure ACN in which THA is not removed until after caprolactam is produced
DE102008060340A1 (de) 2008-12-03 2010-06-10 Wolfgang F. Prof. Dr. Hölderich Herstellung von Lactamen und Carbonsäureamide durch Beckmann-Umlagerung von Oximen in Gegenwart von Nb-Katalysatoren
DE102015005238A1 (de) 2015-04-24 2016-10-27 Wolfgang Hölderich Herstellung von Lactamen durch Beckmann-Umlagerung von Oximen
CN116947693B (zh) * 2022-04-13 2025-05-16 中石化南京化工研究院有限公司 6-氨基己腈的合成方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2245129A (en) * 1935-01-02 1941-06-10 Du Pont Process for preparing linear polyamides
US2301964A (en) * 1941-09-12 1942-11-17 Du Pont Method of preparing lactams
US2357484A (en) * 1941-09-12 1944-09-05 Du Pont Process for producing compounds containing an n-substituted amide group
FR1419684A (fr) * 1964-09-03 1965-12-03 Electrochimie Soc Procédé perfectionné de fabrication d'epsilon-caprolactames
JPS4821958B1 (es) * 1969-01-28 1973-07-02
EP0150295A3 (en) * 1983-12-19 1988-03-30 Allied Corporation Selective production of n-substituted amides by use of cu(o)/metallic oxides catalyst compositions
US4625023A (en) * 1985-09-03 1986-11-25 Allied Corporation Selective conversion of aliphatic and aromatic aminonitriles and/or dinitriles into lactams
DE4319134A1 (de) * 1993-06-09 1994-12-15 Basf Ag Verfahren zur Herstellung von Caprolactam

Also Published As

Publication number Publication date
EP0793650B1 (de) 2002-07-03
CN1070182C (zh) 2001-08-29
KR100403093B1 (ko) 2004-03-18
CN1166830A (zh) 1997-12-03
EP0793650A1 (de) 1997-09-10
AU3928795A (en) 1996-06-19
CZ146997A3 (en) 1997-10-15
JPH10509963A (ja) 1998-09-29
ATE220061T1 (de) 2002-07-15
DE4441962A1 (de) 1996-05-30
WO1996016936A1 (de) 1996-06-06
MY112192A (en) 2001-04-30
RU2153492C2 (ru) 2000-07-27
CZ291034B6 (cs) 2002-12-11
DE59510263D1 (de) 2002-08-08
ES2179888T3 (es) 2003-02-01
US5495016A (en) 1996-02-27
PL320367A1 (en) 1997-09-29

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