MX358513B - E-1-cloro-3,3,3-trifluoropropeno de alta pureza y métodos para elaborar el mismo. - Google Patents

E-1-cloro-3,3,3-trifluoropropeno de alta pureza y métodos para elaborar el mismo.

Info

Publication number
MX358513B
MX358513B MX2013007757A MX2013007757A MX358513B MX 358513 B MX358513 B MX 358513B MX 2013007757 A MX2013007757 A MX 2013007757A MX 2013007757 A MX2013007757 A MX 2013007757A MX 358513 B MX358513 B MX 358513B
Authority
MX
Mexico
Prior art keywords
methods
trifluoropropene
chloro
high purity
making
Prior art date
Application number
MX2013007757A
Other languages
English (en)
Other versions
MX2013007757A (es
Inventor
Sung Tung Hsueh
Ratna Singh Rajiv
Shankland Ian
A Pokrovski Konstantin
Original Assignee
Honeywell Int Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=46381341&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=MX358513(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Honeywell Int Inc filed Critical Honeywell Int Inc
Publication of MX2013007757A publication Critical patent/MX2013007757A/es
Publication of MX358513B publication Critical patent/MX358513B/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/361Preparation of halogenated hydrocarbons by reactions involving a decrease in the number of carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/206Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/25Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/38Separation; Purification; Stabilisation; Use of additives
    • C07C17/383Separation; Purification; Stabilisation; Use of additives by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00Indexing scheme relating to specific properties of organic compounds
    • C07B2200/09Geometrical isomers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La presente invención describe E-1-cloro-3,3,3-trifluoropropeno de alta pureza (1233zd(E)) y métodos para producir el mismo. Más específicamente, la presente invención describe los métodos para elaborar 1233zd(E) esencialmente libres de impurezas tóxicas (por ejemplo, 2-cloro-3,3,3-trifluoropropeno (1233xf), clorotetrafluoro-propeno (1224) y 3,3,3-trifluoropropino). La presente invención además proporciona métodos para elaborar 1233zd(E) de alta pureza con una concentración de 1233xf y 1224 en o debajo de 200 partes por millón (ppm) e impurezas de 3,3,3-trifluoropropino en o debajo de 20 ppm. La formación de impurezas de 1233xf puede evitarse si el 1,1,1,3,3-pentacloropropa no puro se utiliza como un material de partida. También se establece que la formación de 1233xf se evita si se utiliza un proceso de fabricación de fases líquidas.
MX2013007757A 2011-01-04 2012-01-03 E-1-cloro-3,3,3-trifluoropropeno de alta pureza y métodos para elaborar el mismo. MX358513B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US12/984,024 US9156752B2 (en) 2011-01-04 2011-01-04 High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same
PCT/US2012/020035 WO2012094288A2 (en) 2011-01-04 2012-01-03 High purity e-1-chloro-3,3,3-trifluoropropene and methods of making the same

Publications (2)

Publication Number Publication Date
MX2013007757A MX2013007757A (es) 2013-08-15
MX358513B true MX358513B (es) 2018-08-24

Family

ID=46381341

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2013007757A MX358513B (es) 2011-01-04 2012-01-03 E-1-cloro-3,3,3-trifluoropropeno de alta pureza y métodos para elaborar el mismo.

Country Status (8)

Country Link
US (2) US9156752B2 (es)
EP (1) EP2661419B1 (es)
JP (3) JP6225028B2 (es)
KR (1) KR101990066B1 (es)
CN (1) CN103402953B (es)
ES (1) ES2549641T3 (es)
MX (1) MX358513B (es)
WO (1) WO2012094288A2 (es)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9156752B2 (en) * 2011-01-04 2015-10-13 Honeywell International Inc. High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same
US9000240B2 (en) 2011-05-19 2015-04-07 Honeywell International Inc. Integrated process for the production of 1-chloro-3,3,3-trifluoropropene
JP6059711B2 (ja) * 2011-05-19 2017-01-11 アーケマ・インコーポレイテッド クロロ−トリフルオロプロペンの不燃性組成物
US8921621B2 (en) * 2012-02-15 2014-12-30 Honeywell International Inc. Process for the production of HCFC-1233zd
US9272968B2 (en) * 2013-03-14 2016-03-01 Honeywell International Inc. Process to suppress the formation of 3,3,3-trifluoropropyne in fluorocarbon manufacture
JP6213361B2 (ja) 2013-05-09 2017-10-18 セントラル硝子株式会社 2−クロロ−1,3,3,3−テトラフルオロプロペンの製造方法
US9255045B2 (en) 2014-01-13 2016-02-09 Arkema France E-1-chloro-3,3,3-trifluoropropene production process from 1,1,3,3-tetrachloropropene
KR102398138B1 (ko) * 2014-04-29 2022-05-18 알케마 인코포레이티드 불화수소로부터 r-1233의 분리
JP6575526B2 (ja) * 2014-10-02 2019-09-18 セントラル硝子株式会社 2−クロロ−1,3,3,3−テトラフルオロプロペン及び1−クロロ−3,3,3−トリフルオロプロペンを含有する共沸様組成物
FR3027304B1 (fr) * 2014-10-16 2018-02-23 Arkema France Compositions a base de 1,1,1,3,3-pentachloropropane
US9764998B2 (en) * 2015-05-12 2017-09-19 Honeywell International Inc. Process for making HCFO-1233zd
FR3036398B1 (fr) * 2015-05-22 2019-05-03 Arkema France Compositions a base de 1,1,3,3-tetrachloropropene
JP6826280B2 (ja) 2016-01-15 2021-02-03 セントラル硝子株式会社 トランス−1−クロロ−3,3,3−トリフルオロプロペンの製造方法
US10029964B2 (en) * 2016-08-30 2018-07-24 Honeywell International Inc. Azeotropic or azeotrope-like compositions of 3,3,3-trifluoropropyne and water
GB201701099D0 (en) * 2017-01-23 2017-03-08 Mexichem Fluor Sa De Cv Process
US10118879B1 (en) 2017-10-26 2018-11-06 Honeywell International Inc. Process for catalytic conversion of mixtures of HCFO-1233zd(Z) and HCFC-244fa into HCFO-1233zd(E)
FR3081158B1 (fr) * 2018-05-16 2020-07-31 Arkema France Procede de production du 1-chloro-3,3,3-trifluoropropene.
FR3083232B1 (fr) 2018-06-27 2021-11-12 Arkema France Procede de production du 1-chloro-3,3,3-trifluoropropene
FR3086287B1 (fr) 2018-09-26 2020-09-18 Arkema France Stabilisation du 1-chloro-3,3,3-trifluoropropene
KR20210092267A (ko) * 2018-11-15 2021-07-23 알케마 인코포레이티드 하이드로클로로플루오로올레핀을 함유하는 조 스트림으로부터 hf를 중화 및 제거하는 방법
CN112624897A (zh) * 2019-09-24 2021-04-09 江西天宇化工有限公司 同时生产反式-1-氯-3,3,3-三氟丙烯和反式-1,3,3,3-四氟丙烯的方法

Family Cites Families (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2787646A (en) 1953-09-03 1957-04-02 Haszeldine Robert Neville Organic halogen compounds and methods of making same
EP0876314B1 (en) * 1995-08-01 2003-02-26 E.I. Du Pont De Nemours And Company Process for the manufacture of halocarbons and selected compounds and azeotropes with hf
US5902914A (en) * 1995-08-14 1999-05-11 Alliedsignal Inc. Process for the preparation of halogenated alkanes
JP3818398B2 (ja) 1995-12-29 2006-09-06 ダイキン工業株式会社 1,1,1,3,3−ペンタフルオロプロパンの製造方法
JPH09194404A (ja) * 1996-01-17 1997-07-29 Central Glass Co Ltd 1−クロロ−3,3,3−トリフルオロプロペンの製造法
JP3516324B2 (ja) * 1996-08-23 2004-04-05 セントラル硝子株式会社 1−クロロ−3,3,3−トリフルオロプロペンの製造法
US6235951B1 (en) * 1996-01-17 2001-05-22 Central Glass Company, Limited Method for producing 1,1,1,3,3-pentafluoropropane
DE69713503T2 (de) * 1996-04-04 2002-12-05 Honeywell International Inc., Morristown Reinigung von 1,1,1,3,3-pentafluorpropan (r-245fa)
US6111150A (en) 1996-06-20 2000-08-29 Central Glass Company, Limited Method for producing 1,1,1,3,3,-pentafluoropropane
US5705779A (en) * 1996-08-08 1998-01-06 Alliedsignal Inc. Preparation of 1,1,1,3,3-pentachloropropane by photochlorination of 1,1,1,3-tetrachloropropane
US5710352A (en) 1996-09-19 1998-01-20 Alliedsignal Inc. Vapor phase process for making 1,1,1,3,3-pentafluoropropane and 1-chloro-3,3,3-trifluoropropene
US5811603A (en) * 1997-12-01 1998-09-22 Elf Atochem North America, Inc. Gas phase fluorination of 1230za
US5856595A (en) 1998-03-03 1999-01-05 Alliedsignal Inc. Purified 1,1,1,3,3,3-hexafluoropropane and method for making same
JP3518321B2 (ja) 1998-03-23 2004-04-12 ダイキン工業株式会社 1,1,1,3,3−ペンタフルオロプロパンの製造方法
JP3804289B2 (ja) * 1998-09-22 2006-08-02 ダイキン工業株式会社 1,1,1,3,3−ペンタフルオロプロパン及び/又は1−クロロ−3,3,3−トリフルオロプロペンの製造方法
US6313360B1 (en) 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
US6552238B1 (en) 2001-08-31 2003-04-22 Vulcan Chemicals Separation of heavy ends from streams of halogenated alkanes
US6720466B2 (en) 2002-04-17 2004-04-13 Vulcan Chemicals, a division of Vulcan Materials Company 1,1,1,3,3-pentachloropropane process purge stream concentration using a secondary refluxed evaporator and secondary product recovery
US6844475B1 (en) * 2003-08-08 2005-01-18 Honeywell International Business Machines Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd)
US7112709B2 (en) 2003-09-09 2006-09-26 Vulcan Chemicals Method for reusing heavy end by-products in the manufacture of polychlorinated alkanes
US8058486B2 (en) * 2004-04-29 2011-11-15 Honeywell International Inc. Integrated process to produce 2,3,3,3-tetrafluoropropene
US8084653B2 (en) * 2004-04-29 2011-12-27 Honeywell International, Inc. Method for producing fluorinated organic compounds
US7265082B2 (en) 2004-08-04 2007-09-04 Honeywell International Inc. Azeotrope-like compositions of 1,1,1,3,3-pentachloropropane and carbon tetrachloride
CN1911512B (zh) 2005-07-07 2011-12-07 独立行政法人产业技术综合研究所 氟化催化剂及其制备方法、以及使用了该催化剂的氟化合物的制备方法
EP2546223B1 (en) 2006-01-03 2016-08-10 Honeywell International Inc. Method for producing fluorinated organic compounds
EP1837323A1 (en) 2006-03-24 2007-09-26 SOLVAY (Société Anonyme) Process for the manufacture of 1,1,1,3,3-pentafluoropropane
US9738577B2 (en) * 2006-10-11 2017-08-22 Honeywell International Inc. Process for the manufacture of 1,1,1,3,3-pentachloropropane
EP2091897B2 (en) 2006-10-31 2021-12-01 The Chemours Company FC, LLC Processes for the production of fluoropropanes and halopropenes
US8034251B2 (en) 2007-01-03 2011-10-11 Honeywell International Inc. Azeotropic compositions of 2-chloro-3,3,3-trifluoropropene (HCFC-1233xf), 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb), and hydrogen fluoride (HF)
US7795480B2 (en) 2007-07-25 2010-09-14 Honeywell International Inc. Method for producing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf)
AU2009244265B2 (en) * 2008-05-07 2014-06-26 The Chemours Company Fc, Llc. Compositions comprising 2,3-dichloro-1,1,1-trifluoropropane, 2-chloro-1,1,1-trifluoropropene, 2-chloro-1,1,1,2-tetrafluoropropane or 2,3,3,3-tetrafluoropropene
US8163196B2 (en) 2008-10-28 2012-04-24 Honeywell International Inc. Azeotrope-like compositions comprising 1-chloro-3,3,3-trifluoropropene
US8642818B2 (en) * 2008-11-19 2014-02-04 Arkema Inc. Process for the manufacture of hydrofluoroolefins
CN105646135A (zh) 2008-11-19 2016-06-08 阿科玛股份有限公司 用于制造氢氯氟烯烃的方法
US8217208B2 (en) * 2008-12-12 2012-07-10 Honeywell International, Inc. Isomerization of 1-chloro-3,3,3-trifluoropropene
US8075797B2 (en) * 2009-01-29 2011-12-13 Honeywell International Inc. Azeotrope-like compositions of pentafluoropropane, chlorotrifluoropropene, and hydrogen fluoride
JP5360230B2 (ja) 2009-04-23 2013-12-04 ダイキン工業株式会社 2−クロロ−3,3,3−トリフルオロプロペンの製造方法
US9045386B2 (en) 2010-02-18 2015-06-02 Honeywell International Inc. Integrated process and methods of producing (E)-1-chloro-3,3,3-trifluoropropene
US8704017B2 (en) * 2010-09-03 2014-04-22 Honeywell International Inc. Continuous low-temperature process to produce trans-1-chloro-3,3,3-trifluoropropene
US9156752B2 (en) * 2011-01-04 2015-10-13 Honeywell International Inc. High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same
KR20130136500A (ko) * 2011-01-04 2013-12-12 허니웰 인터내셔널 인코포레이티드 고순도의 e-1-클로로-3,3,3-트리플루오로프로펜 및 이의 제조방법
US9000240B2 (en) * 2011-05-19 2015-04-07 Honeywell International Inc. Integrated process for the production of 1-chloro-3,3,3-trifluoropropene
US9018428B2 (en) * 2012-09-06 2015-04-28 Honeywell International Inc. Reactor and agitator useful in a process for making 1-chloro-3,3,3-trifluoropropene
US8907146B2 (en) * 2013-02-04 2014-12-09 Honeywell International Inc. Process for the preparation of 1-chloro-3,3,3-trifluoropropene using a phase transfer catalyst
US9272967B2 (en) * 2013-10-15 2016-03-01 Honeywell International Inc. Process for producing 1-chloro-3,3,3-trifluoropropene in an ionic liquid

Also Published As

Publication number Publication date
CN103402953B (zh) 2015-08-12
US20120172636A1 (en) 2012-07-05
CN103402953A (zh) 2013-11-20
EP2661419B1 (en) 2015-07-29
MX2013007757A (es) 2013-08-15
EP2661419A2 (en) 2013-11-13
US9156752B2 (en) 2015-10-13
WO2012094288A2 (en) 2012-07-12
JP6527575B2 (ja) 2019-06-05
JP2016164172A (ja) 2016-09-08
ES2549641T3 (es) 2015-10-30
KR101990066B1 (ko) 2019-06-17
US20160002128A1 (en) 2016-01-07
JP2018070656A (ja) 2018-05-10
US9862662B2 (en) 2018-01-09
KR20180120276A (ko) 2018-11-05
EP2661419A4 (en) 2014-07-02
JP6225028B2 (ja) 2017-11-01
JP2014509310A (ja) 2014-04-17
WO2012094288A3 (en) 2012-08-30

Similar Documents

Publication Publication Date Title
MX2013007757A (es) E-1-cloro-3,3,3-trifluoropropeno de alta pureza y metodos para elaborar el mismo.
MX2019001056A (es) Purificacion de materia prima mediante tratamiento termico.
PL2665694T3 (pl) Sposób wytwarzania 2,3,3,3-tetrafluoropropenu przez fluorowanie pentachloropropanu w fazie gazowej
MX2012011219A (es) Separacion de compuestos de punto de ebullicion cercano mediante la adicion de un tercer compuesto.
JP2009215294A5 (es)
WO2014151448A3 (en) An improved integrated process to produce 2,3,3,3-tetrafluoropropene
WO2012009114A3 (en) Method for prolonging a catalyst's life during hydrofluorination
WO2012030613A3 (en) 1,3,3,3-tetraflurorpropene process azeotropes with hf
MX2013005514A (es) Proceso para producir 2,3,3,3-tetrafluoropropeno.
MX2023009585A (es) Isomerizacion catalitica de z-1,1,1,4,4,4-hexafluoro-2- buteno a e-1,1,1,4,4,4-hexafluoro-2-buteno.
IN2014DN10381A (es)
PL2563750T3 (pl) SPOSÓB WYTWARZANIA 2-CHLORO-3,3,3-TRIFLUOROPROPENU (HCFO 1233xf) PRZEZ FLUOROWANIE PENTACHLOROPROPANU W FAZIE CIEKŁEJ
MX344948B (es) Proceso para producir 2,3,3,3-tetrafluoropropeno.
MX2015010461A (es) Proceso de fluoracion y reactor.
MX2014004250A (es) Proceso para producir 2,3,3,-tetrafluoropropeno.
WO2013106046A3 (en) Purification of trans-1,3,3,3-tetrafluoropropene
IN2014DN02915A (es)
MX2013009366A (es) Proceso para cis-1-cloro-3,3,3-trifluoropropeno.
MX2018005908A (es) Proceso para preparar 2,3,3,3-tetrafluoropropeno y/o fluoruro de vinilideno.
PL2630107T3 (pl) Sposób wytwarzania 2-chloro-3,3,3-trifluropropenu przez fluorowanie w fazie gazowej pentachloropropanu
AR088658A1 (es) Proceso para producir 2,3,3,3-tetrafluoropropeno
MX2015011156A (es) Procedimiento de fluoracion escalonado y sistema de reactores.
MY185235A (en) New crystalline form vii of agomelatine, preparation method and use thereof and pharmaceutical composition containing same
MX2016012851A (es) Un metodo para producir 1,1,2,3-tetracloropropeno con alto rendimiento.
MX2016010693A (es) Proceso para la fabricacion de hidroclorofluoroolefinas.

Legal Events

Date Code Title Description
FG Grant or registration