MX358513B - E-1-cloro-3,3,3-trifluoropropeno de alta pureza y métodos para elaborar el mismo. - Google Patents
E-1-cloro-3,3,3-trifluoropropeno de alta pureza y métodos para elaborar el mismo.Info
- Publication number
- MX358513B MX358513B MX2013007757A MX2013007757A MX358513B MX 358513 B MX358513 B MX 358513B MX 2013007757 A MX2013007757 A MX 2013007757A MX 2013007757 A MX2013007757 A MX 2013007757A MX 358513 B MX358513 B MX 358513B
- Authority
- MX
- Mexico
- Prior art keywords
- methods
- trifluoropropene
- chloro
- high purity
- making
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/361—Preparation of halogenated hydrocarbons by reactions involving a decrease in the number of carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/09—Geometrical isomers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La presente invención describe E-1-cloro-3,3,3-trifluoropropeno de alta pureza (1233zd(E)) y métodos para producir el mismo. Más específicamente, la presente invención describe los métodos para elaborar 1233zd(E) esencialmente libres de impurezas tóxicas (por ejemplo, 2-cloro-3,3,3-trifluoropropeno (1233xf), clorotetrafluoro-propeno (1224) y 3,3,3-trifluoropropino). La presente invención además proporciona métodos para elaborar 1233zd(E) de alta pureza con una concentración de 1233xf y 1224 en o debajo de 200 partes por millón (ppm) e impurezas de 3,3,3-trifluoropropino en o debajo de 20 ppm. La formación de impurezas de 1233xf puede evitarse si el 1,1,1,3,3-pentacloropropa no puro se utiliza como un material de partida. También se establece que la formación de 1233xf se evita si se utiliza un proceso de fabricación de fases líquidas.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12/984,024 US9156752B2 (en) | 2011-01-04 | 2011-01-04 | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
PCT/US2012/020035 WO2012094288A2 (en) | 2011-01-04 | 2012-01-03 | High purity e-1-chloro-3,3,3-trifluoropropene and methods of making the same |
Publications (2)
Publication Number | Publication Date |
---|---|
MX2013007757A MX2013007757A (es) | 2013-08-15 |
MX358513B true MX358513B (es) | 2018-08-24 |
Family
ID=46381341
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2013007757A MX358513B (es) | 2011-01-04 | 2012-01-03 | E-1-cloro-3,3,3-trifluoropropeno de alta pureza y métodos para elaborar el mismo. |
Country Status (8)
Country | Link |
---|---|
US (2) | US9156752B2 (es) |
EP (1) | EP2661419B1 (es) |
JP (3) | JP6225028B2 (es) |
KR (1) | KR101990066B1 (es) |
CN (1) | CN103402953B (es) |
ES (1) | ES2549641T3 (es) |
MX (1) | MX358513B (es) |
WO (1) | WO2012094288A2 (es) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
US9000240B2 (en) | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
JP6059711B2 (ja) * | 2011-05-19 | 2017-01-11 | アーケマ・インコーポレイテッド | クロロ−トリフルオロプロペンの不燃性組成物 |
US8921621B2 (en) * | 2012-02-15 | 2014-12-30 | Honeywell International Inc. | Process for the production of HCFC-1233zd |
US9272968B2 (en) * | 2013-03-14 | 2016-03-01 | Honeywell International Inc. | Process to suppress the formation of 3,3,3-trifluoropropyne in fluorocarbon manufacture |
JP6213361B2 (ja) | 2013-05-09 | 2017-10-18 | セントラル硝子株式会社 | 2−クロロ−1,3,3,3−テトラフルオロプロペンの製造方法 |
US9255045B2 (en) | 2014-01-13 | 2016-02-09 | Arkema France | E-1-chloro-3,3,3-trifluoropropene production process from 1,1,3,3-tetrachloropropene |
KR102398138B1 (ko) * | 2014-04-29 | 2022-05-18 | 알케마 인코포레이티드 | 불화수소로부터 r-1233의 분리 |
JP6575526B2 (ja) * | 2014-10-02 | 2019-09-18 | セントラル硝子株式会社 | 2−クロロ−1,3,3,3−テトラフルオロプロペン及び1−クロロ−3,3,3−トリフルオロプロペンを含有する共沸様組成物 |
FR3027304B1 (fr) * | 2014-10-16 | 2018-02-23 | Arkema France | Compositions a base de 1,1,1,3,3-pentachloropropane |
US9764998B2 (en) * | 2015-05-12 | 2017-09-19 | Honeywell International Inc. | Process for making HCFO-1233zd |
FR3036398B1 (fr) * | 2015-05-22 | 2019-05-03 | Arkema France | Compositions a base de 1,1,3,3-tetrachloropropene |
JP6826280B2 (ja) | 2016-01-15 | 2021-02-03 | セントラル硝子株式会社 | トランス−1−クロロ−3,3,3−トリフルオロプロペンの製造方法 |
US10029964B2 (en) * | 2016-08-30 | 2018-07-24 | Honeywell International Inc. | Azeotropic or azeotrope-like compositions of 3,3,3-trifluoropropyne and water |
GB201701099D0 (en) * | 2017-01-23 | 2017-03-08 | Mexichem Fluor Sa De Cv | Process |
US10118879B1 (en) | 2017-10-26 | 2018-11-06 | Honeywell International Inc. | Process for catalytic conversion of mixtures of HCFO-1233zd(Z) and HCFC-244fa into HCFO-1233zd(E) |
FR3081158B1 (fr) * | 2018-05-16 | 2020-07-31 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene. |
FR3083232B1 (fr) | 2018-06-27 | 2021-11-12 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene |
FR3086287B1 (fr) | 2018-09-26 | 2020-09-18 | Arkema France | Stabilisation du 1-chloro-3,3,3-trifluoropropene |
KR20210092267A (ko) * | 2018-11-15 | 2021-07-23 | 알케마 인코포레이티드 | 하이드로클로로플루오로올레핀을 함유하는 조 스트림으로부터 hf를 중화 및 제거하는 방법 |
CN112624897A (zh) * | 2019-09-24 | 2021-04-09 | 江西天宇化工有限公司 | 同时生产反式-1-氯-3,3,3-三氟丙烯和反式-1,3,3,3-四氟丙烯的方法 |
Family Cites Families (45)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2787646A (en) | 1953-09-03 | 1957-04-02 | Haszeldine Robert Neville | Organic halogen compounds and methods of making same |
EP0876314B1 (en) * | 1995-08-01 | 2003-02-26 | E.I. Du Pont De Nemours And Company | Process for the manufacture of halocarbons and selected compounds and azeotropes with hf |
US5902914A (en) * | 1995-08-14 | 1999-05-11 | Alliedsignal Inc. | Process for the preparation of halogenated alkanes |
JP3818398B2 (ja) | 1995-12-29 | 2006-09-06 | ダイキン工業株式会社 | 1,1,1,3,3−ペンタフルオロプロパンの製造方法 |
JPH09194404A (ja) * | 1996-01-17 | 1997-07-29 | Central Glass Co Ltd | 1−クロロ−3,3,3−トリフルオロプロペンの製造法 |
JP3516324B2 (ja) * | 1996-08-23 | 2004-04-05 | セントラル硝子株式会社 | 1−クロロ−3,3,3−トリフルオロプロペンの製造法 |
US6235951B1 (en) * | 1996-01-17 | 2001-05-22 | Central Glass Company, Limited | Method for producing 1,1,1,3,3-pentafluoropropane |
DE69713503T2 (de) * | 1996-04-04 | 2002-12-05 | Honeywell International Inc., Morristown | Reinigung von 1,1,1,3,3-pentafluorpropan (r-245fa) |
US6111150A (en) | 1996-06-20 | 2000-08-29 | Central Glass Company, Limited | Method for producing 1,1,1,3,3,-pentafluoropropane |
US5705779A (en) * | 1996-08-08 | 1998-01-06 | Alliedsignal Inc. | Preparation of 1,1,1,3,3-pentachloropropane by photochlorination of 1,1,1,3-tetrachloropropane |
US5710352A (en) | 1996-09-19 | 1998-01-20 | Alliedsignal Inc. | Vapor phase process for making 1,1,1,3,3-pentafluoropropane and 1-chloro-3,3,3-trifluoropropene |
US5811603A (en) * | 1997-12-01 | 1998-09-22 | Elf Atochem North America, Inc. | Gas phase fluorination of 1230za |
US5856595A (en) | 1998-03-03 | 1999-01-05 | Alliedsignal Inc. | Purified 1,1,1,3,3,3-hexafluoropropane and method for making same |
JP3518321B2 (ja) | 1998-03-23 | 2004-04-12 | ダイキン工業株式会社 | 1,1,1,3,3−ペンタフルオロプロパンの製造方法 |
JP3804289B2 (ja) * | 1998-09-22 | 2006-08-02 | ダイキン工業株式会社 | 1,1,1,3,3−ペンタフルオロプロパン及び/又は1−クロロ−3,3,3−トリフルオロプロペンの製造方法 |
US6313360B1 (en) | 2000-09-29 | 2001-11-06 | Vulcan Materials Company | Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane |
US6552238B1 (en) | 2001-08-31 | 2003-04-22 | Vulcan Chemicals | Separation of heavy ends from streams of halogenated alkanes |
US6720466B2 (en) | 2002-04-17 | 2004-04-13 | Vulcan Chemicals, a division of Vulcan Materials Company | 1,1,1,3,3-pentachloropropane process purge stream concentration using a secondary refluxed evaporator and secondary product recovery |
US6844475B1 (en) * | 2003-08-08 | 2005-01-18 | Honeywell International Business Machines | Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) |
US7112709B2 (en) | 2003-09-09 | 2006-09-26 | Vulcan Chemicals | Method for reusing heavy end by-products in the manufacture of polychlorinated alkanes |
US8058486B2 (en) * | 2004-04-29 | 2011-11-15 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
US8084653B2 (en) * | 2004-04-29 | 2011-12-27 | Honeywell International, Inc. | Method for producing fluorinated organic compounds |
US7265082B2 (en) | 2004-08-04 | 2007-09-04 | Honeywell International Inc. | Azeotrope-like compositions of 1,1,1,3,3-pentachloropropane and carbon tetrachloride |
CN1911512B (zh) | 2005-07-07 | 2011-12-07 | 独立行政法人产业技术综合研究所 | 氟化催化剂及其制备方法、以及使用了该催化剂的氟化合物的制备方法 |
EP2546223B1 (en) | 2006-01-03 | 2016-08-10 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
EP1837323A1 (en) | 2006-03-24 | 2007-09-26 | SOLVAY (Société Anonyme) | Process for the manufacture of 1,1,1,3,3-pentafluoropropane |
US9738577B2 (en) * | 2006-10-11 | 2017-08-22 | Honeywell International Inc. | Process for the manufacture of 1,1,1,3,3-pentachloropropane |
EP2091897B2 (en) | 2006-10-31 | 2021-12-01 | The Chemours Company FC, LLC | Processes for the production of fluoropropanes and halopropenes |
US8034251B2 (en) | 2007-01-03 | 2011-10-11 | Honeywell International Inc. | Azeotropic compositions of 2-chloro-3,3,3-trifluoropropene (HCFC-1233xf), 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb), and hydrogen fluoride (HF) |
US7795480B2 (en) | 2007-07-25 | 2010-09-14 | Honeywell International Inc. | Method for producing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf) |
AU2009244265B2 (en) * | 2008-05-07 | 2014-06-26 | The Chemours Company Fc, Llc. | Compositions comprising 2,3-dichloro-1,1,1-trifluoropropane, 2-chloro-1,1,1-trifluoropropene, 2-chloro-1,1,1,2-tetrafluoropropane or 2,3,3,3-tetrafluoropropene |
US8163196B2 (en) | 2008-10-28 | 2012-04-24 | Honeywell International Inc. | Azeotrope-like compositions comprising 1-chloro-3,3,3-trifluoropropene |
US8642818B2 (en) * | 2008-11-19 | 2014-02-04 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
CN105646135A (zh) | 2008-11-19 | 2016-06-08 | 阿科玛股份有限公司 | 用于制造氢氯氟烯烃的方法 |
US8217208B2 (en) * | 2008-12-12 | 2012-07-10 | Honeywell International, Inc. | Isomerization of 1-chloro-3,3,3-trifluoropropene |
US8075797B2 (en) * | 2009-01-29 | 2011-12-13 | Honeywell International Inc. | Azeotrope-like compositions of pentafluoropropane, chlorotrifluoropropene, and hydrogen fluoride |
JP5360230B2 (ja) | 2009-04-23 | 2013-12-04 | ダイキン工業株式会社 | 2−クロロ−3,3,3−トリフルオロプロペンの製造方法 |
US9045386B2 (en) | 2010-02-18 | 2015-06-02 | Honeywell International Inc. | Integrated process and methods of producing (E)-1-chloro-3,3,3-trifluoropropene |
US8704017B2 (en) * | 2010-09-03 | 2014-04-22 | Honeywell International Inc. | Continuous low-temperature process to produce trans-1-chloro-3,3,3-trifluoropropene |
US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
KR20130136500A (ko) * | 2011-01-04 | 2013-12-12 | 허니웰 인터내셔널 인코포레이티드 | 고순도의 e-1-클로로-3,3,3-트리플루오로프로펜 및 이의 제조방법 |
US9000240B2 (en) * | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
US9018428B2 (en) * | 2012-09-06 | 2015-04-28 | Honeywell International Inc. | Reactor and agitator useful in a process for making 1-chloro-3,3,3-trifluoropropene |
US8907146B2 (en) * | 2013-02-04 | 2014-12-09 | Honeywell International Inc. | Process for the preparation of 1-chloro-3,3,3-trifluoropropene using a phase transfer catalyst |
US9272967B2 (en) * | 2013-10-15 | 2016-03-01 | Honeywell International Inc. | Process for producing 1-chloro-3,3,3-trifluoropropene in an ionic liquid |
-
2011
- 2011-01-04 US US12/984,024 patent/US9156752B2/en active Active
-
2012
- 2012-01-03 CN CN201280004641.3A patent/CN103402953B/zh active Active
- 2012-01-03 JP JP2013548454A patent/JP6225028B2/ja active Active
- 2012-01-03 ES ES12732259.2T patent/ES2549641T3/es active Active
- 2012-01-03 KR KR1020187030599A patent/KR101990066B1/ko active IP Right Grant
- 2012-01-03 MX MX2013007757A patent/MX358513B/es active IP Right Grant
- 2012-01-03 EP EP12732259.2A patent/EP2661419B1/en active Active
- 2012-01-03 WO PCT/US2012/020035 patent/WO2012094288A2/en active Application Filing
-
2015
- 2015-08-31 US US14/840,481 patent/US9862662B2/en active Active
-
2016
- 2016-04-04 JP JP2016074840A patent/JP2016164172A/ja not_active Ceased
-
2017
- 2017-12-27 JP JP2017250588A patent/JP6527575B2/ja active Active
Also Published As
Publication number | Publication date |
---|---|
CN103402953B (zh) | 2015-08-12 |
US20120172636A1 (en) | 2012-07-05 |
CN103402953A (zh) | 2013-11-20 |
EP2661419B1 (en) | 2015-07-29 |
MX2013007757A (es) | 2013-08-15 |
EP2661419A2 (en) | 2013-11-13 |
US9156752B2 (en) | 2015-10-13 |
WO2012094288A2 (en) | 2012-07-12 |
JP6527575B2 (ja) | 2019-06-05 |
JP2016164172A (ja) | 2016-09-08 |
ES2549641T3 (es) | 2015-10-30 |
KR101990066B1 (ko) | 2019-06-17 |
US20160002128A1 (en) | 2016-01-07 |
JP2018070656A (ja) | 2018-05-10 |
US9862662B2 (en) | 2018-01-09 |
KR20180120276A (ko) | 2018-11-05 |
EP2661419A4 (en) | 2014-07-02 |
JP6225028B2 (ja) | 2017-11-01 |
JP2014509310A (ja) | 2014-04-17 |
WO2012094288A3 (en) | 2012-08-30 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
MX2013007757A (es) | E-1-cloro-3,3,3-trifluoropropeno de alta pureza y metodos para elaborar el mismo. | |
MX2019001056A (es) | Purificacion de materia prima mediante tratamiento termico. | |
PL2665694T3 (pl) | Sposób wytwarzania 2,3,3,3-tetrafluoropropenu przez fluorowanie pentachloropropanu w fazie gazowej | |
MX2012011219A (es) | Separacion de compuestos de punto de ebullicion cercano mediante la adicion de un tercer compuesto. | |
JP2009215294A5 (es) | ||
WO2014151448A3 (en) | An improved integrated process to produce 2,3,3,3-tetrafluoropropene | |
WO2012009114A3 (en) | Method for prolonging a catalyst's life during hydrofluorination | |
WO2012030613A3 (en) | 1,3,3,3-tetraflurorpropene process azeotropes with hf | |
MX2013005514A (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno. | |
MX2023009585A (es) | Isomerizacion catalitica de z-1,1,1,4,4,4-hexafluoro-2- buteno a e-1,1,1,4,4,4-hexafluoro-2-buteno. | |
IN2014DN10381A (es) | ||
PL2563750T3 (pl) | SPOSÓB WYTWARZANIA 2-CHLORO-3,3,3-TRIFLUOROPROPENU (HCFO 1233xf) PRZEZ FLUOROWANIE PENTACHLOROPROPANU W FAZIE CIEKŁEJ | |
MX344948B (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno. | |
MX2015010461A (es) | Proceso de fluoracion y reactor. | |
MX2014004250A (es) | Proceso para producir 2,3,3,-tetrafluoropropeno. | |
WO2013106046A3 (en) | Purification of trans-1,3,3,3-tetrafluoropropene | |
IN2014DN02915A (es) | ||
MX2013009366A (es) | Proceso para cis-1-cloro-3,3,3-trifluoropropeno. | |
MX2018005908A (es) | Proceso para preparar 2,3,3,3-tetrafluoropropeno y/o fluoruro de vinilideno. | |
PL2630107T3 (pl) | Sposób wytwarzania 2-chloro-3,3,3-trifluropropenu przez fluorowanie w fazie gazowej pentachloropropanu | |
AR088658A1 (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno | |
MX2015011156A (es) | Procedimiento de fluoracion escalonado y sistema de reactores. | |
MY185235A (en) | New crystalline form vii of agomelatine, preparation method and use thereof and pharmaceutical composition containing same | |
MX2016012851A (es) | Un metodo para producir 1,1,2,3-tetracloropropeno con alto rendimiento. | |
MX2016010693A (es) | Proceso para la fabricacion de hidroclorofluoroolefinas. |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG | Grant or registration |