MX355197B - Proceso para la recuperación de betaína de melazas. - Google Patents
Proceso para la recuperación de betaína de melazas.Info
- Publication number
- MX355197B MX355197B MX2014005858A MX2014005858A MX355197B MX 355197 B MX355197 B MX 355197B MX 2014005858 A MX2014005858 A MX 2014005858A MX 2014005858 A MX2014005858 A MX 2014005858A MX 355197 B MX355197 B MX 355197B
- Authority
- MX
- Mexico
- Prior art keywords
- molasses
- fructan
- betaine
- recovery
- iii
- Prior art date
Links
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 title abstract 5
- 235000013379 molasses Nutrition 0.000 title abstract 5
- 229960003237 betaine Drugs 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 238000011084 recovery Methods 0.000 title abstract 2
- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 title 1
- 239000002994 raw material Substances 0.000 abstract 2
- 102000004190 Enzymes Human genes 0.000 abstract 1
- 108090000790 Enzymes Proteins 0.000 abstract 1
- 229920002670 Fructan Polymers 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000013375 chromatographic separation Methods 0.000 abstract 1
- 238000005115 demineralization Methods 0.000 abstract 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/33—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from molasses
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P13/00—Preparation of nitrogen-containing organic compounds
- C12P13/001—Amines; Imines
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
- C13B20/144—Purification of sugar juices using ion-exchange materials using only cationic ion-exchange material
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/007—Separation of sugars provided for in subclass C13K
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Biochemistry (AREA)
- Food Science & Technology (AREA)
- Zoology (AREA)
- Molecular Biology (AREA)
- Nutrition Science (AREA)
- Wood Science & Technology (AREA)
- General Health & Medical Sciences (AREA)
- Biotechnology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Genetics & Genomics (AREA)
- General Engineering & Computer Science (AREA)
- Botany (AREA)
- Animal Husbandry (AREA)
- Physiology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Emergency Medicine (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Fodder In General (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Enzymes And Modification Thereof (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La presente invención se refiere a un proceso para recuperar betaína de una materia prima que consiste esencialmente en melaza, que comprende: i. una etapa de desmineralización, donde la cantidad total de sales en la melaza llega a un nivel inferior al 2% en peso (en materia seca total); ii. Una etapa de conversión, donde la melaza se somete a la acción de una enzima formadora de fructano, para formar una melaza que contiene fructano (fructano-melaza); iii. Una etapa de separación donde la fructano-melaza se somete a una separación cromatográfica, con lo que se obtiene una fracción que contiene betaína, en donde la relación de betaína respecto a otros constituyentes de la materia seca se incrementa a por lo menos 90:10, por lo cual la etapa (i) se ejecuta antes de la etapa (iii) y por lo cual la etapa (i) puede ejecutarse antes, durante o con posterioridad a la etapa (ii), en donde en la etapa de separación (iii) se utiliza un sistema de resina de intercambio iónico de ácido fuerte que consiste de resinas, por lo cual entre 20 y 95% son resinas en forma de sodio o potasio, y entre 5 y 80 % son resinas en forma de calcio.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11009055 | 2011-11-15 | ||
| PCT/EP2012/004732 WO2013072048A1 (en) | 2011-11-15 | 2012-11-15 | Process for the recovery of betaine from molasses |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2014005858A MX2014005858A (es) | 2015-06-02 |
| MX355197B true MX355197B (es) | 2018-04-09 |
Family
ID=47458845
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014005858A MX355197B (es) | 2011-11-15 | 2012-11-15 | Proceso para la recuperación de betaína de melazas. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US9896410B2 (es) |
| EP (1) | EP2802665B1 (es) |
| JP (1) | JP6215833B2 (es) |
| KR (2) | KR102075326B1 (es) |
| CN (1) | CN104080920B (es) |
| BR (1) | BR112014011636B1 (es) |
| CA (1) | CA2855787C (es) |
| CL (1) | CL2014001290A1 (es) |
| EA (1) | EA031950B1 (es) |
| ES (1) | ES2685330T3 (es) |
| MX (1) | MX355197B (es) |
| WO (1) | WO2013072048A1 (es) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2386649A1 (en) | 2010-05-12 | 2011-11-16 | Tiense Suikerraffinaderij N.V. | Process for the recovery of betaine from molasses |
| US20170135377A1 (en) * | 2014-06-26 | 2017-05-18 | Tiense Suikerraffinaderij N.V. | Betaine composition, glucose composition, and uses thereof |
| CN105566137A (zh) * | 2015-12-25 | 2016-05-11 | 安徽丰原发酵技术工程研究有限公司 | 一种从甜菜糖蜜中分离纯化甜菜碱的方法 |
| CN107573253B (zh) * | 2017-10-25 | 2020-03-27 | 广州英赛特生物技术有限公司 | N,n-二甲基甘氨酸有机酸共轭酸盐及其组合物和应用 |
| US12215817B2 (en) | 2019-08-08 | 2025-02-04 | Northwest Pipe Company | Seismic pipe joint |
| JP2023520751A (ja) * | 2020-03-04 | 2023-05-19 | ジトニー，ボリス | 甜菜乾物の定性分布方法、当該方法で得られた製品および当該製品を含む食品 |
| CN112624934A (zh) * | 2020-12-08 | 2021-04-09 | 武汉美味源生物工程有限公司 | 从甜菜糖蜜中提取天然甜菜碱的方法 |
| WO2025144770A1 (en) | 2023-12-29 | 2025-07-03 | Complete Solution For Poultry (Csp), Inc. | High purity betaine products, polyphenol products, and methods of making the same |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3884714A (en) * | 1973-07-09 | 1975-05-20 | Pfeiffer & Langen | Process for making sugar from molasses by ion removal |
| JPS62126951A (ja) * | 1985-11-28 | 1987-06-09 | Nippon Beet Sugar Mfg Co Ltd | ビフイズス菌増殖糖質源を含有する甘味料の製造方法 |
| JPH01109000A (ja) * | 1987-10-23 | 1989-04-26 | Hokuren Federation Of Agricult Coop:The | 甜菜糖液の処理方法 |
| FI86416C (fi) * | 1988-06-09 | 1992-08-25 | Suomen Sokeri Oy | Foerfarande foer tillvaratagande av betain ur melass. |
| JPH10179200A (ja) * | 1996-12-27 | 1998-07-07 | Japan Organo Co Ltd | ビート糖液の精製方法および精製装置 |
| CA2272562A1 (en) * | 1997-09-22 | 1999-04-01 | Organo Corporation | Chromatographic separation process and separator |
| DE60127675T2 (de) | 2000-06-28 | 2007-12-27 | Fuji Nihon Seito Corp. | Neuartige insulin synthase und verfahren zur herstellung von insulin durch anwendung derselben |
| FI20002150L (fi) | 2000-09-29 | 2002-03-30 | Finnfeeds Finland Oy | Menetelmä tuotteiden talteenottamiseksi prosessiliuoksista |
| GB2433518A (en) * | 2005-12-21 | 2007-06-27 | Danisco | Process for the recovery of sucrose and non-sucrose materials |
| EP2386649A1 (en) * | 2010-05-12 | 2011-11-16 | Tiense Suikerraffinaderij N.V. | Process for the recovery of betaine from molasses |
-
2012
- 2012-11-15 EP EP12808250.0A patent/EP2802665B1/en active Active
- 2012-11-15 EA EA201490896A patent/EA031950B1/ru not_active IP Right Cessation
- 2012-11-15 KR KR1020197023054A patent/KR102075326B1/ko active Active
- 2012-11-15 JP JP2014540360A patent/JP6215833B2/ja active Active
- 2012-11-15 ES ES12808250.0T patent/ES2685330T3/es active Active
- 2012-11-15 KR KR1020147016222A patent/KR20140110864A/ko not_active Ceased
- 2012-11-15 CA CA2855787A patent/CA2855787C/en active Active
- 2012-11-15 US US14/358,259 patent/US9896410B2/en not_active Expired - Fee Related
- 2012-11-15 BR BR112014011636-9A patent/BR112014011636B1/pt active IP Right Grant
- 2012-11-15 CN CN201280064269.5A patent/CN104080920B/zh active Active
- 2012-11-15 MX MX2014005858A patent/MX355197B/es active IP Right Grant
- 2012-11-15 WO PCT/EP2012/004732 patent/WO2013072048A1/en not_active Ceased
-
2014
- 2014-05-15 CL CL2014001290A patent/CL2014001290A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA2855787C (en) | 2020-01-14 |
| KR20190097286A (ko) | 2019-08-20 |
| CN104080920B (zh) | 2019-02-26 |
| JP2014534230A (ja) | 2014-12-18 |
| KR20140110864A (ko) | 2014-09-17 |
| BR112014011636B1 (pt) | 2019-10-08 |
| KR102075326B1 (ko) | 2020-02-07 |
| EP2802665B1 (en) | 2018-06-06 |
| US9896410B2 (en) | 2018-02-20 |
| CA2855787A1 (en) | 2013-05-23 |
| CL2014001290A1 (es) | 2014-11-14 |
| US20140295505A1 (en) | 2014-10-02 |
| BR112014011636A2 (pt) | 2017-05-02 |
| WO2013072048A1 (en) | 2013-05-23 |
| CN104080920A (zh) | 2014-10-01 |
| EA201490896A1 (ru) | 2014-11-28 |
| EA031950B1 (ru) | 2019-03-29 |
| MX2014005858A (es) | 2015-06-02 |
| EP2802665A1 (en) | 2014-11-19 |
| JP6215833B2 (ja) | 2017-10-18 |
| ES2685330T3 (es) | 2018-10-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |