MX3304E - Procedimiento para preparar un alfa-aminoacido - Google Patents
Procedimiento para preparar un alfa-aminoacidoInfo
- Publication number
- MX3304E MX3304E MX000157U MX15776U MX3304E MX 3304 E MX3304 E MX 3304E MX 000157 U MX000157 U MX 000157U MX 15776 U MX15776 U MX 15776U MX 3304 E MX3304 E MX 3304E
- Authority
- MX
- Mexico
- Prior art keywords
- amino acid
- alpha
- preparing
- procedure
- salt
- Prior art date
Links
- 235000008206 alpha-amino acids Nutrition 0.000 title abstract 2
- 150000001370 alpha-amino acid derivatives Chemical class 0.000 title 1
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 abstract 1
- IOVCWXUNBOPUCH-UHFFFAOYSA-N Nitrous acid Chemical group ON=O IOVCWXUNBOPUCH-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000001371 alpha-amino acids Chemical class 0.000 abstract 1
- 235000001014 amino acid Nutrition 0.000 abstract 1
- 150000001413 amino acids Chemical class 0.000 abstract 1
- 125000003917 carbamoyl group Chemical group [H]N([H])C(*)=O 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- 239000003456 ion exchange resin Substances 0.000 abstract 1
- 229920003303 ion-exchange polymer Polymers 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000007800 oxidant agent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
- C07C229/08—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to hydrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
- C07C227/18—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters
- C07C227/20—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters by hydrolysis of N-acylated amino-acids or derivatives thereof, e.g. hydrolysis of carbamates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La presente invención se refiere a procedimiento para preparar un alfa-aminoácido, caracterizado porque consiste en hacer reaccionar el derivado de N-carbamoil del aminoácido deseado, o una sal del mismo derivado, con un agente de oxidación en presencia de una resina de intercambio iónico que contiene un grupo ácido, la cantidad de reactivos es tal que el agente de oxidación está en una proporción de 1,0-1,5 equivalentes por mol de derivado de carbamoil, a una temperatura de reacción comprendida entre 0 y 40°C, caracterizado por que el agente de oxidación es ácido nitroso o una sal del mismo.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT22144/75A IT1037176B (it) | 1975-04-09 | 1975-04-09 | Procedimento per la preparazione di ammindacidi |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX3304E true MX3304E (es) | 1980-09-08 |
Family
ID=11192138
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX000157U MX3304E (es) | 1975-04-09 | 1976-04-09 | Procedimiento para preparar un alfa-aminoacido |
Country Status (38)
| Country | Link |
|---|---|
| JP (1) | JPS5940823B2 (es) |
| AR (1) | AR217052A1 (es) |
| AT (1) | AT343092B (es) |
| AU (1) | AU503651B2 (es) |
| BE (1) | BE840527A (es) |
| BG (1) | BG24664A3 (es) |
| BR (1) | BR7602173A (es) |
| CA (1) | CA1058213A (es) |
| CH (1) | CH620421A5 (es) |
| CS (1) | CS194756B2 (es) |
| DD (1) | DD123599A5 (es) |
| DE (1) | DE2615594C3 (es) |
| DK (1) | DK146622C (es) |
| EG (1) | EG12543A (es) |
| ES (1) | ES447176A1 (es) |
| FR (1) | FR2306976A1 (es) |
| GB (1) | GB1490054A (es) |
| HU (1) | HU176009B (es) |
| IE (1) | IE42673B1 (es) |
| IL (1) | IL49372A (es) |
| IN (1) | IN144346B (es) |
| IT (1) | IT1037176B (es) |
| LU (1) | LU74714A1 (es) |
| MW (1) | MW1076A1 (es) |
| MX (1) | MX3304E (es) |
| MY (1) | MY7900100A (es) |
| NL (1) | NL7603816A (es) |
| NO (1) | NO143901C (es) |
| PH (1) | PH12101A (es) |
| PL (1) | PL104015B1 (es) |
| PT (1) | PT64983B (es) |
| RO (1) | RO70427A (es) |
| SE (1) | SE409701B (es) |
| SU (1) | SU670213A3 (es) |
| TR (1) | TR18877A (es) |
| YU (1) | YU90376A (es) |
| ZA (1) | ZA761941B (es) |
| ZM (1) | ZM4476A1 (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS584707B2 (ja) * | 1977-02-21 | 1983-01-27 | 鐘淵化学工業株式会社 | 光学活性フエニルグリシン類の製造法 |
| IT1204979B (it) * | 1987-04-28 | 1989-03-10 | Eniricerche Spa | Sintesi di alfa amminoacidi otticamente attivi |
| FR2725991B1 (fr) * | 1994-10-24 | 1997-01-17 | Univ Montpellier Ii | Procede de synthese peptidique a partir des n-(n'-(r')-n' -nitrosocarbamoyls) aminoacides |
| CN1057518C (zh) * | 1995-09-29 | 2000-10-18 | 中国科学院微生物研究所 | 氮－氨甲酰基氨基酸热水解制备光学活性氨基酸的方法 |
| US6087136A (en) * | 1997-03-31 | 2000-07-11 | Council Of Scientific & Industrial Research | Microbial process for the production of D(-)-N-carbamoylphenylglycine |
| CN105601542B (zh) * | 2016-01-08 | 2017-10-24 | 南京工业大学 | 一种混酸结晶n‑氨甲酰谷氨酸的方法 |
-
1975
- 1975-04-09 IT IT22144/75A patent/IT1037176B/it active
-
1976
- 1976-03-31 ZA ZA761941A patent/ZA761941B/xx unknown
- 1976-03-31 DK DK154676A patent/DK146622C/da not_active IP Right Cessation
- 1976-04-01 MW MW10/76A patent/MW1076A1/xx unknown
- 1976-04-02 CA CA249,437A patent/CA1058213A/en not_active Expired
- 1976-04-05 CH CH423676A patent/CH620421A5/it not_active IP Right Cessation
- 1976-04-05 EG EG196/76A patent/EG12543A/xx active
- 1976-04-05 ZM ZM44/76A patent/ZM4476A1/xx unknown
- 1976-04-05 AU AU12648/76A patent/AU503651B2/en not_active Expired
- 1976-04-06 GB GB13783/76A patent/GB1490054A/en not_active Expired
- 1976-04-06 TR TR18877A patent/TR18877A/xx unknown
- 1976-04-07 DD DD192242A patent/DD123599A5/xx unknown
- 1976-04-07 LU LU74714A patent/LU74714A1/xx unknown
- 1976-04-07 NO NO761189A patent/NO143901C/no unknown
- 1976-04-07 PT PT64983A patent/PT64983B/pt unknown
- 1976-04-07 FR FR7610087A patent/FR2306976A1/fr active Granted
- 1976-04-08 CS CS762334A patent/CS194756B2/cs unknown
- 1976-04-08 PH PH18315A patent/PH12101A/en unknown
- 1976-04-08 BR BR7602173A patent/BR7602173A/pt unknown
- 1976-04-08 YU YU00903/76A patent/YU90376A/xx unknown
- 1976-04-08 HU HU76SA2914A patent/HU176009B/hu unknown
- 1976-04-08 AT AT258276A patent/AT343092B/de not_active IP Right Cessation
- 1976-04-08 BE BE165963A patent/BE840527A/xx not_active IP Right Cessation
- 1976-04-08 IN IN611/CAL/76A patent/IN144346B/en unknown
- 1976-04-08 IE IE737/76A patent/IE42673B1/en unknown
- 1976-04-08 IL IL49372A patent/IL49372A/xx unknown
- 1976-04-09 MX MX000157U patent/MX3304E/es unknown
- 1976-04-09 ES ES447176A patent/ES447176A1/es not_active Expired
- 1976-04-09 PL PL1976188626A patent/PL104015B1/pl unknown
- 1976-04-09 SU SU762343157A patent/SU670213A3/ru active
- 1976-04-09 NL NL7603816A patent/NL7603816A/xx active Search and Examination
- 1976-04-09 BG BG032860A patent/BG24664A3/xx unknown
- 1976-04-09 SE SE7604237A patent/SE409701B/xx unknown
- 1976-04-09 JP JP51039420A patent/JPS5940823B2/ja not_active Expired
- 1976-04-09 RO RO7685571A patent/RO70427A/ro unknown
- 1976-04-09 AR AR262843A patent/AR217052A1/es active
- 1976-04-09 DE DE2615594A patent/DE2615594C3/de not_active Expired
-
1979
- 1979-12-30 MY MY100/79A patent/MY7900100A/xx unknown
Also Published As
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| MX3304E (es) | Procedimiento para preparar un alfa-aminoacido | |
| GB937380A (en) | A method for preparing unsaturated aliphatic nitriles | |
| GB965637A (en) | L-ornithine l-aspartate | |
| ES392133A1 (es) | Procedimiento de preparacion de acido nitrico muy concen- trado. | |
| ES8202818A1 (es) | Un procedimiento para preparar derivados de tetrazolilcuma- rina | |
| GB1287710A (en) | Process for increasing the corrosion resistance of austenitic stainless steels | |
| GB940289A (en) | Process for the manufacture of hydrogen fluoride | |
| ES457127A1 (es) | Procedimiento para recuperar hierro de un lodo de hierro quecontiene una mezcla de yeso e hidroxido ferrico. | |
| GB950774A (en) | The production of cerium (iv) molybdate, tungstate and vanadate | |
| ES449665A1 (es) | Procedimieto de oxidacion de un sulfato ferroso en solucion acuosa sulfurica. | |
| ATE1239T1 (de) | Verfahren zur herstellung von 4-amino-5-chlor-1-phenyl-pyridazon-(6). | |
| GB1061555A (en) | Improvements in or relating to the production of potassium monopersulphate | |
| GB1039376A (en) | Process for preparing bis-hydroxyalkylsulphones and ª‰-hydroxyalkylsulphonic acid salts | |
| GB950364A (en) | Improvements in or relating to a method for producing ferritetracemic acid | |
| GB947842A (en) | Improved process for the preparation of nitrocyclohexane | |
| GB867268A (en) | Process for preparing 3-nitro-azacyclo-alkanone-2-n-carbochlorides | |
| GB991552A (en) | Improvements in or relating to the manufacture of homocysteic acid | |
| GB1063267A (en) | Improved method for the preparation of dicyclohexylketone | |
| GB1077928A (en) | Amino alicylene phosphonic acids | |
| GB1037011A (en) | Novel sulpholane oximes | |
| GR22386B (el) | Μεθοδος δια την παραγωγην π - υδροξυβενζοικου οξεος. | |
| GB1033169A (en) | Auramine process using sulfamic acid | |
| ES454076A1 (es) | Procedimiento para la monoacilacion de una diamina primaria aromatica. | |
| GB1369409A (en) | Process for the manufacture of 1-nitro-anthraquinone | |
| GB970800A (en) | Preparation of azodicarbonamide |