MX2019005254A - Proceso para la purificacion de pirazolpiridazinas. - Google Patents

Proceso para la purificacion de pirazolpiridazinas.

Info

Publication number
MX2019005254A
MX2019005254A MX2019005254A MX2019005254A MX2019005254A MX 2019005254 A MX2019005254 A MX 2019005254A MX 2019005254 A MX2019005254 A MX 2019005254A MX 2019005254 A MX2019005254 A MX 2019005254A MX 2019005254 A MX2019005254 A MX 2019005254A
Authority
MX
Mexico
Prior art keywords
pyrazolpyridazines
purification
hcl
zolpyridazine
aqueos
Prior art date
Application number
MX2019005254A
Other languages
English (en)
Inventor
Dietz Jochen
Gebhardt Joachim
Gockel Birgit
Soergel Sebastian
Goetz Roland
Klauber Eric
Maria Martinus Bastiaans Henricus
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2019005254A publication Critical patent/MX2019005254A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D403/00Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00
    • C07D403/02Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings
    • C07D403/12Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings linked by a chain containing hetero atoms as chain links
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/581,2-Diazines; Hydrogenated 1,2-diazines

Landscapes

  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Environmental Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)

Abstract

La presente invención se refiere a un proceso para la purificación de pirazolpiridazinas de la Formula I (ver Fórmula) en donde las variables son como se definen en la memoria descriptiva, mediante la adición de HCI a una solución de pirazolpiridazina en solvente inerte en condiciones no acuosas, efectuando la cristalización de la sal HCI y el aislamiento de precipitación resultante.
MX2019005254A 2016-11-04 2017-10-27 Proceso para la purificacion de pirazolpiridazinas. MX2019005254A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16197197 2016-11-04
PCT/EP2017/077657 WO2018083040A1 (en) 2016-11-04 2017-10-27 Process for purification of pyrazolpyridazines

Publications (1)

Publication Number Publication Date
MX2019005254A true MX2019005254A (es) 2019-08-05

Family

ID=57226866

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019005254A MX2019005254A (es) 2016-11-04 2017-10-27 Proceso para la purificacion de pirazolpiridazinas.

Country Status (17)

Country Link
US (1) US10961226B2 (es)
EP (1) EP3535257B1 (es)
CN (1) CN109843875A (es)
AR (1) AR110119A1 (es)
AU (1) AU2017353264B2 (es)
BR (1) BR112019009078B1 (es)
CY (1) CY1123846T1 (es)
DK (1) DK3535257T3 (es)
ES (1) ES2858699T3 (es)
HR (1) HRP20210321T1 (es)
LT (1) LT3535257T (es)
MX (1) MX2019005254A (es)
PL (1) PL3535257T3 (es)
PT (1) PT3535257T (es)
SI (1) SI3535257T1 (es)
WO (1) WO2018083040A1 (es)
ZA (1) ZA201903408B (es)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3601202B1 (en) 2017-03-20 2023-05-10 Basf Se Process for preparing bromotrichloromethane
EP3704086B1 (en) 2017-11-02 2024-02-21 Basf Se Process for preparing 4-chlorobenzyl propargyl ether
AU2020267712A1 (en) * 2019-05-03 2021-11-25 Basf Se Stabilization of suspension concentrates by highly sulfonated lignosulfonate
US20220159957A1 (en) * 2019-05-03 2022-05-26 Basf Se Stabilization of suspension concentrates by ethoxylated ricinolein
CA3135715A1 (en) * 2019-05-03 2020-11-12 Wen Xu Stabilization of suspension concentrates by hydrophobic fumed silica

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EA024737B1 (ru) 2011-04-21 2016-10-31 Басф Се Новые пестицидные соединения пиразола
WO2015189080A1 (en) 2014-06-12 2015-12-17 Basf Se Pesticidally active mixtures
WO2016071243A1 (en) 2014-11-05 2016-05-12 Basf Se Process for preparing halogenated alkenone ethers and their use in the synthesis of anthranilamide pesticides
BR112017015061B1 (pt) 2015-02-11 2022-09-27 Basf Se Mistura pesticida compreendendo um composto ativo de fórmula ia e broflanilida
WO2016128239A1 (en) 2015-02-11 2016-08-18 Basf Se Pesticidal mixture comprising a pyrazole compound and a biopesticide
WO2016128240A1 (en) 2015-02-11 2016-08-18 Basf Se Pesticidal mixture comprising a pyrazole compound and two fungicides
WO2016180642A1 (en) 2015-05-08 2016-11-17 BASF Agro B.V. A process for the preparation of terpinolene epoxide
EP3294700B1 (en) 2015-05-08 2020-01-29 BASF Agro B.V. A process for the preparation of limonene-4-ol
CA3187499A1 (en) 2015-05-11 2016-11-17 Eric George KLAUBER Process for preparing 4-amino-pyridazines
CN107709284B (zh) 2015-06-17 2021-11-23 巴斯夫农业公司 制备取代的苯基酮的方法
US20180184654A1 (en) 2015-07-02 2018-07-05 BASF Agro B.V. Pesticidal Compositions Comprising a Triazole Compound
EP3331364A1 (en) 2015-08-07 2018-06-13 Basf Se Control of pests in maize by ginkgolides and bilobalide
BR112018001863B1 (pt) 2015-08-10 2023-11-14 Basf Se Processo para a preparação de n-[2-[[[1-(4-clorofenil)- 1h-pirazol-3-il] oxi]metil]fenil]
AU2016313008A1 (en) 2015-08-25 2018-03-01 Basf Se Control of pests in cotton by ginkgolides and bilobalides
EA201890854A1 (ru) 2015-10-02 2018-10-31 Басф Се Иминосоединения с 2-хлорпиримидин-5-ильным заместителем в качестве средств борьбы с вредителями
KR102642072B1 (ko) 2015-12-18 2024-02-28 바스프 아그로 비.브이. 2-[4-(4-클로로페녹시)-2-(트리플루오로메틸)페닐]-1-(1,2,4-트리아졸-1-일)프로판-2-올의 제조 방법
ES2795874T3 (es) 2016-02-02 2020-11-25 Basf Se Proceso de hidrogenación catalítica para preparar pirazoles
BR112018015328B1 (pt) 2016-02-19 2022-08-16 Basf Se Métodos para o controle de pragas em plantas, método para controlar pragas da família de pentatomidae e/ ou miridae e uso de um ou mais compostos de fórmula i
WO2017144336A1 (en) 2016-02-26 2017-08-31 BASF Agro B.V. Process for preparing terpinene-4-ol
KR20180117658A (ko) 2016-02-26 2018-10-29 바스프 아그로 비.브이. 테르펜 알콜 혼합물의 제조 방법
BR112018068042A2 (pt) 2016-03-11 2019-01-08 Basf Se métodos para controlar pragas de plantas, material de propagação de planta e uso de um ou mais compostos de fórmula i
WO2017215929A1 (en) 2016-06-15 2017-12-21 BASF Agro B.V. Process for the epoxidation of a tetrasubstituted alkene
WO2017215928A1 (en) 2016-06-15 2017-12-21 BASF Agro B.V. Process for the epoxidation of a tetrasubstituted alkene
CN109415280A (zh) 2016-07-07 2019-03-01 巴斯夫欧洲公司 用于制备杀虫环戊烯类化合物的Oxy-Cope重排
CA3033313A1 (en) 2016-08-30 2018-03-08 Basf Se Method for controlling pests in modified plants
ES2878582T3 (es) 2016-09-19 2021-11-19 Basf Agro Bv Proceso para preparar 2-exo-(2-metilbenciloxi)-1-metil-4-isopropil-7-oxabiciclo[2.2.1]heptano
WO2018082962A1 (en) 2016-11-02 2018-05-11 Basf Se Process for preparation of tetrahydrothiophene derivatives
WO2018082964A1 (en) 2016-11-04 2018-05-11 Basf Se Process for the production of pyridazinyl-amides in a one-pot synthesis

Also Published As

Publication number Publication date
EP3535257B1 (en) 2020-12-09
HRP20210321T1 (hr) 2021-04-02
ES2858699T3 (es) 2021-09-30
PT3535257T (pt) 2021-02-17
AU2017353264B2 (en) 2021-08-05
WO2018083040A1 (en) 2018-05-11
ZA201903408B (en) 2021-02-24
SI3535257T1 (sl) 2021-04-30
CN109843875A (zh) 2019-06-04
US20190308954A1 (en) 2019-10-10
BR112019009078B1 (pt) 2022-12-27
CY1123846T1 (el) 2022-05-27
EP3535257A1 (en) 2019-09-11
DK3535257T3 (da) 2021-03-01
BR112019009078A2 (pt) 2019-07-16
LT3535257T (lt) 2021-02-25
AR110119A1 (es) 2019-02-27
PL3535257T3 (pl) 2021-06-14
US10961226B2 (en) 2021-03-30
AU2017353264A1 (en) 2019-05-02

Similar Documents

Publication Publication Date Title
MX2019005254A (es) Proceso para la purificacion de pirazolpiridazinas.
SA518400053B1 (ar) عملية مُحسنة لإنتاج حمض أكريليك
MY172391A (en) Processes for preparing dihydropyrimidine derivatives and intermediates thereof
PH12019502386A1 (en) Process for preparing s-containing pyrimidinium compounds
PH12019502286A1 (en) Process for preparing an optically active pyrimidinium compounds
JOP20160185B1 (ar) طريقة لتحضير (4s)-4-(4- سيانو-2- ميثوكسي فنيل)-5- إيثوكسي-8،2-داي ميثيل-4،1-داي هيدرو-6،1- نافثيريدين-3- كربوكساميد واسترجاع (4s)-4-(4- سيانو-2- ميثوكسي فنيل)-5- إيثوكسي-8،2- داي ميثيل-4،1- داي هيدرو-6،1- نافثيريدين-3- كربوكساميد بواسطة طرق كهروكيميائية
WO2015159275A3 (en) An improved process for the preparation of rifamycin derivatives
BR112017001177A2 (pt) processo para a purificação de poliovírus a partir de culturas celulares
BR112017019850A2 (pt) ?processo melhorado para a preparação de apremilast?
MX2016000390A (es) Proceso para fabricar haloacetamidas.
MX2017017022A (es) Metodo para la sintesis de derivados de rapamicina.
MX2017005630A (es) Metodo para preparar bifenilaminas a partir de azobencenos mediante catalisis de rutenio.
NZ725417A (en) New sulfonylaminobenzamide compounds
NZ728623A (en) Novel sulfonylaminobenzamide compounds as anthelmintics
PH12017501404A1 (en) Diaza-benzofluoranthrene compounds
WO2014087208A3 (en) A process of preparing alcaftadine
MX350430B (es) Proceso para preparar compuestos acido 4-amino-5-bifenil-4-il-2-hi droximetil-2-metil-pentanoico.
MY174153A (en) Processes for the preparation of pyrimidinylcyclopentane compounds
MX367267B (es) Proceso para preparar 3-(3-(4-(1-aminociclobutil)fenil)-5-fenil-3h -imidazo[4,5-b]piridin-2-il)piridin-2-amina.
BR112016022437A2 (pt) Processo para preparação de (2s,5r)-6-(benziloxi)-7-oxo-1,6- diazabiciclo[3,2,1]octano-2-carboxilato de sódio
MX2016009325A (es) Metodo para la preparacion de 1-alquil-3-difluorometil-5-fluor-1h- pirazol-4-carbaldehidos y 1-alquil-3-difluorometil-5-fluor-1h-pira zol-4-carboxilatos.
MX2016007186A (es) Nuevo procedimiento de sintesis de la agomelatina.
PH12019500081A1 (en) Method for producing crystal of uracil compound
WO2014102834A3 (en) Process for lurasidone
IN2013MU01457A (es)