MX2017006073A - Procedimiento para la produccion de ciclohexanona a partir de fenol. - Google Patents
Procedimiento para la produccion de ciclohexanona a partir de fenol.Info
- Publication number
- MX2017006073A MX2017006073A MX2017006073A MX2017006073A MX2017006073A MX 2017006073 A MX2017006073 A MX 2017006073A MX 2017006073 A MX2017006073 A MX 2017006073A MX 2017006073 A MX2017006073 A MX 2017006073A MX 2017006073 A MX2017006073 A MX 2017006073A
- Authority
- MX
- Mexico
- Prior art keywords
- phenol
- cyclohexanone
- production
- hydrogenation reactor
- charged
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/006—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrogenation of aromatic hydroxy compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
- B01J21/04—Alumina
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B01J23/44—Palladium
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
- C07C29/19—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds in six-membered aromatic rings
- C07C29/20—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds in six-membered aromatic rings in a non-condensed rings substituted with hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
- C07C35/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic
- C07C35/08—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
- C07C39/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with no unsaturation outside the aromatic ring
- C07C39/04—Phenol
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/002—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by dehydrogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/385—Saturated compounds containing a keto group being part of a ring
- C07C49/403—Saturated compounds containing a keto group being part of a ring of a six-membered ring
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00027—Process aspects
- B01J2219/00033—Continuous processes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Abstract
Se describe un procedimiento continuo a escala industrial para la producción y recuperación de ciclohexanona a partir de fenol e hidrógeno, dicho procedimiento comprendiendo: hidrogenar fenol en un reactor de hidrogenación de fenol; separar ciclohexanona a partir de una corriente de producto hidrogenado en una sección de separación y purificación [II] que comprende por lo menos 4 secciones de destilación; en donde por lo menos parte del calor de reacción producido en la sección de reacción de hidrogenación de fenol [I] se aplica para la producción de vapor; y en donde la relación molar de ciclohexanona a fenol que es cargada a dicho reactor de hidrogenación de fenol es de 0.02 a 0.10; y/o en donde la relación molar de ciclohexanol a fenol que es cargada a dicho reactor de hidrogenación de fenol es de 0.001 a 0.10.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP14192423 | 2014-11-10 | ||
EP2015075113 | 2015-10-29 | ||
PCT/EP2015/075951 WO2016075047A1 (en) | 2014-11-10 | 2015-11-06 | Process for the production of cyclohexanone from phenol |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2017006073A true MX2017006073A (es) | 2018-01-11 |
Family
ID=55953768
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2017006073A MX2017006073A (es) | 2014-11-10 | 2015-11-06 | Procedimiento para la produccion de ciclohexanona a partir de fenol. |
Country Status (12)
Country | Link |
---|---|
US (1) | US10301243B2 (es) |
EP (1) | EP3218338B1 (es) |
JP (1) | JP6249467B1 (es) |
KR (1) | KR101820639B1 (es) |
CN (1) | CN107124881B (es) |
EA (1) | EA031615B1 (es) |
ES (1) | ES2803082T3 (es) |
MX (1) | MX2017006073A (es) |
PL (1) | PL3218338T3 (es) |
SA (1) | SA517381498B1 (es) |
UA (1) | UA122897C2 (es) |
WO (1) | WO2016075047A1 (es) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110563564B (zh) * | 2018-06-06 | 2022-02-01 | 中国石油化工股份有限公司 | 苯酚加氢制备环己酮的方法 |
CN108816223B (zh) * | 2018-07-09 | 2021-08-20 | 江苏凌飞科技股份有限公司 | 一种制备壬基环己醇聚氧乙烯醚用的催化剂及其制备方法 |
CN110372462A (zh) * | 2019-08-06 | 2019-10-25 | 吉林凯莱英医药化学有限公司 | 连续化合成-纯化一体装置及含有其的连续化反应系统 |
EP4288401A1 (en) | 2021-02-04 | 2023-12-13 | Cap Iii B.V. | Process control for the hydrogenation of phenol |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2829166A (en) | 1933-04-04 | 1958-04-01 | Allied Chem & Dye Corp | Hydrogenation of phenol |
US5015787A (en) | 1989-04-10 | 1991-05-14 | Allied-Signal Inc. | Process for production cyclohexanol |
CN101945844B (zh) * | 2007-12-20 | 2013-09-18 | 帝斯曼知识产权资产管理有限公司 | 具有多次后蒸馏的环己酮生产方法 |
EP2234952A1 (en) | 2007-12-20 | 2010-10-06 | DSM IP Assets B.V. | Cyclohexanone production process with modified post-distillation |
EA017568B1 (ru) * | 2007-12-20 | 2013-01-30 | ДСМ АйПи АССЕТС Б.В. | Способ получения циклогексанона с удалением примесей |
CN104428276B (zh) | 2012-06-28 | 2017-03-08 | Cap Iii 有限公司 | 从苯酚生产包含环己酮和环己醇的混合物的方法 |
WO2014163080A1 (ja) * | 2013-04-05 | 2014-10-09 | 三井化学株式会社 | シクロヘキサノン化合物の製造方法 |
US20160368844A1 (en) | 2013-07-24 | 2016-12-22 | Exxonmobil Chemical Patents Inc. | Process for Producing Mixtures of Cyclohexanone and Cyclohexanol |
US10233140B2 (en) | 2014-09-30 | 2019-03-19 | Exxonmobil Chemical Patents Inc. | Process for making cyclohexanone |
-
2015
- 2015-11-06 ES ES15790590T patent/ES2803082T3/es active Active
- 2015-11-06 MX MX2017006073A patent/MX2017006073A/es unknown
- 2015-11-06 EA EA201791013A patent/EA031615B1/ru not_active IP Right Cessation
- 2015-11-06 UA UAA201705673A patent/UA122897C2/uk unknown
- 2015-11-06 KR KR1020177015774A patent/KR101820639B1/ko active IP Right Grant
- 2015-11-06 PL PL15790590T patent/PL3218338T3/pl unknown
- 2015-11-06 WO PCT/EP2015/075951 patent/WO2016075047A1/en active Application Filing
- 2015-11-06 US US15/525,448 patent/US10301243B2/en active Active
- 2015-11-06 CN CN201580060894.6A patent/CN107124881B/zh active Active
- 2015-11-06 EP EP15790590.2A patent/EP3218338B1/en active Active
- 2015-11-06 JP JP2017543886A patent/JP6249467B1/ja active Active
-
2017
- 2017-05-10 SA SA517381498A patent/SA517381498B1/ar unknown
Also Published As
Publication number | Publication date |
---|---|
ES2803082T3 (es) | 2021-01-22 |
EP3218338A1 (en) | 2017-09-20 |
US10301243B2 (en) | 2019-05-28 |
KR20170077249A (ko) | 2017-07-05 |
CN107124881A (zh) | 2017-09-01 |
UA122897C2 (uk) | 2021-01-20 |
WO2016075047A1 (en) | 2016-05-19 |
US20180290955A1 (en) | 2018-10-11 |
SA517381498B1 (ar) | 2020-09-03 |
JP2018501301A (ja) | 2018-01-18 |
JP6249467B1 (ja) | 2017-12-20 |
EP3218338B1 (en) | 2020-06-10 |
PL3218338T3 (pl) | 2020-09-21 |
CN107124881B (zh) | 2019-04-19 |
KR101820639B1 (ko) | 2018-01-19 |
EA201791013A1 (ru) | 2017-12-29 |
EA031615B1 (ru) | 2019-01-31 |
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