MX2013012674A - Proceso integrado para la produccion de 1 - cloro - 3, 3, 3 - trifluoropropeno. - Google Patents
Proceso integrado para la produccion de 1 - cloro - 3, 3, 3 - trifluoropropeno.Info
- Publication number
- MX2013012674A MX2013012674A MX2013012674A MX2013012674A MX2013012674A MX 2013012674 A MX2013012674 A MX 2013012674A MX 2013012674 A MX2013012674 A MX 2013012674A MX 2013012674 A MX2013012674 A MX 2013012674A MX 2013012674 A MX2013012674 A MX 2013012674A
- Authority
- MX
- Mexico
- Prior art keywords
- production
- chloro
- integrated process
- trifluoro propene
- distillations
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La presente invención está dirigida a procesos para la producción de 1233zd a partir de 240fa y HF, con o sin un catalizador, a escala comercial. El 240fa y HF son alimentados a un reactor que opera a alta presión. La corriente de producto resultante que comprende 1233zd, HCl, HF y otros sub-productos es tratada a una o más técnicas de purificación incluyendo separación de fases y una o más destilaciones para proveer 1233zd purificado, que cumple con las especificaciones del producto comercial, es decir, que tiene pureza de GC de 99.5% o mayor.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161487735P | 2011-05-19 | 2011-05-19 | |
US13/471,565 US9000240B2 (en) | 2011-05-19 | 2012-05-15 | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
PCT/US2012/038269 WO2012158872A2 (en) | 2011-05-19 | 2012-05-17 | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2013012674A true MX2013012674A (es) | 2013-12-02 |
Family
ID=47175419
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2013012674A MX2013012674A (es) | 2011-05-19 | 2012-05-17 | Proceso integrado para la produccion de 1 - cloro - 3, 3, 3 - trifluoropropeno. |
Country Status (8)
Country | Link |
---|---|
US (4) | US9000240B2 (es) |
EP (1) | EP2709970A4 (es) |
JP (1) | JP2014518873A (es) |
KR (1) | KR20140027404A (es) |
CN (1) | CN103827067A (es) |
CA (1) | CA2835948A1 (es) |
MX (1) | MX2013012674A (es) |
WO (1) | WO2012158872A2 (es) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9926244B2 (en) | 2008-10-28 | 2018-03-27 | Honeywell International Inc. | Process for drying HCFO-1233zd |
US9540296B2 (en) | 2015-03-19 | 2017-01-10 | Honeywell International Inc. | Process for drying HCFO-1233zd |
US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
US9000240B2 (en) | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
US8921621B2 (en) * | 2012-02-15 | 2014-12-30 | Honeywell International Inc. | Process for the production of HCFC-1233zd |
US8519200B1 (en) * | 2012-02-23 | 2013-08-27 | Honeywell International Inc. | Azeotropic compositions of 1,1,3,3-tetrachloro-1-fluoropropane and hydrogen fluoride |
US9018428B2 (en) | 2012-09-06 | 2015-04-28 | Honeywell International Inc. | Reactor and agitator useful in a process for making 1-chloro-3,3,3-trifluoropropene |
US9272968B2 (en) | 2013-03-14 | 2016-03-01 | Honeywell International Inc. | Process to suppress the formation of 3,3,3-trifluoropropyne in fluorocarbon manufacture |
US9272967B2 (en) * | 2013-10-15 | 2016-03-01 | Honeywell International Inc. | Process for producing 1-chloro-3,3,3-trifluoropropene in an ionic liquid |
CN104016305B (zh) * | 2014-05-26 | 2016-06-22 | 浙江衢化氟化学有限公司 | 一种从氢氟烃粗品中回收氟化氢的方法 |
JP2016023146A (ja) * | 2014-07-17 | 2016-02-08 | 旭硝子株式会社 | トリフルオロエチレンの精製方法 |
US20160332935A1 (en) * | 2015-05-12 | 2016-11-17 | Honeywell International Inc. | Integrated Process for Making HCFO-1233zd and HFC-245fa |
US9938213B2 (en) | 2015-08-19 | 2018-04-10 | Honeywell International Inc. | Methods for removing acidic impurities from halogenated propenes |
JP6826280B2 (ja) | 2016-01-15 | 2021-02-03 | セントラル硝子株式会社 | トランス−1−クロロ−3,3,3−トリフルオロプロペンの製造方法 |
US10029964B2 (en) | 2016-08-30 | 2018-07-24 | Honeywell International Inc. | Azeotropic or azeotrope-like compositions of 3,3,3-trifluoropropyne and water |
US9950974B2 (en) | 2016-08-31 | 2018-04-24 | Honeywell International Inc. | Azeotropic or azeotrope-like compositions of 1,3,3-trichloro-3-fluoro-1-ene (HCFO-1231zd) and hydrogen fluoride (HF) |
US9950973B2 (en) | 2016-08-31 | 2018-04-24 | Honeywell International Inc. | Azeotropic or azeotrope-like compositions of 1,3-dichloro-3,3-difluoroprop-1-ene (HCFO-1232zd) and hydrogen fluoride (HF) |
JP2020502085A (ja) * | 2016-12-21 | 2020-01-23 | アーケマ・インコーポレイテッド | R1233zdを精製された形で回収するための方法及びシステム |
CN107324968B (zh) * | 2017-07-24 | 2020-08-04 | 浙江衢化氟化学有限公司 | 一种联产低碳发泡剂的方法 |
US10035743B1 (en) | 2017-10-30 | 2018-07-31 | Honeywell International Inc. | Method for conversion of 1, 3, 3, 3-tetrafluoropropene (HFO-1234ze) to 1-chloro-3, 3, 3-trifluoropropene (HCFO-1233zd) |
FR3081158B1 (fr) * | 2018-05-16 | 2020-07-31 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene. |
Family Cites Families (30)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH09194404A (ja) * | 1996-01-17 | 1997-07-29 | Central Glass Co Ltd | 1−クロロ−3,3,3−トリフルオロプロペンの製造法 |
US6235951B1 (en) | 1996-01-17 | 2001-05-22 | Central Glass Company, Limited | Method for producing 1,1,1,3,3-pentafluoropropane |
FR2748473B1 (fr) * | 1996-05-13 | 1998-07-24 | Atochem Elf Sa | Synthese du 1-chloro-3,3,3 trifluoropropene et sa fluoration en 1,1,1,3,3 pentafluoropropane |
US5710352A (en) * | 1996-09-19 | 1998-01-20 | Alliedsignal Inc. | Vapor phase process for making 1,1,1,3,3-pentafluoropropane and 1-chloro-3,3,3-trifluoropropene |
US6023004A (en) * | 1996-11-12 | 2000-02-08 | Alliedsignal, Inc. | Liquid phase catalytic fluorination of hydrochlorocarbon and hydrochlorofluorocarbon |
US5877359A (en) * | 1998-01-27 | 1999-03-02 | Elf Atochem North America, Inc. | Uncatalyzed liquid phase fluorination of 1230ZA |
BE1011765A3 (fr) | 1998-02-26 | 2000-01-11 | Solvay | Procede d'hydrofluoration d'hydrocarbures. |
CN1178883C (zh) * | 1998-06-02 | 2004-12-08 | 纳幕尔杜邦公司 | 六氟丙烯和任选地其他含氟卤代碳氢化合物的制备方法 |
US6362382B1 (en) * | 2001-07-20 | 2002-03-26 | Atofina Chemicals, Inc. | Uncatalyzed fluorination of 240fa |
US7214839B2 (en) | 2003-05-23 | 2007-05-08 | Honeywell International Inc. | Method of making hydrofluorocarbons |
US7592494B2 (en) * | 2003-07-25 | 2009-09-22 | Honeywell International Inc. | Process for the manufacture of 1,3,3,3-tetrafluoropropene |
US6844475B1 (en) * | 2003-08-08 | 2005-01-18 | Honeywell International Business Machines | Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) |
FR2916755B1 (fr) * | 2007-05-31 | 2009-08-21 | Arkema France | Procede de preparation d'(hydro)(chloro)(fluoro)olefines |
WO2009114397A2 (en) | 2008-03-07 | 2009-09-17 | Arkema Inc. | Stable formulated systems with chloro-3,3,3-trifluoropropene |
US8168837B2 (en) | 2008-05-15 | 2012-05-01 | Honeywell International Inc. | Process for separating hydrogen fluoride from organic feedstocks |
JP5338240B2 (ja) * | 2008-10-06 | 2013-11-13 | セントラル硝子株式会社 | フッ化水素の分離方法 |
US7935268B2 (en) * | 2008-10-28 | 2011-05-03 | Honeywell International Inc. | Azeotrope-like compositions comprising trans-1-chloro-3,3,3-trifluoropropene |
US8163196B2 (en) * | 2008-10-28 | 2012-04-24 | Honeywell International Inc. | Azeotrope-like compositions comprising 1-chloro-3,3,3-trifluoropropene |
US8642819B2 (en) * | 2008-11-19 | 2014-02-04 | Arkema Inc. | Process for the manufacture of hydrochlorofluoroolefins |
US8075797B2 (en) | 2009-01-29 | 2011-12-13 | Honeywell International Inc. | Azeotrope-like compositions of pentafluoropropane, chlorotrifluoropropene, and hydrogen fluoride |
PL2411353T3 (pl) | 2009-03-24 | 2019-01-31 | Arkema Inc. | Oddzielanie R-1233 od fluorowodoru |
US7829748B1 (en) * | 2009-09-21 | 2010-11-09 | Honeywell International Inc. | Process for the manufacture of 1,3,3,3-tetrafluoropropene |
US8618340B2 (en) | 2009-11-03 | 2013-12-31 | Honeywell International Inc. | Integrated process for fluoro-olefin production |
US9045386B2 (en) | 2010-02-18 | 2015-06-02 | Honeywell International Inc. | Integrated process and methods of producing (E)-1-chloro-3,3,3-trifluoropropene |
WO2011135416A1 (en) | 2010-04-26 | 2011-11-03 | Arkema France | Process for the manufacture of 2-chloro-3, 3, 3-trifluoropropene (hcfo 1233xf) by liquid phase fluorination of pentachloropropane |
US8704017B2 (en) * | 2010-09-03 | 2014-04-22 | Honeywell International Inc. | Continuous low-temperature process to produce trans-1-chloro-3,3,3-trifluoropropene |
US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
US9000240B2 (en) | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
US8921621B2 (en) * | 2012-02-15 | 2014-12-30 | Honeywell International Inc. | Process for the production of HCFC-1233zd |
US9018428B2 (en) | 2012-09-06 | 2015-04-28 | Honeywell International Inc. | Reactor and agitator useful in a process for making 1-chloro-3,3,3-trifluoropropene |
-
2012
- 2012-05-15 US US13/471,565 patent/US9000240B2/en active Active
- 2012-05-17 KR KR1020137033149A patent/KR20140027404A/ko not_active Application Discontinuation
- 2012-05-17 EP EP12786229.0A patent/EP2709970A4/en not_active Withdrawn
- 2012-05-17 JP JP2014511516A patent/JP2014518873A/ja active Pending
- 2012-05-17 WO PCT/US2012/038269 patent/WO2012158872A2/en active Application Filing
- 2012-05-17 CN CN201280024023.5A patent/CN103827067A/zh active Pending
- 2012-05-17 MX MX2013012674A patent/MX2013012674A/es unknown
- 2012-05-17 CA CA2835948A patent/CA2835948A1/en not_active Abandoned
-
2015
- 2015-01-30 US US14/609,471 patent/US9682905B2/en active Active
- 2015-01-30 US US14/609,462 patent/US9227894B2/en active Active
- 2015-11-23 US US14/948,756 patent/US9556091B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
US9556091B2 (en) | 2017-01-31 |
KR20140027404A (ko) | 2014-03-06 |
US9682905B2 (en) | 2017-06-20 |
JP2014518873A (ja) | 2014-08-07 |
EP2709970A2 (en) | 2014-03-26 |
US20160083316A1 (en) | 2016-03-24 |
US20120296127A1 (en) | 2012-11-22 |
CN103827067A (zh) | 2014-05-28 |
US9227894B2 (en) | 2016-01-05 |
WO2012158872A3 (en) | 2013-05-02 |
US9000240B2 (en) | 2015-04-07 |
US20150148570A1 (en) | 2015-05-28 |
CA2835948A1 (en) | 2012-11-22 |
WO2012158872A2 (en) | 2012-11-22 |
EP2709970A4 (en) | 2014-10-29 |
US20150197468A1 (en) | 2015-07-16 |
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