MX337640B - Proceso para la produccion de hcfc-1233zd. - Google Patents
Proceso para la produccion de hcfc-1233zd.Info
- Publication number
- MX337640B MX337640B MX2014009815A MX2014009815A MX337640B MX 337640 B MX337640 B MX 337640B MX 2014009815 A MX2014009815 A MX 2014009815A MX 2014009815 A MX2014009815 A MX 2014009815A MX 337640 B MX337640 B MX 337640B
- Authority
- MX
- Mexico
- Prior art keywords
- reactor
- hcfc
- hcc
- scrubbed
- hcl
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Se describe un proceso para la fabricación de 1-cloro-3,3,3-trifluoropropeno (HCFC-1233zd) a escala comercial de la reacción de HCC-240 y HF. En una modalidad, el HCC-240fa y HF se alimentan a un reactor que funciona a alta presión. En este proceso se incluyen varios diseños de reactores diferentes útiles; un reactor de tanque agitado (lote y/o de flujo continuo); un reactor de flujo de pistón; un mezclador estático utilizado como un reactor; al menos uno de los reactores anteriores que funcionan a alta presión; opcionalmente se combina con una columna de destilación funciona a una presión más baja; y las combinaciones de los anteriores; y/o con una columna de destilación. La corriente de producto resultante que consiste en 1233zd, HCl, HF, y otros subproductos se condensan parcialmente para recuperar HF por separación de fases. La fase HF recuperada se recicla al reactor. El HCl se lava de la corriente de vapor y se recupera como una solución acuosa. Los componentes orgánicos restantes, incluyendo el HCFC-1233zd deseada se lavan, se secan y se destilan para cumplir con las especificaciones de productos comerciales.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261598938P | 2012-02-15 | 2012-02-15 | |
| US13/757,963 US8921621B2 (en) | 2012-02-15 | 2013-02-04 | Process for the production of HCFC-1233zd |
| PCT/US2013/025523 WO2013122860A1 (en) | 2012-02-15 | 2013-02-11 | PROCESS FOR THE PRODUCTION OF HCFC-1233zd |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2014009815A MX2014009815A (es) | 2014-09-25 |
| MX337640B true MX337640B (es) | 2016-03-14 |
Family
ID=48946152
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014009815A MX337640B (es) | 2012-02-15 | 2013-02-11 | Proceso para la produccion de hcfc-1233zd. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8921621B2 (es) |
| EP (2) | EP2814795B1 (es) |
| JP (1) | JP6220352B2 (es) |
| KR (1) | KR102050520B1 (es) |
| CN (2) | CN107827702A (es) |
| CA (1) | CA2863860C (es) |
| ES (1) | ES2869223T3 (es) |
| IN (1) | IN2014DN06601A (es) |
| MX (1) | MX337640B (es) |
| PL (1) | PL2814795T3 (es) |
| WO (1) | WO2013122860A1 (es) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9926244B2 (en) | 2008-10-28 | 2018-03-27 | Honeywell International Inc. | Process for drying HCFO-1233zd |
| US9540296B2 (en) * | 2015-03-19 | 2017-01-10 | Honeywell International Inc. | Process for drying HCFO-1233zd |
| US9000240B2 (en) | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
| US9272969B2 (en) * | 2013-03-13 | 2016-03-01 | Honeywell International Inc. | Azeotropic compositions of 1,3,3-trichloro-1,1-difluoropropane and hydrogen fluoride |
| US9272968B2 (en) * | 2013-03-14 | 2016-03-01 | Honeywell International Inc. | Process to suppress the formation of 3,3,3-trifluoropropyne in fluorocarbon manufacture |
| US9255045B2 (en) | 2014-01-13 | 2016-02-09 | Arkema France | E-1-chloro-3,3,3-trifluoropropene production process from 1,1,3,3-tetrachloropropene |
| CN110746266A (zh) | 2014-01-13 | 2020-02-04 | 阿科玛法国公司 | 从1,1,3,3-四氯丙烯生产e-1-氯-3,3,3-三氟丙烯的方法 |
| US9764998B2 (en) * | 2015-05-12 | 2017-09-19 | Honeywell International Inc. | Process for making HCFO-1233zd |
| FR3036398B1 (fr) | 2015-05-22 | 2019-05-03 | Arkema France | Compositions a base de 1,1,3,3-tetrachloropropene |
| JP6826280B2 (ja) * | 2016-01-15 | 2021-02-03 | セントラル硝子株式会社 | トランス−１−クロロ−３，３，３−トリフルオロプロペンの製造方法 |
| JP2020502085A (ja) * | 2016-12-21 | 2020-01-23 | アーケマ・インコーポレイテッド | Ｒ１２３３ｚｄを精製された形で回収するための方法及びシステム |
| US9994502B1 (en) | 2018-01-30 | 2018-06-12 | Honeywell International Inc. | Process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) |
| US10000431B1 (en) | 2018-01-30 | 2018-06-19 | Honeywell International Inc. | Process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) |
| US10717662B2 (en) | 2018-02-07 | 2020-07-21 | Honeywell International Inc. | Process for the removal of iron and phosphate ions from a chlorinated hydrocarbon waste stream |
| FR3081158B1 (fr) | 2018-05-16 | 2020-07-31 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene. |
| FR3083232B1 (fr) | 2018-06-27 | 2021-11-12 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene |
| FR3086287B1 (fr) | 2018-09-26 | 2020-09-18 | Arkema France | Stabilisation du 1-chloro-3,3,3-trifluoropropene |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3818398B2 (ja) | 1995-12-29 | 2006-09-06 | ダイキン工業株式会社 | １，１，１，３，３−ペンタフルオロプロパンの製造方法 |
| US6111150A (en) | 1996-06-20 | 2000-08-29 | Central Glass Company, Limited | Method for producing 1,1,1,3,3,-pentafluoropropane |
| US6023004A (en) | 1996-11-12 | 2000-02-08 | Alliedsignal, Inc. | Liquid phase catalytic fluorination of hydrochlorocarbon and hydrochlorofluorocarbon |
| BE1011765A3 (fr) | 1998-02-26 | 2000-01-11 | Solvay | Procede d'hydrofluoration d'hydrocarbures. |
| DE69937499T2 (de) | 1998-11-13 | 2008-08-21 | Daikin Industries, Ltd. | Azeotropes gemisch aus 1,1,1,3,3-pentafluorpropan und 1,1,1-trifluoro-3-chlor-2-propen, eine methode zur trennung und reinigung derselben und ein verfahren zur herstellung von1,1,1,3,3-pentafluorpropan und 1,1,1-trifluor-3-chlor-2-propen |
| US6844475B1 (en) * | 2003-08-08 | 2005-01-18 | Honeywell International Business Machines | Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) |
| US8067650B2 (en) * | 2006-08-24 | 2011-11-29 | Honeywell International Inc. | Process for the production of HFO trans-1234ze from HFC-245fa |
| BRPI0717091A2 (pt) * | 2006-10-03 | 2013-11-26 | Ineos Fluor Holdings Ltd | Processos para preparação de um composto e para isomerização de um composto, uso de um catalisador, fluido, mistura refrigerante, e, automóvel. |
| JP5416087B2 (ja) | 2007-03-29 | 2014-02-12 | アーケマ・インコーポレイテッド | ヒドロフルオロプロペンおよびヒドロクロロフルオロオレフィンの発泡剤組成物 |
| US8388857B2 (en) | 2007-06-27 | 2013-03-05 | Arkema Inc. | Stabilized hydrochlorofluoroolefins and hydrofluoroolefins |
| US8076521B2 (en) | 2007-06-27 | 2011-12-13 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
| US20090018377A1 (en) * | 2007-07-09 | 2009-01-15 | Boyce C Bradford | Catalytic process for the preparation of fluorinated halocarbons |
| WO2009048048A1 (ja) | 2007-10-10 | 2009-04-16 | Central Glass Company, Limited | トランス-１，３，３，３-テトラフルオロプロペンの製造方法 |
| US20110232306A1 (en) | 2008-04-30 | 2011-09-29 | Honeywell International Inc. | Absorption refrigeration cycles using a lgwp refrigerant |
| US9051231B2 (en) * | 2008-09-25 | 2015-06-09 | Central Glass Company, Limited | Process for producing 1,3,3,3-tetrafluoropropene |
| JP5515555B2 (ja) * | 2008-09-25 | 2014-06-11 | セントラル硝子株式会社 | １，３，３，３−テトラフルオロプロペンの製造方法 |
| US8642819B2 (en) | 2008-11-19 | 2014-02-04 | Arkema Inc. | Process for the manufacture of hydrochlorofluoroolefins |
| CN102216245B (zh) | 2008-11-19 | 2014-04-23 | 阿科玛股份有限公司 | 用于制造氢氟烯烃的方法 |
| PL2411353T3 (pl) * | 2009-03-24 | 2019-01-31 | Arkema Inc. | Oddzielanie R-1233 od fluorowodoru |
| US9045386B2 (en) | 2010-02-18 | 2015-06-02 | Honeywell International Inc. | Integrated process and methods of producing (E)-1-chloro-3,3,3-trifluoropropene |
| US8426656B2 (en) * | 2010-04-05 | 2013-04-23 | Honeywell International Inc. | Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene and trans-1,3,3,3-tetrafluoropropene |
| US20110269999A1 (en) | 2010-04-29 | 2011-11-03 | Honeywell International Inc. | Process for dehydrohalogenation of halogenated alkanes |
| US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
| US9000240B2 (en) * | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
-
2013
- 2013-02-04 US US13/757,963 patent/US8921621B2/en not_active Expired - Fee Related
- 2013-02-11 CN CN201711224589.3A patent/CN107827702A/zh active Pending
- 2013-02-11 ES ES13748643T patent/ES2869223T3/es active Active
- 2013-02-11 PL PL13748643T patent/PL2814795T3/pl unknown
- 2013-02-11 CA CA2863860A patent/CA2863860C/en active Active
- 2013-02-11 WO PCT/US2013/025523 patent/WO2013122860A1/en active Application Filing
- 2013-02-11 MX MX2014009815A patent/MX337640B/es active IP Right Grant
- 2013-02-11 EP EP13748643.7A patent/EP2814795B1/en active Active
- 2013-02-11 JP JP2014557705A patent/JP6220352B2/ja not_active Expired - Fee Related
- 2013-02-11 KR KR1020147025558A patent/KR102050520B1/ko active IP Right Grant
- 2013-02-11 IN IN6601DEN2014 patent/IN2014DN06601A/en unknown
- 2013-02-11 CN CN201380009478.4A patent/CN104105682A/zh active Pending
- 2013-02-11 EP EP21160560.5A patent/EP3858808A1/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US20130211154A1 (en) | 2013-08-15 |
| WO2013122860A1 (en) | 2013-08-22 |
| CA2863860A1 (en) | 2013-08-22 |
| ES2869223T3 (es) | 2021-10-25 |
| KR20140129165A (ko) | 2014-11-06 |
| KR102050520B1 (ko) | 2019-11-29 |
| EP3858808A1 (en) | 2021-08-04 |
| JP6220352B2 (ja) | 2017-10-25 |
| MX2014009815A (es) | 2014-09-25 |
| EP2814795A1 (en) | 2014-12-24 |
| US8921621B2 (en) | 2014-12-30 |
| PL2814795T3 (pl) | 2021-09-13 |
| CN104105682A (zh) | 2014-10-15 |
| EP2814795A4 (en) | 2015-09-30 |
| EP2814795B1 (en) | 2021-04-07 |
| CA2863860C (en) | 2020-09-22 |
| IN2014DN06601A (es) | 2015-05-22 |
| JP2015511946A (ja) | 2015-04-23 |
| CN107827702A (zh) | 2018-03-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |