MX337640B - Proceso para la produccion de hcfc-1233zd. - Google Patents
Proceso para la produccion de hcfc-1233zd.Info
- Publication number
- MX337640B MX337640B MX2014009815A MX2014009815A MX337640B MX 337640 B MX337640 B MX 337640B MX 2014009815 A MX2014009815 A MX 2014009815A MX 2014009815 A MX2014009815 A MX 2014009815A MX 337640 B MX337640 B MX 337640B
- Authority
- MX
- Mexico
- Prior art keywords
- reactor
- hcfc
- hcc
- scrubbed
- hcl
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Se describe un proceso para la fabricación de 1-cloro-3,3,3-trifluoropropeno (HCFC-1233zd) a escala comercial de la reacción de HCC-240 y HF. En una modalidad, el HCC-240fa y HF se alimentan a un reactor que funciona a alta presión. En este proceso se incluyen varios diseños de reactores diferentes útiles; un reactor de tanque agitado (lote y/o de flujo continuo); un reactor de flujo de pistón; un mezclador estático utilizado como un reactor; al menos uno de los reactores anteriores que funcionan a alta presión; opcionalmente se combina con una columna de destilación funciona a una presión más baja; y las combinaciones de los anteriores; y/o con una columna de destilación. La corriente de producto resultante que consiste en 1233zd, HCl, HF, y otros subproductos se condensan parcialmente para recuperar HF por separación de fases. La fase HF recuperada se recicla al reactor. El HCl se lava de la corriente de vapor y se recupera como una solución acuosa. Los componentes orgánicos restantes, incluyendo el HCFC-1233zd deseada se lavan, se secan y se destilan para cumplir con las especificaciones de productos comerciales.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261598938P | 2012-02-15 | 2012-02-15 | |
| US13/757,963 US8921621B2 (en) | 2012-02-15 | 2013-02-04 | Process for the production of HCFC-1233zd |
| PCT/US2013/025523 WO2013122860A1 (en) | 2012-02-15 | 2013-02-11 | PROCESS FOR THE PRODUCTION OF HCFC-1233zd |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2014009815A MX2014009815A (es) | 2014-09-25 |
| MX337640B true MX337640B (es) | 2016-03-14 |
Family
ID=48946152
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014009815A MX337640B (es) | 2012-02-15 | 2013-02-11 | Proceso para la produccion de hcfc-1233zd. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8921621B2 (es) |
| EP (2) | EP2814795B1 (es) |
| JP (1) | JP6220352B2 (es) |
| KR (1) | KR102050520B1 (es) |
| CN (2) | CN104105682A (es) |
| CA (1) | CA2863860C (es) |
| ES (1) | ES2869223T3 (es) |
| IN (1) | IN2014DN06601A (es) |
| MX (1) | MX337640B (es) |
| PL (1) | PL2814795T3 (es) |
| WO (1) | WO2013122860A1 (es) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9540296B2 (en) | 2015-03-19 | 2017-01-10 | Honeywell International Inc. | Process for drying HCFO-1233zd |
| US9926244B2 (en) | 2008-10-28 | 2018-03-27 | Honeywell International Inc. | Process for drying HCFO-1233zd |
| US9000240B2 (en) * | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
| US9272969B2 (en) * | 2013-03-13 | 2016-03-01 | Honeywell International Inc. | Azeotropic compositions of 1,3,3-trichloro-1,1-difluoropropane and hydrogen fluoride |
| US9272968B2 (en) * | 2013-03-14 | 2016-03-01 | Honeywell International Inc. | Process to suppress the formation of 3,3,3-trifluoropropyne in fluorocarbon manufacture |
| US9255045B2 (en) | 2014-01-13 | 2016-02-09 | Arkema France | E-1-chloro-3,3,3-trifluoropropene production process from 1,1,3,3-tetrachloropropene |
| JP6668254B2 (ja) | 2014-01-13 | 2020-03-18 | アルケマ フランス | １，１，３，３−テトラクロロプロペンからｅ−１−クロロ−３，３，３−トリフルオロプロペンを製造する方法 |
| US9764998B2 (en) * | 2015-05-12 | 2017-09-19 | Honeywell International Inc. | Process for making HCFO-1233zd |
| FR3036398B1 (fr) | 2015-05-22 | 2019-05-03 | Arkema France | Compositions a base de 1,1,3,3-tetrachloropropene |
| JP6826280B2 (ja) * | 2016-01-15 | 2021-02-03 | セントラル硝子株式会社 | トランス−１−クロロ−３，３，３−トリフルオロプロペンの製造方法 |
| JP2020502085A (ja) | 2016-12-21 | 2020-01-23 | アーケマ・インコーポレイテッド | Ｒ１２３３ｚｄを精製された形で回収するための方法及びシステム |
| US10000431B1 (en) | 2018-01-30 | 2018-06-19 | Honeywell International Inc. | Process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) |
| US9994502B1 (en) * | 2018-01-30 | 2018-06-12 | Honeywell International Inc. | Process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) |
| US10717662B2 (en) | 2018-02-07 | 2020-07-21 | Honeywell International Inc. | Process for the removal of iron and phosphate ions from a chlorinated hydrocarbon waste stream |
| FR3081158B1 (fr) | 2018-05-16 | 2020-07-31 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene. |
| FR3083232B1 (fr) | 2018-06-27 | 2021-11-12 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene |
| FR3086287B1 (fr) | 2018-09-26 | 2020-09-18 | Arkema France | Stabilisation du 1-chloro-3,3,3-trifluoropropene |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3818398B2 (ja) | 1995-12-29 | 2006-09-06 | ダイキン工業株式会社 | １，１，１，３，３−ペンタフルオロプロパンの製造方法 |
| US6111150A (en) | 1996-06-20 | 2000-08-29 | Central Glass Company, Limited | Method for producing 1,1,1,3,3,-pentafluoropropane |
| US6023004A (en) | 1996-11-12 | 2000-02-08 | Alliedsignal, Inc. | Liquid phase catalytic fluorination of hydrochlorocarbon and hydrochlorofluorocarbon |
| BE1011765A3 (fr) | 1998-02-26 | 2000-01-11 | Solvay | Procede d'hydrofluoration d'hydrocarbures. |
| WO2000029361A1 (en) | 1998-11-13 | 2000-05-25 | Daikin Industries, Ltd. | Azeotropic composition comprising 1,1,1,3,3-pentafluoropropane and 1,1,1-trifluoro-3-chloro-2-propene, method of separation and purification of the same, and process for producing 1,1,1,3,3-pentafluoropropane and 1,1,1-trifluoro-3-chloro-2-propene |
| US6844475B1 (en) * | 2003-08-08 | 2005-01-18 | Honeywell International Business Machines | Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) |
| US8067650B2 (en) * | 2006-08-24 | 2011-11-29 | Honeywell International Inc. | Process for the production of HFO trans-1234ze from HFC-245fa |
| WO2008040969A2 (en) * | 2006-10-03 | 2008-04-10 | Ineos Fluor Holdings Limited | Dehydrogenationhalogenation process for the production of c3-c6-(hydro)fluoroalkenes |
| US9279039B2 (en) | 2007-03-29 | 2016-03-08 | Arkema Inc. | Blowing agent composition of hydrochlorofluoroolefin and hydrofluoroolefin |
| JP5337799B2 (ja) | 2007-06-27 | 2013-11-06 | アーケマ・インコーポレイテッド | ヒドロフルオロオレフィンの製造方法 |
| US8388857B2 (en) | 2007-06-27 | 2013-03-05 | Arkema Inc. | Stabilized hydrochlorofluoroolefins and hydrofluoroolefins |
| US20090018377A1 (en) * | 2007-07-09 | 2009-01-15 | Boyce C Bradford | Catalytic process for the preparation of fluorinated halocarbons |
| US8513473B2 (en) | 2007-10-10 | 2013-08-20 | Central Glass Company, Limited | Method for producing trans-1,3,3,3-tetrafluoropropene |
| US20110232306A1 (en) | 2008-04-30 | 2011-09-29 | Honeywell International Inc. | Absorption refrigeration cycles using a lgwp refrigerant |
| EP2341040B1 (en) * | 2008-09-25 | 2017-09-06 | Central Glass Company, Limited | Process for producing 1,3,3,3-tetrafluoropropene |
| JP5515555B2 (ja) * | 2008-09-25 | 2014-06-11 | セントラル硝子株式会社 | １，３，３，３−テトラフルオロプロペンの製造方法 |
| CA2743670C (en) | 2008-11-19 | 2016-04-12 | Arkema Inc. | Process for the manufacture of hydrochlorofluoroolefins |
| WO2010059493A1 (en) * | 2008-11-19 | 2010-05-27 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
| PL2411353T3 (pl) * | 2009-03-24 | 2019-01-31 | Arkema Inc. | Oddzielanie R-1233 od fluorowodoru |
| US9045386B2 (en) * | 2010-02-18 | 2015-06-02 | Honeywell International Inc. | Integrated process and methods of producing (E)-1-chloro-3,3,3-trifluoropropene |
| US8426656B2 (en) * | 2010-04-05 | 2013-04-23 | Honeywell International Inc. | Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene and trans-1,3,3,3-tetrafluoropropene |
| US20110269999A1 (en) | 2010-04-29 | 2011-11-03 | Honeywell International Inc. | Process for dehydrohalogenation of halogenated alkanes |
| US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
| US9000240B2 (en) * | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
-
2013
- 2013-02-04 US US13/757,963 patent/US8921621B2/en not_active Expired - Fee Related
- 2013-02-11 JP JP2014557705A patent/JP6220352B2/ja not_active Expired - Fee Related
- 2013-02-11 CN CN201380009478.4A patent/CN104105682A/zh active Pending
- 2013-02-11 IN IN6601DEN2014 patent/IN2014DN06601A/en unknown
- 2013-02-11 KR KR1020147025558A patent/KR102050520B1/ko active IP Right Grant
- 2013-02-11 ES ES13748643T patent/ES2869223T3/es active Active
- 2013-02-11 WO PCT/US2013/025523 patent/WO2013122860A1/en active Application Filing
- 2013-02-11 EP EP13748643.7A patent/EP2814795B1/en active Active
- 2013-02-11 MX MX2014009815A patent/MX337640B/es active IP Right Grant
- 2013-02-11 EP EP21160560.5A patent/EP3858808A1/en active Pending
- 2013-02-11 PL PL13748643T patent/PL2814795T3/pl unknown
- 2013-02-11 CA CA2863860A patent/CA2863860C/en active Active
- 2013-02-11 CN CN201711224589.3A patent/CN107827702A/zh active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| KR20140129165A (ko) | 2014-11-06 |
| CA2863860A1 (en) | 2013-08-22 |
| EP2814795A4 (en) | 2015-09-30 |
| CN104105682A (zh) | 2014-10-15 |
| WO2013122860A1 (en) | 2013-08-22 |
| CN107827702A (zh) | 2018-03-23 |
| JP2015511946A (ja) | 2015-04-23 |
| EP3858808A1 (en) | 2021-08-04 |
| ES2869223T3 (es) | 2021-10-25 |
| IN2014DN06601A (es) | 2015-05-22 |
| US20130211154A1 (en) | 2013-08-15 |
| US8921621B2 (en) | 2014-12-30 |
| CA2863860C (en) | 2020-09-22 |
| EP2814795A1 (en) | 2014-12-24 |
| MX2014009815A (es) | 2014-09-25 |
| EP2814795B1 (en) | 2021-04-07 |
| PL2814795T3 (pl) | 2021-09-13 |
| KR102050520B1 (ko) | 2019-11-29 |
| JP6220352B2 (ja) | 2017-10-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |