MX2008010941A - Sistema de produccion de acido policarboxilico que emplea remocion de licor caliente corriente abajo de la digestion oxidante. - Google Patents

Sistema de produccion de acido policarboxilico que emplea remocion de licor caliente corriente abajo de la digestion oxidante.

Info

Publication number
MX2008010941A
MX2008010941A MX2008010941A MX2008010941A MX2008010941A MX 2008010941 A MX2008010941 A MX 2008010941A MX 2008010941 A MX2008010941 A MX 2008010941A MX 2008010941 A MX2008010941 A MX 2008010941A MX 2008010941 A MX2008010941 A MX 2008010941A
Authority
MX
Mexico
Prior art keywords
production system
polycarboxylic acid
acid production
system employing
oxidative digestion
Prior art date
Application number
MX2008010941A
Other languages
English (en)
Inventor
Ronald Buford Sheppard
Martin De Boer
Alan George Wonders
Original Assignee
Eastman Chem Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eastman Chem Co filed Critical Eastman Chem Co
Publication of MX2008010941A publication Critical patent/MX2008010941A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Se divulga un sistema optimizado para producir ácido tereftálico más eficiente y económicamente. El sistema incluye una etapa de enfriamiento de post-digestión optimizada que proporciona un producto de TPA que tiene pureza aumentada, mientras que minimiza los costos asociados con la remoción de impurezas del solvente reciclado.
MX2008010941A 2006-03-01 2007-02-27 Sistema de produccion de acido policarboxilico que emplea remocion de licor caliente corriente abajo de la digestion oxidante. MX2008010941A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/365,258 US7420082B2 (en) 2006-03-01 2006-03-01 Polycarboxylic acid production system employing hot liquor removal downstream of oxidative digestion
PCT/US2007/004938 WO2007103028A2 (en) 2006-03-01 2007-02-27 Polycarboxylic acid production system employing hot liquor removal downstream of oxidative digestion

Publications (1)

Publication Number Publication Date
MX2008010941A true MX2008010941A (es) 2008-09-03

Family

ID=38331532

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2008010941A MX2008010941A (es) 2006-03-01 2007-02-27 Sistema de produccion de acido policarboxilico que emplea remocion de licor caliente corriente abajo de la digestion oxidante.

Country Status (7)

Country Link
US (1) US7420082B2 (es)
EP (1) EP1993987A2 (es)
CN (2) CN104892391A (es)
BR (1) BRPI0708394A2 (es)
MX (1) MX2008010941A (es)
TW (1) TW200736210A (es)
WO (1) WO2007103028A2 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
WO2017014264A1 (ja) * 2015-07-22 2017-01-26 三菱瓦斯化学株式会社 高純度テレフタル酸の製造方法
CN106167451B (zh) * 2016-07-25 2018-12-18 浙江大学 间二甲苯与乙苯多步共氧化生产芳香羧酸的方法
CN106220489B (zh) * 2016-07-25 2018-12-18 浙江大学 以对二甲苯抽余液为原料生产间苯二甲酸的方法
US10000435B1 (en) * 2017-02-28 2018-06-19 Grupo Petrotemex, S.A. De C.V. Energy and environmentally integrated method for production of aromatic dicarboxylic acids by oxidation
CN108003006A (zh) * 2017-11-17 2018-05-08 杭州多向流化学科技有限公司 一种以碳八芳烃为原料生产对苯二甲酸与间苯二甲酸的方法

Family Cites Families (92)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3064044A (en) 1957-08-15 1962-11-13 Standard Oil Co Multistage oxidation system for preparing dicarboxylic acid
NL276649A (es) 1960-10-12
GB983677A (en) 1962-04-27 1965-02-17 Mitsui Petrochemical Ind A process for the preparation of terephthalic acid having extremely high purity
GB1152575A (en) 1965-05-17 1969-05-21 Standard Oil Co Purification of Aromatic Polycarboxylic Acids.
NL6606774A (es) 1965-05-17 1966-11-18
US3584039A (en) 1967-08-30 1971-06-08 Standard Oil Co Fiber-grade terephthalic acid by catalytic hydrogen treatment of dissolved impure terephthalic acid
FR2006269A1 (es) * 1968-04-16 1969-12-26 Celanese Corp
US3626001A (en) * 1968-05-09 1971-12-07 Atlantic Richfield Co Method for the production of high-purity isophthalic or terephthalic acid
DE1927937A1 (de) * 1969-05-31 1970-12-17 Dynamit Nobel Ag Verfahren zur Herstellung von Benzoldicarbonsaeuren bzw. Benzoldicarbonsaeureestern
JPS5414098B1 (es) * 1970-12-25 1979-06-05
GB1358520A (en) 1972-06-05 1974-07-03 Crampton K J A Oxidation of aromatic organic compounds
JPS5328421B2 (es) 1973-05-15 1978-08-15
US3931305A (en) 1973-08-20 1976-01-06 Standard Oil Company Terephthalic acid recovery by continuous flash crystallization
US3850983A (en) 1973-10-15 1974-11-26 Standard Oil Co Separation of terephthalic from paratoluic acid from solutions thereof in water and/or acetic acid
JPS5614101B2 (es) 1974-07-31 1981-04-02
JPS5936230B2 (ja) 1975-06-03 1984-09-03 株式会社光電製作所 過電圧表示回路
PL102150B1 (pl) 1976-07-29 1979-03-31 Inst Ciezkiej Syntezy Orga A method oxidizing p-xylene and methyl p-toluylate
JPS5949212B2 (ja) 1976-09-16 1984-12-01 三菱化学株式会社 テレフタル酸の製造法
US4158738A (en) 1977-05-26 1979-06-19 E. I. Du Pont De Nemours And Company Process for the production of fiber-grade terephthalic acid
JPS5425292A (en) 1977-07-28 1979-02-26 Mitsubishi Chem Ind Ltd Method of recovering liquid phase oxidation catalyst of terephthalic acid
JPS5555138A (en) 1978-10-19 1980-04-22 Mitsubishi Chem Ind Ltd Preparation of highly pure terephthalic acid
IT1129759B (it) * 1980-01-23 1986-06-11 Montedison Spa Metodo per ricuperare in forma attiva i componenti del sistema catalitico della sintesi dell'acido tereftalico
JPS57188543A (en) 1981-05-13 1982-11-19 Mitsubishi Chem Ind Ltd Preparation of terephthalic acid
JPS59104345A (ja) 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
JPS59106435A (ja) 1982-12-10 1984-06-20 Mitsubishi Chem Ind Ltd 高純度テレフタル酸の製法
EP0121438A1 (en) 1983-03-31 1984-10-10 Vickers Plc Flexible manufacturing system and method
US4500732A (en) 1983-09-15 1985-02-19 Standard Oil Company (Indiana) Process for removal and recycle of p-toluic acid from terephthalic acid crystallizer solvent
US4898717A (en) * 1984-01-04 1990-02-06 Mobil Oil Corp. Multistage process for converting oxygenates to distillate hydrocarbons with interstage ethene recovery
US4892970A (en) 1985-12-30 1990-01-09 Amoco Corporation Staged aromatics oxidation in aqueous systems
US4719247A (en) * 1987-02-10 1988-01-12 Ici Americas Inc. Deformable polyurethane having improved cure time
JP2504461B2 (ja) 1987-04-24 1996-06-05 三菱化学株式会社 高品質テレフタル酸の製法
US4939297A (en) * 1989-06-05 1990-07-03 Eastman Kodak Company Extraction process for removal of impurities from terephthalic acid filtrate
US5095145A (en) * 1990-11-05 1992-03-10 Amoco Corporation Preparation of purified terephthalic acid from waste polyethylene terephthalate
US5095146A (en) 1991-03-25 1992-03-10 Amoco Corporation Water addition to crystallization train to purify terephthalic acid product
US5175355A (en) 1991-04-12 1992-12-29 Amoco Corporation Improved process for recovery of purified terephthalic acid
JP2557578B2 (ja) 1991-07-12 1996-11-27 三菱化学株式会社 パラキシレンの液相酸化触媒の回収方法
GB9310070D0 (en) 1992-05-29 1993-06-30 Ici Plc Process for the production of purified terephthalic acid
KR970000136B1 (ko) * 1993-09-28 1997-01-04 브이.피. 유리예프 고순도 벤젠디카르복실산 이성질체의 제조방법
US5567842A (en) 1994-11-16 1996-10-22 Mitsubishi Chemical Corporation Process for producing terephthalic acid
US5510521A (en) 1995-03-27 1996-04-23 Eastman Chemical Company Process for the production of aromatic carboxylic acids
JPH09157214A (ja) 1995-10-05 1997-06-17 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
US5756833A (en) 1996-02-01 1998-05-26 Amoco Corporation Catalytic purification and recovery of dicarboxylic aromatic acids
ID15851A (id) * 1996-02-13 1997-08-14 Mitsubishi Chem Corp Proses untuk menghasilkan suatu asam aromatik karboksilik
AU3858497A (en) 1996-08-29 1998-03-19 E.I. Du Pont De Nemours And Company Catalyst recovery
ID19133A (id) * 1996-12-12 1998-06-18 Praxair Technology Inc Pengisian oksigen langsung kedalam reaktor-reaktor ruang gelembung
US5821270A (en) * 1997-05-02 1998-10-13 Exxon Research And Engineering Company Slurry hydrocarbon synthesis process with multistage catalyst rejuvenation
HUP0100656A3 (en) 1997-12-15 2002-03-28 Shell Int Research Method for produce aromatic carboxylic acids
US6137001A (en) * 1998-02-11 2000-10-24 Bp Amoco Corporation Process for preparing aromatic carboxylic acids with efficient treatments of gaseous effluent
JPH11343264A (ja) 1998-05-28 1999-12-14 Mitsubishi Chemical Corp 芳香族カルボン酸の製造方法
US6392091B2 (en) * 1998-11-24 2002-05-21 Tsong-Dar Vincent Lin Process of purifying and producing high purity aromatic polycarboxylic acids
US6297348B1 (en) 1999-08-30 2001-10-02 Shell Oil Company Closely linking a NDA process with a pen process
WO2001038279A1 (en) * 1999-11-26 2001-05-31 Chemintel (India) Private Limited Process for preparation of benzene dicarboxylic acids
US6949673B2 (en) * 2000-01-12 2005-09-27 E.I. Du Pont De Nemours And Company Process for producing carboxylic acids
JP2003520263A (ja) * 2000-01-21 2003-07-02 ビーピー・コーポレーション・ノース・アメリカ・インコーポレーテッド 安息香酸・水溶剤中での酸化による高純度芳香族カルボン酸の製造
JP2001288139A (ja) 2000-02-04 2001-10-16 Mitsubishi Chemicals Corp 高純度テレフタル酸の製造方法
JP2001247511A (ja) 2000-03-07 2001-09-11 Mitsubishi Chemicals Corp 芳香族カルボン酸の製造方法
US6679951B2 (en) * 2000-05-15 2004-01-20 Asm Intenational N.V. Metal anneal with oxidation prevention
US6765113B2 (en) * 2000-07-19 2004-07-20 E.I. Du Pont De Nemours And Company Production of aromatic carboxylic acids
US6436720B1 (en) * 2000-09-15 2002-08-20 Cellular Process Chemistry, Inc. Residence time providing module/apparatus
US7196215B2 (en) * 2001-06-04 2007-03-27 Eastman Chemical Company Process for the production of purified terephthalic acid
US7485747B2 (en) * 2001-06-04 2009-02-03 Eastman Chemical Company Two stage oxidation process for the production of aromatic dicarboxylic acids
US6504051B1 (en) * 2001-06-04 2003-01-07 Eastman Chemical Company Process for production of aromatic carboxylic acids with improved water removal technique
US6689903B2 (en) 2001-06-04 2004-02-10 Eastman Chemical Company Crystallization method for production of purified aromatic dicarboxylic acids
AU2003280809A1 (en) * 2002-11-14 2004-06-03 Mitsubishi Chemical Corporation Process for producing terephthalic acid
JP2004168716A (ja) 2002-11-20 2004-06-17 Mitsubishi Chemicals Corp テレフタル酸の製造方法
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7132566B2 (en) * 2003-09-22 2006-11-07 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry
JP2006509044A (ja) 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法
US7161027B2 (en) * 2002-12-09 2007-01-09 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US20040215036A1 (en) * 2003-04-25 2004-10-28 Robert Lin Method for heating a crude carboxylic acid slurry in a post oxidation zone by the addition of steam
US7153480B2 (en) * 2003-05-22 2006-12-26 David Robert Bickham Apparatus for and method of producing aromatic carboxylic acids
US6800664B1 (en) * 2003-05-23 2004-10-05 Conocophillips Company Conjoined reactor system
US7410632B2 (en) * 2003-06-05 2008-08-12 Eastman Chemical Company Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid
US7494641B2 (en) * 2003-06-05 2009-02-24 Eastman Chemical Company Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid
US7282151B2 (en) * 2003-06-05 2007-10-16 Eastman Chemical Company Process for removal of impurities from mother liquor in the synthesis of carboxylic acid using pressure filtration
US7452522B2 (en) * 2003-06-05 2008-11-18 Eastman Chemical Company Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid
US7547803B2 (en) * 2003-06-20 2009-06-16 Mitsubishi Gas Chemical Company, Inc. Process for producing a high purity aromatic polycarboxylic acid
KR100575192B1 (ko) 2003-11-19 2006-04-28 메탈화학(주) 테레프탈산(tpa) 폐촉매로부터 코발트 망간 회수 방법
US7546747B2 (en) * 2004-01-15 2009-06-16 Eastman Chemical Company Process for production of a dried carboxylic acid cake suitable for use in polyester production
CN1914145B (zh) 2004-02-05 2010-12-08 三菱化学株式会社 芳香族羧酸的制造方法
US7348452B2 (en) * 2004-04-22 2008-03-25 Eastman Chemical Company Liquid phase oxidation of P-xylene to terephthalic acid in the presence of a catalyst system containing nickel, manganese, and bromine atoms
US20050283022A1 (en) * 2004-06-18 2005-12-22 Sheppard Ronald B Filtrate preparation process for terephthalic acid filtrate treatment
US7504535B2 (en) * 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7910769B2 (en) * 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7692037B2 (en) * 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7572936B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) * 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US7381836B2 (en) * 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7589231B2 (en) * 2004-09-02 2009-09-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7741515B2 (en) * 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7572932B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7371894B2 (en) * 2004-09-02 2008-05-13 Eastman Chemical Company Optimized liquid-phase oxidation

Also Published As

Publication number Publication date
US20070208192A1 (en) 2007-09-06
CN101395117A (zh) 2009-03-25
CN104892391A (zh) 2015-09-09
US7420082B2 (en) 2008-09-02
EP1993987A2 (en) 2008-11-26
WO2007103028A3 (en) 2007-11-01
BRPI0708394A2 (pt) 2011-05-31
TW200736210A (en) 2007-10-01
WO2007103028A2 (en) 2007-09-13

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