LTIP575A - 5-dichloracetil-3,3,6-trimetil-9-okso-i,5-diazabiciklo [4,3,0] nonano gavimo būdas - Google Patents

5-dichloracetil-3,3,6-trimetil-9-okso-i,5-diazabiciklo [4,3,0] nonano gavimo būdas

Info

Publication number
LTIP575A
LTIP575A LTIP575A LTIP575A LTIP575A LT IP575 A LTIP575 A LT IP575A LT IP575 A LTIP575 A LT IP575A LT IP575 A LTIP575 A LT IP575A LT IP575 A LTIP575 A LT IP575A
Authority
LT
Lithuania
Prior art keywords
nonane
trimethyl
oxo
dichloroacetyl
diazabicyclo
Prior art date
Application number
LTIP575A
Other languages
English (en)
Inventor
Gernot Reissenweber
Winfried Richarz
Knut Koob
Original Assignee
Basf Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Aktiengesellschaft filed Critical Basf Aktiengesellschaft
Publication of LTIP575A publication Critical patent/LTIP575A/lt
Publication of LT3016B publication Critical patent/LT3016B/lt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
    • C07D487/04—Ortho-condensed systems

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Cephalosporin Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)

Abstract

5-Dichloracetil-3,3,6-trimetil-9-okso-1,5-diabiciklo-[4,3,0]nonano gavimas veikiant 3,3,6-trimetil-9-okso-1,5-diabiciklo-[4,3,0]nonaną dichloracetilchloridu, esant tirpikliui ir bazei, pasižymintis tuo, kad@a) ši reakcija vyksta dvifazėje sistemoje, sudarytoje iš praktiškai netirpaus vandenyje organinio tirpiklio ir vandens, o natrio arba kalio šarmas kaip bazė dozuojamas pagal dichloracetilchlorido sunaudojimą tokiu būdu, kad vandeninės fazės pH būtų nuo 7 iki 9, ir@b) susidarantį kietą produktą atskiria.
LTIP575A 1992-05-29 1993-05-28 5-dichloracetil-3,3,6-trimetil-9-okso-i,5-diazabiciklo £4,3,0| nonano gavimo budas LT3016B (lt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4217846A DE4217846C1 (de) 1992-05-29 1992-05-29 Verfahren zur Herstellung von 5-Dichloracetyl-3,3,6-trimethyl-9-oxo-1,5-diazabicyclo[4,3,0]nonan

Publications (2)

Publication Number Publication Date
LTIP575A true LTIP575A (lt) 1994-04-25
LT3016B LT3016B (lt) 1994-08-25

Family

ID=6460024

Family Applications (1)

Application Number Title Priority Date Filing Date
LTIP575A LT3016B (lt) 1992-05-29 1993-05-28 5-dichloracetil-3,3,6-trimetil-9-okso-i,5-diazabiciklo £4,3,0| nonano gavimo budas

Country Status (15)

Country Link
US (1) US5677452A (lt)
EP (1) EP0642511B1 (lt)
AT (1) ATE142210T1 (lt)
AU (1) AU4313293A (lt)
CA (1) CA2136872C (lt)
CZ (1) CZ276094A3 (lt)
DE (2) DE4217846C1 (lt)
ES (1) ES2091007T3 (lt)
HU (1) HU213833B (lt)
LT (1) LT3016B (lt)
LV (1) LV11036B (lt)
PL (1) PL173088B1 (lt)
RU (1) RU94046203A (lt)
SK (1) SK142894A3 (lt)
WO (1) WO1993024489A1 (lt)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6476046B1 (en) 2000-12-04 2002-11-05 Sepracor, Inc. Diazabicyclo[4.3.0]nonanes, and methods of use thereof

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1802468A1 (de) 1968-10-11 1970-05-21 Bayer Ag Diazabicycloalkane
DE2948535A1 (de) * 1979-12-03 1981-06-25 Basf Ag, 6700 Ludwigshafen Dichloracetamide, herbizide mittel, die acetanilide als herbizide wirkstoffe und diese dichloracetamide als antagonistische mittel enthalten, sowie ihre verwendung zur bekaempfung unerwuenschten pflanzenwuchses
EP0190105A3 (de) * 1985-01-31 1988-10-26 Ciba-Geigy Ag Herbizides Mittel
US4995899A (en) * 1986-01-15 1991-02-26 Basf Aktiengesellschaft Optically active diazabicycloalkane derivatives and their use for protecting crops from the phytotoxic effect of herbicides
DE3600903A1 (de) * 1986-01-15 1987-07-16 Basf Ag Optisch aktive diazabicycloalkanderivate, ein verfahren zu ihrer herstellung und ihre verwendung zum schutz von kulturpflanzen vor der phytotoxischen wirkung von herbiziden
GB8916395D0 (en) * 1989-07-18 1989-09-06 Zambeletti Spa L Pharmaceuticals

Also Published As

Publication number Publication date
PL173088B1 (pl) 1998-01-30
ES2091007T3 (es) 1996-10-16
ATE142210T1 (de) 1996-09-15
EP0642511B1 (de) 1996-09-04
LV11036B (en) 1996-06-20
SK142894A3 (en) 1995-06-07
LT3016B (lt) 1994-08-25
HU9403409D0 (en) 1995-03-28
EP0642511A1 (de) 1995-03-15
LV11036A (lv) 1996-02-20
DE59303673D1 (de) 1996-10-10
WO1993024489A1 (de) 1993-12-09
HU213833B (en) 1997-10-28
DE4217846C1 (de) 1993-12-23
CA2136872C (en) 2004-01-20
RU94046203A (ru) 1996-09-27
CA2136872A1 (en) 1993-05-18
CZ276094A3 (en) 1995-02-15
AU4313293A (en) 1993-12-30
US5677452A (en) 1997-10-14
HUT69060A (en) 1995-08-28

Similar Documents

Publication Publication Date Title
IE40651B1 (en) Triazolopyaridazines
CA2002430A1 (en) Method for the resolution of folinic acid
EP0142811A3 (en) Method of preparing 1,2,4-triazolo [1,5-a] - pyrimidine-2-sulfonyl chlorides
CA2072283A1 (en) Process for the preparation of diacetylrhein
GB1377313A (en) Process for purifying phenylalanine derivatives
DE59602236D1 (de) Verfahren zur Herstellung von Ascorbinsäure
LTIP575A (lt) 5-dichloracetil-3,3,6-trimetil-9-okso-i,5-diazabiciklo [4,3,0] nonano gavimo būdas
IE843217L (en) Antibiotic l 17392
WO2003010172A1 (en) Process for producing highly pure riboflavin-5’-phosphate sodium
ZA952805B (en) Stable aqueous folinate solution
TW427991B (en) Production of pharmaceutically acceptable salts of clavulanic acid
JPS5416452A (en) Preparation of dis(amnomethyl) cyclohexane
AU7761587A (en) Process
IE820844L (en) Production of sodium amoxicillin by spray-drying
IE822017L (en) N-methyl-d-glucamine salt
EP0646586A4 (lt)
JPS57145858A (en) Preparation of aziridine-2-carboxylic acid salt
JPS56150049A (en) Production of d-2-amino-2- 1,4-cyclohexadienyl acetic acid
JPS5653685A (en) Production of cephalosporin derivative
JPS53119822A (en) Preparation of 2-dimethylaminoethylisothiocyanate
SU1295715A1 (ru) Способ получения ампициллина или цефалексина
JPS5551088A (en) Pyrrolopyrimidine derivative
JPS51149222A (en) Preparation of highly purified leucine
JPS53144587A (en) Purification of aminopyrazinecarboxylic acid
JPS5524102A (en) Preparation of trichloroisocyanuric acid

Legal Events

Date Code Title Description
MM9A Lapsed patents

Effective date: 19990528