LT4340B - Granuliuoto karbamido paruošimo būdas - Google Patents
Granuliuoto karbamido paruošimo būdas Download PDFInfo
- Publication number
- LT4340B LT4340B LT97-156A LT97156A LT4340B LT 4340 B LT4340 B LT 4340B LT 97156 A LT97156 A LT 97156A LT 4340 B LT4340 B LT 4340B
- Authority
- LT
- Lithuania
- Prior art keywords
- urea
- solution
- formaldehyde
- urea solution
- aqueous
- Prior art date
Links
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title claims abstract description 126
- 239000004202 carbamide Substances 0.000 title claims abstract description 125
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 9
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 157
- 239000000243 solution Substances 0.000 claims abstract description 66
- 238000000034 method Methods 0.000 claims abstract description 16
- 239000008098 formaldehyde solution Substances 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims description 10
- 239000007864 aqueous solution Substances 0.000 claims description 9
- 238000005469 granulation Methods 0.000 abstract description 24
- 230000003179 granulation Effects 0.000 abstract description 24
- 239000011259 mixed solution Substances 0.000 abstract description 15
- 239000007788 liquid Substances 0.000 abstract description 5
- 239000008187 granular material Substances 0.000 description 15
- 238000006243 chemical reaction Methods 0.000 description 14
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 229920000642 polymer Polymers 0.000 description 9
- 229910021529 ammonia Inorganic materials 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 6
- 238000006116 polymerization reaction Methods 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 5
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 3
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- OHJMTUPIZMNBFR-UHFFFAOYSA-N biuret Chemical compound NC(=O)NC(N)=O OHJMTUPIZMNBFR-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 230000015271 coagulation Effects 0.000 description 2
- 238000005345 coagulation Methods 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- CUHVTYCUTYWQOR-UHFFFAOYSA-N formaldehyde Chemical compound O=C.O=C CUHVTYCUTYWQOR-UHFFFAOYSA-N 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
- B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
- C05C9/005—Post-treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/14—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Glanulating (AREA)
- Fertilizers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP01654196A JP3667418B2 (ja) | 1996-02-01 | 1996-02-01 | 粒状尿素の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| LT97156A LT97156A (en) | 1998-02-25 |
| LT4340B true LT4340B (lt) | 1998-05-25 |
Family
ID=11919135
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| LT97-156A LT4340B (lt) | 1996-02-01 | 1997-09-30 | Granuliuoto karbamido paruošimo būdas |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US5965071A (id) |
| EP (1) | EP0819106B1 (id) |
| JP (1) | JP3667418B2 (id) |
| CN (1) | CN1098234C (id) |
| AR (1) | AR005588A1 (id) |
| AU (1) | AU705068B2 (id) |
| BR (1) | BR9702047A (id) |
| CA (1) | CA2215596C (id) |
| DE (1) | DE69716177T2 (id) |
| ES (1) | ES2182019T3 (id) |
| ID (1) | ID15864A (id) |
| LT (1) | LT4340B (id) |
| RU (1) | RU2134251C1 (id) |
| SA (1) | SA97170602B1 (id) |
| WO (1) | WO1997028100A1 (id) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102004005907B4 (de) * | 2004-02-05 | 2006-01-05 | Uhde Gmbh | Anlage zur Herstellung von biuretarmem harnstoffhaltigem Düngemittelgranulat |
| NL1025805C2 (nl) * | 2004-03-25 | 2005-09-27 | Dsm Ip Assets Bv | Werkwijze voor de granulatie van ureum. |
| US7862642B2 (en) * | 2006-12-14 | 2011-01-04 | Georgia-Pacific Chemicals Llc | Extended-release urea-based granular fertilizer |
| EP2489429A1 (en) * | 2011-02-21 | 2012-08-22 | Urea Casale S.A. | Fluid bed granulation of urea and related apparatus |
| CN102976499B (zh) * | 2012-12-03 | 2013-12-04 | 北京师范大学 | 同时缓释氮和吸附-生物降解石油烃的复合板制备方法 |
| EP2745901A1 (en) * | 2012-12-19 | 2014-06-25 | Urea Casale SA | Method for transforming a prilling tower, in particular in a plant for the synthesis of urea |
| CN103011982B (zh) * | 2012-12-29 | 2014-12-31 | 金正大生态工程集团股份有限公司 | 一种脲醛缓释复合肥料的工业化生产方法和装置 |
| GB201502893D0 (en) * | 2015-02-20 | 2015-04-08 | Johnson Matthey Plc | Process |
| GB201502894D0 (en) | 2015-02-20 | 2015-04-08 | Johnson Matthey Plc | Process |
| US10519103B2 (en) | 2015-04-01 | 2019-12-31 | Toyo Engineering Corporation | Urea production method |
| CN105461361B (zh) * | 2015-12-25 | 2019-05-14 | 北方华锦化学工业股份有限公司 | 多路蒸发尿素造粒系统 |
| DE102017108842A1 (de) * | 2017-04-25 | 2018-10-25 | Thyssenkrupp Ag | Verfahren und Vorrichtung zur Herstellung von Harnstoff |
| CN117756573B (zh) * | 2023-12-14 | 2026-01-02 | 宁波中科远东催化工程技术有限公司 | 一种大颗粒尿素的生产方法 |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3067177A (en) | 1957-10-30 | 1962-12-04 | Montedison Spa | Process for producing concentrated urea-formaldehyde solutions by absorbing gaseous formaldehyde in aqueous urea solutions |
| US3112313A (en) | 1963-11-26 | Process for the production thereof | ||
| JPS5034536A (id) | 1973-07-27 | 1975-04-02 | ||
| US4219589A (en) | 1977-06-09 | 1980-08-26 | Compagnie Neerlandaise De L'azote | Process for urea granulation |
| JPH063729A (ja) | 1992-06-18 | 1994-01-14 | Nikon Corp | 縦走りフォーカルプレーンシャッタ用遮光羽根の製造方 法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB926781A (en) * | 1959-06-02 | 1963-05-22 | Vulcan Cincinnati Inc | Dehydration of urea melts |
| US3112343A (en) * | 1959-08-20 | 1963-11-26 | Chemie Linz Ag | Free-flowing, storage stable granular or pelletized urea |
| US3059280A (en) * | 1960-10-27 | 1962-10-23 | Grace W R & Co | Urea prilling |
| US3130225A (en) * | 1962-02-12 | 1964-04-21 | Pullman Inc | Urea production |
| US3378584A (en) * | 1963-07-05 | 1968-04-16 | Grace W R & Co | Process for reducing the caking tendency of crystalline urea |
| US3686373A (en) * | 1970-02-09 | 1972-08-22 | George T Griesheimer | Urea-prill anti-caking process |
| US3970625A (en) * | 1973-03-14 | 1976-07-20 | Allied Chemical Corporation | Production of urea-formaldehyde concentrates |
| CA1101641A (en) * | 1977-06-09 | 1981-05-26 | Anton Niks | Urea granulation |
| NO148744C (no) * | 1977-09-19 | 1983-12-07 | Norsk Hydro As | Fremgangsmaate til fremstilling av urea med hoey mekanisk styrke |
| JPS6034517B2 (ja) * | 1978-03-03 | 1985-08-09 | 宇部興産株式会社 | 流動層で尿素を造粒する方法 |
| DE3013616C2 (de) * | 1979-05-11 | 1984-08-02 | VEB Stickstoffwerk Piesteritz, DDR 4602 Wittenberg-Lutherstadt-Piesteritz | Verfahren zur Behandlung von Harnstoff sowie ammonium- und nitrathaltigen Düngemitteln |
| JPS6058193B2 (ja) * | 1980-01-31 | 1985-12-18 | 宇部興産株式会社 | 尿素の流動造粒方法 |
| NL8001876A (nl) * | 1980-03-29 | 1981-11-02 | Unie Van Kunstmestfab Bv | Werkwijze voor het maken van ureumprils en ureumprils verkregen met deze werkwijze. |
| JPS61216725A (ja) * | 1985-03-20 | 1986-09-26 | Mitsui Toatsu Chem Inc | 尿素の造粒方法 |
| SU1507761A1 (ru) * | 1987-03-19 | 1989-09-15 | Предприятие П/Я А-1676 | Способ получени гранулированного карбамида |
| JPH01286985A (ja) * | 1988-05-11 | 1989-11-17 | Mitsui Toatsu Chem Inc | 緩効性窒素肥料の製造方法 |
| JPH06305869A (ja) * | 1993-04-28 | 1994-11-01 | Mitsui Toatsu Chem Inc | 緩効性窒素肥料の製造法 |
-
1996
- 1996-02-01 JP JP01654196A patent/JP3667418B2/ja not_active Expired - Lifetime
-
1997
- 1997-01-21 BR BR9702047A patent/BR9702047A/pt not_active IP Right Cessation
- 1997-01-21 US US08/913,871 patent/US5965071A/en not_active Expired - Lifetime
- 1997-01-21 CN CN97190048A patent/CN1098234C/zh not_active Expired - Lifetime
- 1997-01-21 ES ES97900462T patent/ES2182019T3/es not_active Expired - Lifetime
- 1997-01-21 CA CA002215596A patent/CA2215596C/en not_active Expired - Lifetime
- 1997-01-21 RU RU97118419A patent/RU2134251C1/ru active
- 1997-01-21 DE DE69716177T patent/DE69716177T2/de not_active Revoked
- 1997-01-21 AU AU20172/97A patent/AU705068B2/en not_active Ceased
- 1997-01-21 EP EP97900462A patent/EP0819106B1/en not_active Revoked
- 1997-01-21 WO PCT/JP1997/000108 patent/WO1997028100A1/en not_active Ceased
- 1997-01-29 AR ARP970100351A patent/AR005588A1/es active IP Right Grant
- 1997-01-31 ID IDP970309A patent/ID15864A/id unknown
- 1997-02-01 SA SA97170602A patent/SA97170602B1/ar unknown
- 1997-09-30 LT LT97-156A patent/LT4340B/lt not_active IP Right Cessation
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3112313A (en) | 1963-11-26 | Process for the production thereof | ||
| US3067177A (en) | 1957-10-30 | 1962-12-04 | Montedison Spa | Process for producing concentrated urea-formaldehyde solutions by absorbing gaseous formaldehyde in aqueous urea solutions |
| JPS5034536A (id) | 1973-07-27 | 1975-04-02 | ||
| US4219589A (en) | 1977-06-09 | 1980-08-26 | Compagnie Neerlandaise De L'azote | Process for urea granulation |
| JPH063729A (ja) | 1992-06-18 | 1994-01-14 | Nikon Corp | 縦走りフォーカルプレーンシャッタ用遮光羽根の製造方 法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1098234C (zh) | 2003-01-08 |
| SA97170602B1 (ar) | 2006-08-20 |
| JP3667418B2 (ja) | 2005-07-06 |
| RU2134251C1 (ru) | 1999-08-10 |
| WO1997028100A1 (en) | 1997-08-07 |
| DE69716177D1 (de) | 2002-11-14 |
| ID15864A (id) | 1997-08-14 |
| US5965071A (en) | 1999-10-12 |
| CA2215596A1 (en) | 1997-08-07 |
| DE69716177T2 (de) | 2003-05-28 |
| BR9702047A (pt) | 1998-01-13 |
| EP0819106B1 (en) | 2002-10-09 |
| AR005588A1 (es) | 1999-06-23 |
| LT97156A (en) | 1998-02-25 |
| AU705068B2 (en) | 1999-05-13 |
| ES2182019T3 (es) | 2003-03-01 |
| EP0819106A1 (en) | 1998-01-21 |
| CN1178516A (zh) | 1998-04-08 |
| CA2215596C (en) | 2001-10-16 |
| JPH09208552A (ja) | 1997-08-12 |
| AU2017297A (en) | 1997-08-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM9A | Lapsed patents |
Effective date: 20020121 |