KR950701679A - 페이스트형 세제의 제조 방법(process for producing pasty washing agents) - Google Patents
페이스트형 세제의 제조 방법(process for producing pasty washing agents)Info
- Publication number
- KR950701679A KR950701679A KR1019940704096A KR19940704096A KR950701679A KR 950701679 A KR950701679 A KR 950701679A KR 1019940704096 A KR1019940704096 A KR 1019940704096A KR 19940704096 A KR19940704096 A KR 19940704096A KR 950701679 A KR950701679 A KR 950701679A
- Authority
- KR
- South Korea
- Prior art keywords
- nonionic
- soap
- mixture
- anionic surfactants
- process according
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract 13
- 238000005406 washing Methods 0.000 title 1
- 239000003599 detergent Substances 0.000 claims abstract 9
- 239000002736 nonionic surfactant Substances 0.000 claims abstract 9
- 239000000344 soap Substances 0.000 claims abstract 9
- 239000003945 anionic surfactant Substances 0.000 claims abstract 8
- 239000000203 mixture Substances 0.000 claims abstract 7
- 239000011874 heated mixture Substances 0.000 claims abstract 3
- 239000007844 bleaching agent Substances 0.000 claims abstract 2
- 238000001816 cooling Methods 0.000 claims abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- 230000006203 ethylation Effects 0.000 claims 2
- 238000006200 ethylation reaction Methods 0.000 claims 2
- 238000010348 incorporation Methods 0.000 claims 2
- 102000004190 Enzymes Human genes 0.000 claims 1
- 108090000790 Enzymes Proteins 0.000 claims 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 claims 1
- AWMVMTVKBNGEAK-UHFFFAOYSA-N Styrene oxide Chemical compound C1OC1C1=CC=CC=C1 AWMVMTVKBNGEAK-UHFFFAOYSA-N 0.000 claims 1
- -1 anionic anhydride Chemical class 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims 1
- 235000014113 dietary fatty acids Nutrition 0.000 claims 1
- VTIIJXUACCWYHX-UHFFFAOYSA-L disodium;carboxylatooxy carbonate Chemical compound [Na+].[Na+].[O-]C(=O)OOC([O-])=O VTIIJXUACCWYHX-UHFFFAOYSA-L 0.000 claims 1
- 239000002270 dispersing agent Substances 0.000 claims 1
- 239000000975 dye Substances 0.000 claims 1
- 229930195729 fatty acid Natural products 0.000 claims 1
- 239000000194 fatty acid Substances 0.000 claims 1
- 150000004665 fatty acids Chemical class 0.000 claims 1
- 239000006260 foam Substances 0.000 claims 1
- 239000003205 fragrance Substances 0.000 claims 1
- 239000003112 inhibitor Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 230000003287 optical effect Effects 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 229920005646 polycarboxylate Polymers 0.000 claims 1
- 150000004760 silicates Chemical class 0.000 claims 1
- 229960001922 sodium perborate Drugs 0.000 claims 1
- 229940045872 sodium percarbonate Drugs 0.000 claims 1
- 159000000000 sodium salts Chemical class 0.000 claims 1
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 claims 1
- 239000002689 soil Substances 0.000 claims 1
- 239000000375 suspending agent Substances 0.000 claims 1
- FRPJTGXMTIIFIT-UHFFFAOYSA-N tetraacetylethylenediamine Chemical compound CC(=O)C(N)(C(C)=O)C(N)(C(C)=O)C(C)=O FRPJTGXMTIIFIT-UHFFFAOYSA-N 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0004—Non aqueous liquid compositions comprising insoluble particles
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3947—Liquid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
본 발명은 페이스트형 세제에 관한 것이다. 소프는 비이온계 및 음이온계 계면 활성제의 가열 혼합물 중에 혼입되며 이 혼합물은 냉각 후 빌더 및 표백제와 같은 세제의 기타 성분과 혼입된다. 이렇게 제조된 수분을 전혀 함유하지 않거나 거의 함유하지 않는 세제는 침강에 대하여 안정하고 오랜 저장 후에도 활성 산소와 양이 현저히 저하되지 않는다.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (11)
- 비이온계 및 음이온계 계면 활성제, 소프, 빌더 및 표백제를 함유하는 페이스트형의 수분이 전혀 존재하지 않거나 거의 존재 하지 않는 세제의 제조방법에 있어서, 소프를 비이온계 및 음이온계 계면 활성제의 가열된 혼합물 중에 미립자 및 분산자 형태로 혼입하고 나머지 세제 성분을 이 혼합물의 냉각 후에 혼입함을 특징으로 하는 제조 방법.
- 제1항에 있어서, 비이온계 및 음이온계 계면 활성제가 소프의 혼입 전에 70~90℃, 바람직하게는 80~85℃로 가열함을 특징으로 하는 제조 방법.
- 제1 또는 2항에 있어서, 소프를 물의 첨가 없이 0.4㎜ 이하의 크기를 가진 입자 형태로 비이온계 및 음이온계 계면 활성제의 가열 혼하불에 혼합물을 특징으로 하는 제조 방법.
- 제1내지 3항 중 어느 한 항에 있어서, 소프를 고정자/회전자 원리로 조작되는 혼합 단위 장치를 사용하여 비이온계 및 음이온계 계면 활성제의 가열 혼합물에 혼입함을 특징으로 하는 제조 방법.
- 제1또는 2항에 있어서, 혼입 전에, 최종 세제가 1중량% 이하를 함유하도록 하는 양의 물에 소프를 분산시킴을 특징으로 하는 제조 방법.
- 제1내지 5항 중 어느 한 항에 있어서, 비이온계 및 음이온계 계면활성제와 소프의 혼합물을 30℃ 미만으로 냉각시킨 후 세제의 나머지 성분을 혼입시킴을 특징으로 하는 제조 방법.
- 제1내지 6항중 어느 한 항에 있어서, 최종 세제에 대하여 3~60중량%의 양으로 2이상의 다른 비이온계 계면 활성제, 바람직하게는 지방족 알콜 1몰당 에티렌 옥사이드가 2~7몰인 에특실화가 다른 지방족 알콜 성분중의 탄소수 12~18의 지방족 알콜 에톡실레이트가 비이온계 및 음이온계 계면 활성제의 혼합물에 사용됨을 특징으로 하는 제조 방법.
- 제1내지 7항 중 어느 한 항에 있어서, 탄소수 12~22의 선형의 지방산의 나트륨염이 소프로서 최종 세제를 기준으로 0.5~10중량%의 양으로 사용됨을 특징으로 하는 제조 방법.
- 제1내지 8항 중 어느 한 항에 있어서, 폴리카르복실레이트 및/또는 포스포네이트 및/또는 카르보네이트 및/또는 실리케이트가 빌더로서 최종세제를 기준으로 10~50중량%의 양으로 사용됨을 특징으로 하는 제조방법.
- 제1내지 5항중 어느 한 항에 있어서, 과붕산나트륨 및/또는 과탄산나트륨이 표백제로서, 원한다면 특히 테트라아세틸 에틸렌디아민 또는 디피옥시도데칸 디온산 무수물과 활성제화 배합하여 최종 세제를 기준으로 10~30중량%의 양으로 사용됨을 특징으로 하는 제조 방법.
- 제1내지 10항 중 어느 한 항에 있어서, 효소, 발포 억제제, 광학 중백제, 토양 현탁제, 향료 및 염료와 같은 기타의 성분을 추가로 소량으로 혼입함을 특징으로 하는 제조 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4216453A DE4216453A1 (de) | 1992-05-19 | 1992-05-19 | Verfahren zur Herstellung pastenförmiger Waschmittel |
DEP4216453.2 | 1992-05-19 | ||
PCT/EP1993/001146 WO1993023521A1 (de) | 1992-05-19 | 1993-05-11 | Verfahren zur herstellung pastenförmiger waschmittel |
Publications (1)
Publication Number | Publication Date |
---|---|
KR950701679A true KR950701679A (ko) | 1995-04-28 |
Family
ID=6459194
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019940704096A KR950701679A (ko) | 1992-05-19 | 1993-05-11 | 페이스트형 세제의 제조 방법(process for producing pasty washing agents) |
Country Status (13)
Country | Link |
---|---|
US (1) | US5518645A (ko) |
EP (1) | EP0641381B2 (ko) |
JP (1) | JPH07506607A (ko) |
KR (1) | KR950701679A (ko) |
AT (1) | ATE134384T1 (ko) |
CA (1) | CA2136173A1 (ko) |
DE (2) | DE4216453A1 (ko) |
DK (1) | DK0641381T4 (ko) |
ES (1) | ES2083285T5 (ko) |
FI (1) | FI945417A (ko) |
GR (2) | GR3019219T3 (ko) |
NO (1) | NO306560B1 (ko) |
WO (1) | WO1993023521A1 (ko) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6916596B2 (en) | 1993-06-25 | 2005-07-12 | Michael Wen-Chein Yang | Laser imaged printing plates |
US6756181B2 (en) | 1993-06-25 | 2004-06-29 | Polyfibron Technologies, Inc. | Laser imaged printing plates |
US5506201A (en) * | 1994-04-29 | 1996-04-09 | International Flavors & Fragrances Inc. | Formulation of a fat surfactant vehicle containing a fragrance |
DE4436151A1 (de) * | 1994-08-16 | 1996-05-02 | Henkel Kgaa | Verfahren zur Herstellung eines Flüssigwaschmittels mit Bleiche |
CA2199817C (en) * | 1994-09-26 | 2000-07-25 | The Procter & Gamble Company | Nonaqueous bleach-containing liquid detergent compositions |
JPH10506930A (ja) * | 1994-09-26 | 1998-07-07 | ザ、プロクター、エンド、ギャンブル、カンパニー | 非水性漂白剤含有液体洗剤組成物の製法 |
DE19535082A1 (de) * | 1995-09-21 | 1997-03-27 | Henkel Ecolab Gmbh & Co Ohg | Pastenförmiges Wasch- und Reinigungsmittel |
US6083488A (en) * | 1996-12-04 | 2000-07-04 | The Block Drug Company | Barrier to plaque formation |
DE19703364A1 (de) * | 1997-01-30 | 1998-08-06 | Henkel Ecolab Gmbh & Co Ohg | Pastenförmiges Wasch- und Reinigungsmittel |
US5863887A (en) * | 1997-12-01 | 1999-01-26 | Precision Fabrics Group, Inc. | Laundry compositions having antistatic and fabric softening properties, and laundry detergent sheets containing the same |
US6130193A (en) * | 1998-02-06 | 2000-10-10 | Precision Fabrics Group, Inc. | Laundry detergent compositions containing silica for laundry detergent sheets |
DE10017540C2 (de) * | 2000-04-08 | 2002-07-04 | Henkel Kgaa | Verfahren zur Herstellung von flüssigen bis gelförmigen Reinigungsmitteln |
US7694583B2 (en) * | 2005-05-05 | 2010-04-13 | Control Gaging, Inc. | Gripper gage assembly |
JP5868747B2 (ja) * | 2012-03-19 | 2016-02-24 | 花王株式会社 | 界面活性剤混合物の製造方法 |
DE102012015826A1 (de) | 2012-08-09 | 2014-02-13 | Clariant International Ltd. | Flüssige tensidhaltige Alkanolamin-freie Zusammensetzungen |
DE102017208559A1 (de) * | 2017-05-19 | 2018-11-22 | Henkel Ag & Co. Kgaa | Verfahren zur Herstellung gelförmiger Substanzen |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB8522621D0 (en) * | 1985-09-12 | 1985-10-16 | Unilever Plc | Detergent powder |
DE3621536A1 (de) * | 1986-06-27 | 1988-01-07 | Henkel Kgaa | Fluessiges waschmittel und verfahren zu seiner herstellung |
DE3842007A1 (de) * | 1988-12-14 | 1990-06-21 | Henkel Kgaa | Fluessiges bis pastoeses, bleichmittelhaltiges waschmittel |
DE3914504A1 (de) * | 1989-05-02 | 1990-11-08 | Henkel Kgaa | Pastoeses, phosphatfreies, im wesentlichen wasserfreies waschmittel |
GB2237285A (en) * | 1989-10-27 | 1991-05-01 | Unilever Plc | Liquid soap composition |
DE4009532A1 (de) * | 1990-03-24 | 1991-09-26 | Henkel Kgaa | Waschmittel-formkoerper |
US5244593A (en) * | 1992-01-10 | 1993-09-14 | The Procter & Gamble Company | Colorless detergent compositions with enhanced stability |
-
1992
- 1992-05-19 DE DE4216453A patent/DE4216453A1/de not_active Withdrawn
-
1993
- 1993-05-11 DK DK93909938T patent/DK0641381T4/da active
- 1993-05-11 JP JP5519856A patent/JPH07506607A/ja active Pending
- 1993-05-11 ES ES93909938T patent/ES2083285T5/es not_active Expired - Lifetime
- 1993-05-11 DE DE59301689T patent/DE59301689D1/de not_active Expired - Fee Related
- 1993-05-11 AT AT93909938T patent/ATE134384T1/de not_active IP Right Cessation
- 1993-05-11 CA CA002136173A patent/CA2136173A1/en not_active Abandoned
- 1993-05-11 EP EP93909938A patent/EP0641381B2/de not_active Expired - Lifetime
- 1993-05-11 KR KR1019940704096A patent/KR950701679A/ko not_active Application Discontinuation
- 1993-05-11 WO PCT/EP1993/001146 patent/WO1993023521A1/de active IP Right Grant
-
1994
- 1994-09-08 NO NO943320A patent/NO306560B1/no not_active IP Right Cessation
- 1994-11-17 FI FI945417A patent/FI945417A/fi unknown
- 1994-12-07 US US08/338,565 patent/US5518645A/en not_active Expired - Fee Related
-
1996
- 1996-03-05 GR GR960400626T patent/GR3019219T3/el unknown
-
1999
- 1999-11-08 GR GR990402868T patent/GR3031777T3/el unknown
Also Published As
Publication number | Publication date |
---|---|
EP0641381B1 (de) | 1996-02-21 |
NO306560B1 (no) | 1999-11-22 |
NO943320L (no) | 1994-09-08 |
NO943320D0 (no) | 1994-09-08 |
DE59301689D1 (de) | 1996-03-28 |
JPH07506607A (ja) | 1995-07-20 |
CA2136173A1 (en) | 1993-11-25 |
WO1993023521A1 (de) | 1993-11-25 |
FI945417A0 (fi) | 1994-11-17 |
DK0641381T3 (da) | 1996-06-24 |
FI945417A (fi) | 1994-11-17 |
EP0641381A1 (de) | 1995-03-08 |
ES2083285T5 (es) | 1999-11-16 |
GR3031777T3 (en) | 2000-02-29 |
DE4216453A1 (de) | 1993-11-25 |
US5518645A (en) | 1996-05-21 |
DK0641381T4 (da) | 2000-01-03 |
GR3019219T3 (en) | 1996-06-30 |
ATE134384T1 (de) | 1996-03-15 |
ES2083285T3 (es) | 1996-04-01 |
EP0641381B2 (de) | 1999-09-29 |
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