KR920017733A - 금속의 냉연을 위한 윤활조성물 및 윤활방법 - Google Patents
금속의 냉연을 위한 윤활조성물 및 윤활방법 Download PDFInfo
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- KR920017733A KR920017733A KR1019920004722A KR920004722A KR920017733A KR 920017733 A KR920017733 A KR 920017733A KR 1019920004722 A KR1019920004722 A KR 1019920004722A KR 920004722 A KR920004722 A KR 920004722A KR 920017733 A KR920017733 A KR 920017733A
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- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
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Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (20)
- (A)물중에 용해 또는 분산시킬 수 있는 충분한 수의 염그룹을 포함하는 말레산 부분과 스티렌의 공중합체; 및 (B) 에톡실화된 알코올 분자로 이루어진 성분; 및 선택적으로 (C) 물; 및 선택적으로 (D) 고도한 압력내성 및 내식성의 추가성분; 및 선택적으로 (E) 분산되거나 또는 용해된 고체 윤활제의 성분; 및 선택적으로 (F) 고체와 액체 하이드로카본으로부터 선택된 성분으로 본질적으로 이루어진 물질의 액체 조성물.
- 제1항에 있어서, 성분(B)는 단지 하나의 히드록실그룹과 분자당 약 30 내지 약65개의 탄소원자를 갖는 주 직쇄지방족 선구물질 알코올과 에틸렌 옥시드가 축합됨에 의해 제조될 수 있는 화학구조를 갖고, n이 양의 정수인 화학구조-(CH2-CH2-O)n′을 갖는 각 분자의 부분중에 전체 중량의 20 내지 80%를 갖는 에톡실화된 알코올로부터 선택되는 것을 특징으로 하는 조성물.
- 제2항에 있어서, 성분(A)는 스티렌 대 말레산 부분의 분자비가 1:1 내지 3:1인 중합체로부터 선택되고 선분(A) 대 (B)의 중량비의 범위가 약 6:1 내지 약 1:6인 것을 특징으로 하는 조성물.
- 제3항에 있어서, 성분(A)중의 중합체의 염그룹과 관련된 적어도 78몰%의 양이온은 물중에서 적어도 10의 pH값을 갖고 적어도 0.01M 용액을 형성할 수 있는 아민분자에 양자를 부가함에 의해 형성된 암모늄 양이온인 것을 특징으로 하는 조성물.
- 제4항에 있어서, (a) 성분 (D)는 (i)m이 약 16내지 약 22의 정수진 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 1.3중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적에스테르와의 염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분(D)는 전체성분(A)와(B)에 대한 중량비가 약1:40 내지 1:55의 범위로 제공되는 것을 특징으로 하는 조성물.
- 제3항에 있어서, (a) 성분 (D)가 (i)m이 약 12 내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.9중량%의 범위로 물중에 용해될 수 있는 충분히 큰값을 갖는 정수인 구조 (CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분(D)는 전체성분(A)와(B)에 대한 중량비가 약1:25 내지 약 1:70의 범위로 제공되는 것을 특징으로 하는 조성물.
- 제2항에 있어서, (a) 성분 (D)는 (i)m이 약 12 내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.4중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약1:10 내지 2:200의 범위로 제공되는 것을 특징으로 하는 조성물.
- 제1항에 있어서, (a) 성분 (D)가 (i)m이 약 12내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.1중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약 1:10 내지 1:200의 범위로 제공되는 것을 특징으로 하는 조성물.
- (A)물중에 용해 또는 분산시킬 수 있는 충분한 수의 염그룹을 포함하는, 말레산 부분과 스티렌의 공중합체 및 (B) 에톡실화된 알코올 분자로 이루어진 성분; 및 선택적으로 (C) 물; 및 선택적으로 (D) 고도한 압력내성 및 내식성의 추가성분; 및 선택적으로 (E) 분산되거나 또는 용해된 고체 윤활제의 성분; 및 선택적으로 (F) 고체와 액체 하이드로카본으로부터 선택된 성분으로 본질적으로 이루어진 윤활 조성물로 냉간가공되는 금속 가재표면에서 냉간가공시키는 것을 특징으로 하는 금속기재를 냉연하는 방법.
- 제9항에 있어서, 성분(B)는 단지 하나의 히드록실 그룹과 분자당 약 30 내지 약65개의 탄소원자를 갖는 주 직쇄지방족 선구물질 알코올과 에틸렌 옥시드가 축합됨에 의해 제조될 수 있는 화학구조를 갖고, n이 양의 정수인 화학구조-(CH2-CH2-O)n′을 갖는 각 분자의 부분중에 전체 중량의 20 내지 80%를 갖는 에톡실화된 알코올로부터 선택되는 것을 특징으로 하는 방법.
- 제10항에 있어서, 성분(A)는 스티렌 대 말레산 부분의 분자비가 1:1 내지 3:1인 중합체로부터 선택되고 성분(A) 대 (B)의 중량비의 범위가 약 6:1 내지 약 1:6인 것을 특징으로 하는 방법.
- 제11항에 있어서, 70℃의 온도에서 본발명에 따른 상기 윤활조성물상의 대기압에서 드라저 시험 장치에 의해 측정된 평형 과압의 NH3당량이 암모니아 당량의 25ppm이하인 것을 특징으로 하는 방법.
- 제12항에 있어서, (a) 성분 (D)는 (i)m이 약 16내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 1.3중량%의 범위로 물중에 용해될 수 있는 충분히 큰값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약1:40 내지 1:55의 범위로 제공되는 것을 특징으로 하는 방법.
- 제11항에 있어서, (a) 성분 (D)가 (i)m이 약 12내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.9중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분(D)는 약1:25 내지 약 1:7의 범위로 제공되는 것을 특징으로 하는 방법.
- 제10항에 있어서, (a) 성분 (D)는 (i)m이 약 12내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.4중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약1:10 내지 1:200의 범위로 제공되는 것을 특징으로 하는 방법.
- 제9항에 있어서, (a) 성분 (D)는 (i)m이 약 12내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.1중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약1:25 내지 1:70의 범위로 제공되는 것을 특징으로 하는 방법.
- 제16항에 있어서, (a)냉간 가공하고자 하는 금속기재의 표면에, 상기 윤활조성물을 제공하기 전에 약 1 내지 약 50g/㎡의 양으로 피복하고 (ii) 냉간 가공전에 주변 공기중에서 피복을 수용액을 건조시킴에 의해 냉간 가공하고자 하는 금속기재의 표면상에 적용시키는 것을 특징으로 하는 방법.
- 제15항에 있어서, (a) 냉간 가공하고자 하는 금속기재의 표면에, 상기 윤활조성물을 제공하기 전에 약 1 내지 약 50g/㎡의 면적 밀도를 갖는 인산 아연 전환 피복물을 제공하고 (b) 상기 윤활 조성물을 (i) 약 6 내지 약 11의 pH범위를 갖고 전체 용해된 고체의 약 5 내지 20중량%를 포함하는 수용액 조성물을 냉간 가공하고자 하는 금속 기재 표면상에서 고체의 밀적밀도를 약 0.1 내지 약 8g/㎡의 양으로 피복하고, (ii) 냉간 가공전에 주변공기중에서 피복물 수용액을 건조함에 의해 냉간 가공하고자 하는 금속 기재의 표면상에 적용시키는 것을 특징으로 하는 방법.
- 제16항에 있어서, (a) 냉간 가공하고자 하는 금속기재의 표면에, 상기 윤활조성물을 제공하기 전에 약 1 내지 약 20g/㎡의 면적 밀도를 갖는 인산 아연 전환 피복물을 제공하고 (b) 상기 윤활 조성물을 (i) 약 7.5 내지 약 9의 pH범위를 갖고 전체 용해된 고체의 약 8 내지 12중량%를 포함하는 수용액 조성물을 냉간 가공하고자 하는 금속 기재 표면상에서 고체의 밀적밀도를 약 2.0 내지 약 6g/㎡의 양으로 피복하고, (ii) 냉간 가공전에 주변공기중에서 피복물 수용액을 건조함에 의해 냉간 가공하고자 하는 금속 기재의 표면상에 적용시키는 것을 특징으로 하는 방법.
- 제13항에 있어서, (a) 냉간 가공하고자 하는 금속기재의 표면에, 상기 윤활혼합물을 제공하기 전에 약 2 내지 약 15g/㎡의 면적 밀도를 갖는 인산 아연 전화 피복물을 제공하고 (b) 상기 윤활 조성물을 (i) 약 7.5 내지 약 9의 pH범위를 갖고 전체 용해된 고체의 약 8 내지 12중량%를 포함하는 수용액 혼합물을 냉간 가공하고자 하는 금속 기재표면상에서 고체의 면적밀도를 약 2.0 내지 약 6g/mℓ의 양으로 피복하고, (ii) 냉간 가공전에 주변공기중에서 피복물 수용액을 건조함에 의해 냉간 가공하고자 하는 금속 기재의 표면상에 적용시키는 것을 특징으로 하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US67387491A | 1991-03-22 | 1991-03-22 | |
US07/673,874 | 1991-03-22 | ||
US77108991A | 1991-10-02 | 1991-10-02 | |
US07/771089 | 1991-10-02 |
Publications (1)
Publication Number | Publication Date |
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KR920017733A true KR920017733A (ko) | 1992-10-21 |
Family
ID=27101041
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Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019920004722A KR920017733A (ko) | 1991-03-22 | 1992-03-21 | 금속의 냉연을 위한 윤활조성물 및 윤활방법 |
Country Status (7)
Country | Link |
---|---|
US (1) | US5368757A (ko) |
KR (1) | KR920017733A (ko) |
AU (1) | AU1467292A (ko) |
BR (1) | BR9200993A (ko) |
MX (1) | MX9201190A (ko) |
TW (1) | TW202479B (ko) |
WO (1) | WO1992016603A1 (ko) |
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CA2116880A1 (en) * | 1993-03-23 | 1994-09-24 | Anthony P. Willoughby | Forging lubricant composition and process |
EP0759818A4 (en) * | 1994-05-13 | 1997-08-20 | Henkel Corp | AQUEOUS METAL COATING COMPOSITION AND METHOD WITH REDUCED SPOTTING AND CORROSION |
US5484541A (en) * | 1994-05-17 | 1996-01-16 | Century Chemical Corporation | Process and product for lubricating metal prior to cold forming |
US5531912A (en) * | 1994-09-02 | 1996-07-02 | Henkel Corporation | Composition and process for lubricating metal before cold forming |
WO1996011247A1 (en) * | 1994-10-07 | 1996-04-18 | Henkel Corporation | Aqueous metal coating composition and process with improved wetting of oily or similarly soiled surfaces |
DE4445993A1 (de) * | 1994-12-22 | 1996-06-27 | Metallgesellschaft Ag | Schmiermittel für die Metallumformung |
US5547595A (en) * | 1995-02-07 | 1996-08-20 | Henkel Corporation | Aqueous lubricant and process for cold forming metal, particularly pointing thick-walled metal tubes |
CA2271730A1 (en) * | 1996-11-27 | 1998-06-04 | Henkel Corporation | Aqueous composition and process for preparing metal substrate for cold forming |
US5891268A (en) * | 1996-12-06 | 1999-04-06 | Henkel Corporation | High coating weight iron phosphating, compositions therefor, and use of the coating formed as a lubricant carrier |
US5853506A (en) * | 1997-07-07 | 1998-12-29 | Ford Motor Company | Method of treating metal working dies |
AU6212000A (en) | 1999-07-13 | 2001-01-30 | Century Chemical Corporation | Improved process and product for lubricating metal prior to cold forming |
WO2001094663A1 (en) * | 2000-06-06 | 2001-12-13 | Henkel Kommanditgesellschaft Auf Aktien | Coating for cold working metals |
CA2423086A1 (en) * | 2000-09-22 | 2002-03-28 | Henkel Kommanditgesellschaft Auf Aktien | Hydroforming lubricants |
US20030181340A1 (en) * | 2000-09-22 | 2003-09-25 | Botz Frank K. | Lubricants suitable for hydroforming and other metal manipulating applications |
DE10115696A1 (de) * | 2001-03-29 | 2002-10-10 | Henkel Kgaa | Schmierstoffmischung und ihre Verwendung |
US20060172064A1 (en) * | 2003-01-10 | 2006-08-03 | Henkel Kommanditgesellschaft Auf Aktien | Process of coating metals prior to cold forming |
US10472585B2 (en) * | 2013-07-10 | 2019-11-12 | Nihon Parkerizing Co., Ltd. | Aqueous lubricant for plastic working of metal material and having superior gas clogging resistance and post-moisture absorption workability |
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US3372117A (en) * | 1965-11-26 | 1968-03-05 | Hooker Chemical Corp | Cold forming lubricant |
US3527726A (en) * | 1968-07-17 | 1970-09-08 | Atlantic Richfield Co | Water-soluble ammonium or amine salts of phosphate esters of styrene-maleic anhydride copolymer - polyalkylene glycol esters |
US3629112A (en) * | 1968-11-25 | 1971-12-21 | Atlantic Richfield Co | Aqueous lubricating compositions containing salts of styrene-maleic anhydride copolymers and an inorganic boron compound |
US3568486A (en) * | 1969-01-31 | 1971-03-09 | Montgomery H A Co | Preparation of metal for deforming operations |
US3657123A (en) * | 1970-03-23 | 1972-04-18 | Atlantic Richfield Co | Lubricant compositions |
SU433201A1 (ru) * | 1971-12-15 | 1974-06-25 | ЙПНП Ппсотпо | Эмульсионный смазочный материал дня холожюй обраютш металлов |
US3833502A (en) * | 1973-04-30 | 1974-09-03 | Nalco Chemical Co | Method for improving the adherence of metalworking coolants to metal surfaces |
JPS5337817B2 (ko) * | 1974-07-08 | 1978-10-12 | ||
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US4285223A (en) * | 1979-02-12 | 1981-08-25 | Narayan Das | Phosphate and ester coating method |
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JPS638489A (ja) * | 1986-06-27 | 1988-01-14 | Nippon Parkerizing Co Ltd | 金属の冷間加工用潤滑剤 |
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JP2564136B2 (ja) * | 1987-05-30 | 1996-12-18 | 大同化学工業株式会社 | 金属圧延油組成物 |
-
1992
- 1992-03-09 WO PCT/US1992/001942 patent/WO1992016603A1/en active Application Filing
- 1992-03-09 AU AU14672/92A patent/AU1467292A/en not_active Abandoned
- 1992-03-18 MX MX9201190A patent/MX9201190A/es unknown
- 1992-03-20 BR BR929200993A patent/BR9200993A/pt not_active Application Discontinuation
- 1992-03-21 KR KR1019920004722A patent/KR920017733A/ko not_active Application Discontinuation
- 1992-04-15 TW TW081102946A patent/TW202479B/zh active
-
1993
- 1993-01-19 US US08/005,913 patent/US5368757A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
AU1467292A (en) | 1992-10-21 |
US5368757A (en) | 1994-11-29 |
WO1992016603A1 (en) | 1992-10-01 |
MX9201190A (es) | 1992-10-01 |
TW202479B (ko) | 1993-03-21 |
BR9200993A (pt) | 1992-11-24 |
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