KR920017733A - 금속의 냉연을 위한 윤활조성물 및 윤활방법 - Google Patents

금속의 냉연을 위한 윤활조성물 및 윤활방법 Download PDF

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KR920017733A
KR920017733A KR1019920004722A KR920004722A KR920017733A KR 920017733 A KR920017733 A KR 920017733A KR 1019920004722 A KR1019920004722 A KR 1019920004722A KR 920004722 A KR920004722 A KR 920004722A KR 920017733 A KR920017733 A KR 920017733A
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에프. 킹 피터
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원본미기재
헨켈 코포레이션
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Abstract

내용 없음

Description

금속의 냉연을 위한 윤활조성물 및 윤활방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (20)

  1. (A)물중에 용해 또는 분산시킬 수 있는 충분한 수의 염그룹을 포함하는 말레산 부분과 스티렌의 공중합체; 및 (B) 에톡실화된 알코올 분자로 이루어진 성분; 및 선택적으로 (C) 물; 및 선택적으로 (D) 고도한 압력내성 및 내식성의 추가성분; 및 선택적으로 (E) 분산되거나 또는 용해된 고체 윤활제의 성분; 및 선택적으로 (F) 고체와 액체 하이드로카본으로부터 선택된 성분으로 본질적으로 이루어진 물질의 액체 조성물.
  2. 제1항에 있어서, 성분(B)는 단지 하나의 히드록실그룹과 분자당 약 30 내지 약65개의 탄소원자를 갖는 주 직쇄지방족 선구물질 알코올과 에틸렌 옥시드가 축합됨에 의해 제조될 수 있는 화학구조를 갖고, n이 양의 정수인 화학구조-(CH2-CH2-O)n′을 갖는 각 분자의 부분중에 전체 중량의 20 내지 80%를 갖는 에톡실화된 알코올로부터 선택되는 것을 특징으로 하는 조성물.
  3. 제2항에 있어서, 성분(A)는 스티렌 대 말레산 부분의 분자비가 1:1 내지 3:1인 중합체로부터 선택되고 선분(A) 대 (B)의 중량비의 범위가 약 6:1 내지 약 1:6인 것을 특징으로 하는 조성물.
  4. 제3항에 있어서, 성분(A)중의 중합체의 염그룹과 관련된 적어도 78몰%의 양이온은 물중에서 적어도 10의 pH값을 갖고 적어도 0.01M 용액을 형성할 수 있는 아민분자에 양자를 부가함에 의해 형성된 암모늄 양이온인 것을 특징으로 하는 조성물.
  5. 제4항에 있어서, (a) 성분 (D)는 (i)m이 약 16내지 약 22의 정수진 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 1.3중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적에스테르와의 염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분(D)는 전체성분(A)와(B)에 대한 중량비가 약1:40 내지 1:55의 범위로 제공되는 것을 특징으로 하는 조성물.
  6. 제3항에 있어서, (a) 성분 (D)가 (i)m이 약 12 내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.9중량%의 범위로 물중에 용해될 수 있는 충분히 큰값을 갖는 정수인 구조 (CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분(D)는 전체성분(A)와(B)에 대한 중량비가 약1:25 내지 약 1:70의 범위로 제공되는 것을 특징으로 하는 조성물.
  7. 제2항에 있어서, (a) 성분 (D)는 (i)m이 약 12 내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.4중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약1:10 내지 2:200의 범위로 제공되는 것을 특징으로 하는 조성물.
  8. 제1항에 있어서, (a) 성분 (D)가 (i)m이 약 12내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.1중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약 1:10 내지 1:200의 범위로 제공되는 것을 특징으로 하는 조성물.
  9. (A)물중에 용해 또는 분산시킬 수 있는 충분한 수의 염그룹을 포함하는, 말레산 부분과 스티렌의 공중합체 및 (B) 에톡실화된 알코올 분자로 이루어진 성분; 및 선택적으로 (C) 물; 및 선택적으로 (D) 고도한 압력내성 및 내식성의 추가성분; 및 선택적으로 (E) 분산되거나 또는 용해된 고체 윤활제의 성분; 및 선택적으로 (F) 고체와 액체 하이드로카본으로부터 선택된 성분으로 본질적으로 이루어진 윤활 조성물로 냉간가공되는 금속 가재표면에서 냉간가공시키는 것을 특징으로 하는 금속기재를 냉연하는 방법.
  10. 제9항에 있어서, 성분(B)는 단지 하나의 히드록실 그룹과 분자당 약 30 내지 약65개의 탄소원자를 갖는 주 직쇄지방족 선구물질 알코올과 에틸렌 옥시드가 축합됨에 의해 제조될 수 있는 화학구조를 갖고, n이 양의 정수인 화학구조-(CH2-CH2-O)n′을 갖는 각 분자의 부분중에 전체 중량의 20 내지 80%를 갖는 에톡실화된 알코올로부터 선택되는 것을 특징으로 하는 방법.
  11. 제10항에 있어서, 성분(A)는 스티렌 대 말레산 부분의 분자비가 1:1 내지 3:1인 중합체로부터 선택되고 성분(A) 대 (B)의 중량비의 범위가 약 6:1 내지 약 1:6인 것을 특징으로 하는 방법.
  12. 제11항에 있어서, 70℃의 온도에서 본발명에 따른 상기 윤활조성물상의 대기압에서 드라저 시험 장치에 의해 측정된 평형 과압의 NH3당량이 암모니아 당량의 25ppm이하인 것을 특징으로 하는 방법.
  13. 제12항에 있어서, (a) 성분 (D)는 (i)m이 약 16내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 1.3중량%의 범위로 물중에 용해될 수 있는 충분히 큰값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약1:40 내지 1:55의 범위로 제공되는 것을 특징으로 하는 방법.
  14. 제11항에 있어서, (a) 성분 (D)가 (i)m이 약 12내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.9중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분(D)는 약1:25 내지 약 1:7의 범위로 제공되는 것을 특징으로 하는 방법.
  15. 제10항에 있어서, (a) 성분 (D)는 (i)m이 약 12내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.4중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약1:10 내지 1:200의 범위로 제공되는 것을 특징으로 하는 방법.
  16. 제9항에 있어서, (a) 성분 (D)는 (i)m이 약 12내지 약 22의 정수인 구조-(CH2)m-를 갖는 부분 및 (ii)p가 전체 알코올이 적어도 약 0.1중량%의 범위로 물중에 용해될 수 있는 충분히 큰 값을 갖는 정수인 구조-(CH2-CH2-O)p을 갖는 부분을 포함하는 분자구조를 갖는 알코올과 인산의 부분적 에스테르와의염 및 부분적 에스테르로 이루어진 그룹으로부터 선택되고; (b)성분 (D)는 전체성분(A)와 (B)에 대한 중량비가 약1:25 내지 1:70의 범위로 제공되는 것을 특징으로 하는 방법.
  17. 제16항에 있어서, (a)냉간 가공하고자 하는 금속기재의 표면에, 상기 윤활조성물을 제공하기 전에 약 1 내지 약 50g/㎡의 양으로 피복하고 (ii) 냉간 가공전에 주변 공기중에서 피복을 수용액을 건조시킴에 의해 냉간 가공하고자 하는 금속기재의 표면상에 적용시키는 것을 특징으로 하는 방법.
  18. 제15항에 있어서, (a) 냉간 가공하고자 하는 금속기재의 표면에, 상기 윤활조성물을 제공하기 전에 약 1 내지 약 50g/㎡의 면적 밀도를 갖는 인산 아연 전환 피복물을 제공하고 (b) 상기 윤활 조성물을 (i) 약 6 내지 약 11의 pH범위를 갖고 전체 용해된 고체의 약 5 내지 20중량%를 포함하는 수용액 조성물을 냉간 가공하고자 하는 금속 기재 표면상에서 고체의 밀적밀도를 약 0.1 내지 약 8g/㎡의 양으로 피복하고, (ii) 냉간 가공전에 주변공기중에서 피복물 수용액을 건조함에 의해 냉간 가공하고자 하는 금속 기재의 표면상에 적용시키는 것을 특징으로 하는 방법.
  19. 제16항에 있어서, (a) 냉간 가공하고자 하는 금속기재의 표면에, 상기 윤활조성물을 제공하기 전에 약 1 내지 약 20g/㎡의 면적 밀도를 갖는 인산 아연 전환 피복물을 제공하고 (b) 상기 윤활 조성물을 (i) 약 7.5 내지 약 9의 pH범위를 갖고 전체 용해된 고체의 약 8 내지 12중량%를 포함하는 수용액 조성물을 냉간 가공하고자 하는 금속 기재 표면상에서 고체의 밀적밀도를 약 2.0 내지 약 6g/㎡의 양으로 피복하고, (ii) 냉간 가공전에 주변공기중에서 피복물 수용액을 건조함에 의해 냉간 가공하고자 하는 금속 기재의 표면상에 적용시키는 것을 특징으로 하는 방법.
  20. 제13항에 있어서, (a) 냉간 가공하고자 하는 금속기재의 표면에, 상기 윤활혼합물을 제공하기 전에 약 2 내지 약 15g/㎡의 면적 밀도를 갖는 인산 아연 전화 피복물을 제공하고 (b) 상기 윤활 조성물을 (i) 약 7.5 내지 약 9의 pH범위를 갖고 전체 용해된 고체의 약 8 내지 12중량%를 포함하는 수용액 혼합물을 냉간 가공하고자 하는 금속 기재표면상에서 고체의 면적밀도를 약 2.0 내지 약 6g/mℓ의 양으로 피복하고, (ii) 냉간 가공전에 주변공기중에서 피복물 수용액을 건조함에 의해 냉간 가공하고자 하는 금속 기재의 표면상에 적용시키는 것을 특징으로 하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019920004722A 1991-03-22 1992-03-21 금속의 냉연을 위한 윤활조성물 및 윤활방법 KR920017733A (ko)

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