KR890700569A - 3-클로로-4-폴로로니트로벤젠의 제법 - Google Patents
3-클로로-4-폴로로니트로벤젠의 제법Info
- Publication number
- KR890700569A KR890700569A KR1019880700728A KR880700728A KR890700569A KR 890700569 A KR890700569 A KR 890700569A KR 1019880700728 A KR1019880700728 A KR 1019880700728A KR 880700728 A KR880700728 A KR 880700728A KR 890700569 A KR890700569 A KR 890700569A
- Authority
- KR
- South Korea
- Prior art keywords
- chloro
- iodine
- antimony
- preparation
- poloronitrobenzene
- Prior art date
Links
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 4
- 239000011630 iodine Substances 0.000 claims 4
- 229910052740 iodine Inorganic materials 0.000 claims 4
- 150000002497 iodine compounds Chemical class 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- NTBYINQTYWZXLH-UHFFFAOYSA-N 1,2-dichloro-4-nitrobenzene Chemical compound [O-][N+](=O)C1=CC=C(Cl)C(Cl)=C1 NTBYINQTYWZXLH-UHFFFAOYSA-N 0.000 claims 1
- WFQDTOYDVUWQMS-UHFFFAOYSA-N 1-fluoro-4-nitrobenzene Chemical compound [O-][N+](=O)C1=CC=C(F)C=C1 WFQDTOYDVUWQMS-UHFFFAOYSA-N 0.000 claims 1
- DPHCXXYPSYMICK-UHFFFAOYSA-N 2-chloro-1-fluoro-4-nitrobenzene Chemical compound [O-][N+](=O)C1=CC=C(F)C(Cl)=C1 DPHCXXYPSYMICK-UHFFFAOYSA-N 0.000 claims 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims 1
- 229910052787 antimony Inorganic materials 0.000 claims 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims 1
- 150000001463 antimony compounds Chemical class 0.000 claims 1
- VMPVEPPRYRXYNP-UHFFFAOYSA-I antimony(5+);pentachloride Chemical compound Cl[Sb](Cl)(Cl)(Cl)Cl VMPVEPPRYRXYNP-UHFFFAOYSA-I 0.000 claims 1
- DAMJCWMGELCIMI-UHFFFAOYSA-N benzyl n-(2-oxopyrrolidin-3-yl)carbamate Chemical compound C=1C=CC=CC=1COC(=O)NC1CCNC1=O DAMJCWMGELCIMI-UHFFFAOYSA-N 0.000 claims 1
- 238000005660 chlorination reaction Methods 0.000 claims 1
- 229960002089 ferrous chloride Drugs 0.000 claims 1
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 claims 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/13—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups
- C07C205/26—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups and being further substituted by halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C62/00—Compounds having carboxyl groups bound to carbon atoms of rings other than six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
Abstract
내용 없음.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (3)
- (1)요오드 또는 요오드화합물과 철 그렇지 않으면 철화합물이나, (2) 요오드 또는 요오드화합물과 안티몬 또는 안티몬화합물의 존재하에서 4-플로로니트로벤젠을 염소화하는 것을 특징으로 하는 3-클로로-4-플로로니트로벤젠의 제법.
- 제1항에 있어서 요오드 및 염화제 1철 또는 염화 제2 철의 존재하에서 염소화하는 것을 특징으로 하는 3-클로로-4-플로로니트로 벤젠의 제법.
- 제1항에 있어서, 요오드 및 3염화안티몬 또는 5염화안티몬의 존재하에 염소화하는 것을 특징으로 하는 3-클로로-4-클로로니트로벤젠의 제법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP87-68792 | 1987-03-25 | ||
JP62068792A JPH0780818B2 (ja) | 1987-03-25 | 1987-03-25 | 3−クロロ−4−フロロニトロベンゼンの製法 |
JP8975187A JPH0764793B2 (ja) | 1987-04-14 | 1987-04-14 | フルオロモノニトロベンゼン類の製法 |
JP87-89751 | 1987-04-14 | ||
PCT/JP1988/000283 WO1988007519A1 (en) | 1987-03-25 | 1988-03-18 | Process for preparing 3-chloro-4-fluoronitrobenzene |
Publications (2)
Publication Number | Publication Date |
---|---|
KR890700569A true KR890700569A (ko) | 1989-04-25 |
KR940011129B1 KR940011129B1 (ko) | 1994-11-23 |
Family
ID=26409977
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019880700728A KR940011129B1 (ko) | 1987-03-25 | 1988-03-18 | 3-클로로-4-플루오로니트로벤젠의 제법 |
Country Status (5)
Country | Link |
---|---|
US (1) | US4898996A (ko) |
EP (2) | EP0551144B1 (ko) |
KR (1) | KR940011129B1 (ko) |
DE (2) | DE3885823T2 (ko) |
WO (1) | WO1988007519A1 (ko) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4898996A (en) | 1987-03-25 | 1990-02-06 | Nippon Kayaku Kabushiki Kaisha | Process for producing 3-chloro-4-fluoronitrobenzene |
ES2059184T3 (es) * | 1991-10-11 | 1994-11-01 | Hoechst Ag | Procedimiento para la preparacion de 2,4-diclorofluorobenceno. |
DE4411064A1 (de) * | 1994-03-30 | 1995-10-05 | Bayer Ag | Verfahren zur adiabatischen Herstellung von Mononitrohalogenbenzolen |
CN1044899C (zh) * | 1994-12-29 | 1999-09-01 | 浙江大学 | 2.4-二氯氟苯制备方法 |
CN103180272B (zh) * | 2010-11-26 | 2015-03-18 | 北京大学 | 用于芳族化合物的超声辅助氯化的方法 |
CN106631811A (zh) * | 2016-11-23 | 2017-05-10 | 山东友帮生化科技有限公司 | 一种3‑氯‑4‑氟硝基苯的制备方法 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2256999A (en) * | 1939-03-08 | 1941-09-23 | Du Pont | Nitration of organic compounds |
US3005031A (en) * | 1958-09-30 | 1961-10-17 | Du Pont | Process for chlorinating nitro aromatic hydrocarbons |
CH522585A (de) * | 1970-04-29 | 1972-06-30 | Grupul Ind De Petrochimie Borz | Verfahren zur Herstellung von Metachlornitrobenzol |
US4021498A (en) * | 1975-12-09 | 1977-05-03 | American Cyanamid Company | Adiabatic process for nitration of nitratable aromatic compounds |
DE3006685C2 (de) * | 1980-02-22 | 1982-09-09 | Riedel-De Haen Ag, 3016 Seelze | 3-Brom-4-fluorbenzonitril und Verfahren zur Herstellung eines substituierten 3-Brom-4-fluorbenzols |
DE3128442A1 (de) * | 1981-07-18 | 1983-02-03 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von 2-chlor-4-nitrotoluol |
JPS58222040A (ja) * | 1982-06-18 | 1983-12-23 | Central Glass Co Ltd | メタ−クロロベンゾトリフルオリドの製造方法 |
US4453027A (en) * | 1982-12-10 | 1984-06-05 | Monsanto Company | Adiabatic process for the nitration of halobenzenes |
US4898996A (en) | 1987-03-25 | 1990-02-06 | Nippon Kayaku Kabushiki Kaisha | Process for producing 3-chloro-4-fluoronitrobenzene |
-
1988
- 1988-03-18 US US07/229,175 patent/US4898996A/en not_active Expired - Lifetime
- 1988-03-18 KR KR1019880700728A patent/KR940011129B1/ko not_active IP Right Cessation
- 1988-03-18 WO PCT/JP1988/000283 patent/WO1988007519A1/ja not_active Application Discontinuation
- 1988-03-18 DE DE88902565T patent/DE3885823T2/de not_active Revoked
- 1988-03-18 EP EP93102299A patent/EP0551144B1/en not_active Expired - Lifetime
- 1988-03-18 DE DE3855937T patent/DE3855937T2/de not_active Expired - Fee Related
- 1988-03-18 EP EP88902565A patent/EP0307481B1/en not_active Revoked
Also Published As
Publication number | Publication date |
---|---|
DE3885823T2 (de) | 1994-04-14 |
KR940011129B1 (ko) | 1994-11-23 |
WO1988007519A1 (en) | 1988-10-06 |
US4898996A (en) | 1990-02-06 |
EP0551144B1 (en) | 1997-06-04 |
DE3855937T2 (de) | 1997-09-18 |
EP0307481A1 (en) | 1989-03-22 |
EP0307481B1 (en) | 1993-11-24 |
EP0307481A4 (en) | 1991-01-30 |
DE3855937D1 (de) | 1997-07-10 |
DE3885823D1 (de) | 1994-01-05 |
EP0551144A1 (en) | 1993-07-14 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
DE3885826D1 (de) | Verfahren zur Herstellung von in den Benzolringen chloriertem Tricyclo[8.2.2.2]hexadeca-4,6,10,12,13,15-hexaen. | |
GB1456830A (en) | Substituted undecanes | |
ATE38992T1 (de) | Herstellung von uebergangsmetallkomplexen. | |
FI96412C (fi) | Menetelmä ferrikloridin valmistamiseksi laimennetusta kloorivetyhaposta lähtemällä | |
AU514228B2 (en) | Recovering chlorine valves from iron chloride | |
KR890700569A (ko) | 3-클로로-4-폴로로니트로벤젠의 제법 | |
KR950702507A (ko) | 염화 제이철의 제조방법(process for the preparation of ferric chloride) | |
IT7922083A0 (it) | Processo per la produzione di cloro e ossido di ferro da cloruro ferrico. | |
IT7922082A0 (it) | Processo e apparato per produrre cloro e ossido di ferro da cloruro ferrico. | |
KR910000530A (ko) | 염화마그네슘의 제조방법 | |
GB1381472A (en) | 2,2,2-trichloro-4,-tert-butylacetophenone | |
GB1490677A (en) | Process for the preparation of 2,5-dichlorotoluene | |
DE3685284D1 (de) | Chlorieren von eisenhaltigen metallstoffen. | |
KR860002446A (ko) | 2,4-디클로로-5-플루오로-벤조산의 제조방법 | |
JPS525617A (en) | Wear resistant cast iron | |
IT8026464A0 (it) | Processo per la separazione di impurezze, a base di ferro, alluminio e manganese da soluzioni cloridriche di cloruro di magnesio. | |
IT1089008B (it) | Procedimento di produzione di ossido di alluminio contenente dallo 0,01% al 25% di ossido di cromo e/oppure di ossido di ferro | |
FR2389603A1 (ko) | ||
KR880011058A (ko) | 카르복실산 또는 카르복실산 할로겐화물 그룹을 트리할로메틸 그룹으로 전환시키는 방법 | |
PL199935A1 (pl) | Sposob sterowania procesem swiezenia stali o zawartosci wegla 0,1-0,8% | |
KR880010698A (ko) | 해조류 가공법 | |
KR830005087A (ko) | 염소처리에 의한 4-메톡시벤조일 클로라이드의 개선된 제조방법 | |
KR830004290A (ko) | 3-하이드라지노-6-py-피리다진이나 그의 산부가염의 제조방법 | |
GB1183006A (en) | Regeneration of Etchant. | |
JPS51151295A (en) | Process for production of chlorine dioxide |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A201 | Request for examination | ||
G160 | Decision to publish patent application | ||
E701 | Decision to grant or registration of patent right | ||
GRNT | Written decision to grant | ||
FPAY | Annual fee payment |
Payment date: 19970902 Year of fee payment: 4 |
|
LAPS | Lapse due to unpaid annual fee |