KR880003857A - 독립 다결정물질을 구비하는 합성물의 제조방법 - Google Patents
독립 다결정물질을 구비하는 합성물의 제조방법 Download PDFInfo
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- KR880003857A KR880003857A KR870010273A KR870010273A KR880003857A KR 880003857 A KR880003857 A KR 880003857A KR 870010273 A KR870010273 A KR 870010273A KR 870010273 A KR870010273 A KR 870010273A KR 880003857 A KR880003857 A KR 880003857A
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- polycrystalline material
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- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Glass Compositions (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명의 공정이 이루어질 수도 있는 반응 용기의 횡단면도.
제2도는 여러가지 상들을 분명히 도시하기 위해서 크게 확대한 부분적으로 침투된 충전재의 일부를 통과하는 제1도의 선 A-A에 관한 단면도.
제3도는 기질이 세라믹인 본 발명의 공정에 의해 얻어지는 다결정 합성물의 현미경의 사진.
제4도는 다공성 산화반응생성물에 의해 부분적으로 채워지는 내부입자 채널들과 모금속 침투를 개시한 직후의 제3도의 합성물 구조의 현미경 사진.
제5도는 기질이 금속인 본 발명의 공정으로 얻어지는 다결정 합성물의 현미경 사진.
Claims (33)
- 용융 모금속과 증기상 산화제의 산화반응으로 얻어지는 독립다결정 물질을 구비하는 합성물의 제조방법에 있어서, 상기 방법이 ⒜모금속을 선택하는 단계,⒝산화분위기에서 상기 모금속을 용융점 이상의 온도로 가열하고 만들어진 용융금속체를 중간입자 공극용적을 나타내는 충전재의 투과층과 접촉시키는 단계, ⒞(ⅰ)상기 충전재의 상기 용융금속으로의 침투 및 (ⅱ)산화반응이 충전재의 침투층의 입자간 공극용적의 최소한 일부에서 산화제와 용융모금속 사이에서 발생해서 산화반응 생성물이 상기 침투층내에 형성되고 만약있다면 모금속중 산화되지 않은 부분이 충전재입자들에 삽입하는 기질을 제공하게끔 상기 산화반응과 상기 금속침투의 상대속도를 제어하는 조건하에서 상기 금속과 상기 증기상 산화제의 산화반응하기에 충분한 시간 동안 상기 온도를 유지시키는 단계 및 ⒟상기 합성물을 회복시키는 단계들을 구비하는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항에 있어서 충전재의 침투층이 내부입자 공급용적을 나타내며, 모금속 산화반응 생성물의 입자간 공극 용적과 침투층의 내부입자 공극용적내에서 발생하는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물을 제조하는 방법
- 제2항에 있어서 충전재 입자들의 총 기공률이 20-80%범위내에 있는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제3항에 있어서 상기 기공률이 약 50%인 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 제2항에 있어서, 상기 충전재가 결합되지 않은 입자들의 충전층으로 이루어지는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 제2항에 있어서, 충전재가 결합된 입자들의 예비성형체로 이루어지는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제6항에 있어서 충전재가 스폰지타입의 구조로 이루어지는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제5항에 있어서 결합되지 않은 입자들이 위스커, 로드 또는 혈소판의 형태인 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 제2항에 있어서 유체정압이 상기 침투속도를 제어하기 위해 ⒞단계 중에 상기 용융 모금속체에 가해지는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제9항에 있어서, 상기 압력이 침투속도를 증가시키기 위해 상기 용융 모금속체에 적용가스압력에 의해 증가되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제9항에 있어서, 상기 압력이 상기 용융 모금속체와 통하는 라이저안의 용융모금속기둥에 의해 증가되고, 상기 라이저안의 상기 금속이 상기 용융금속체의 표면보다 더 높은 표면을 가지고 있는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 제2항에 있어서, 유체정압이 상기 침투속도를 감소시키기 위해 1기압보다 적게 감소되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제12항에 있어서 거기에서 접촉하게 충전제밑에 상기 용융 금속체를 배치함으로써 상기 감소가 이루어지며, 중력과 모세관력이 반대인 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 제2항에 있어서, 상기 증기상 산화제의 분압이 0.1-1대기압으로 감소되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제14항에 있어서, 상기 감소된 분압이 상기 산화제를 불활성가스로 희석시킴으로써 이루어지는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제15항에 있어서, 상기 가스가 아르곤인 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제14항에 있어서 상기 감소된 분압이 밀봉된 챔버안에서 상기 공정을 수행함으로써 이루어지고, 상기 산화제가 상기 산화반응 중에 고상반응 생성물의 형성에 의해 그리고 제어된 속도로 상기 산화제를 상기 밀봉챔버안에 넣음으로서 소모되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 2항에 있어서, 상기 증기상 산화제의 분압이 상기 압력을 1-2기압으로 상승시키기 위한 수단을 가지는 압력용기 안에서 상기 공정을 수행함으로서 증가되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 제2항에 있어서, 상기 반응을 촉진시키기 위해서 첨가제가 상기 산화반응의 영역안으로 도입되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제19항에 있어서 상기 첨가제가 상기 모금속에 합금되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제18항에 있어서 상기 첨가제가 상기 모금속 표면위에 피막으로 제공되며, 상기 표면과 상기 충전재 사이에 위치하는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제18항에 있어서, 상기 첨가제가 상기 충전재와 혼합되는 입자형태로 제공되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제18항에 있어서, 상기 첨가제가 수성 또는 유성맥상매질에 뜨며, 상기 부유물이 상기 충전재 입자들의 표면피막으로 제공되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 제2항에 있어서, 상기 증기상 산화제가 질화제이며, 상기 합성물이 질화 모금속을 구비하고 있는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제24항에 있어서, 상기 모금속이 실리콘, 알루미늄 및 티타늄에서 선택되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제24항에 있어서, 상기 질화제가 고순도의 질소가스 또는 그 반응 화합물을 구비하는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제24항에 있어서, 상기 증기상 질화에 앞서, 흡수된 표면산소 및/또는 수분을 제거하기 위해 상기 충전재가 질소가스, 수소, 또는 불활성가스로 처리되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제27항에 있어서, 상기 처리가 1-5시간 동안 1550-1800℃에서 수행되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제27항에 있어서, 상기 충전재가 실리콘, 알루미늄 또는 티타늄의 질화물을 구비하는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제24항에 있어서 상기 충전재가 실리콘 또는 알루미늄 예비체 금속의 다공체의 증기상 질화에 의해 생성되는 질화규소 또는 질화알루미늄인 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제24항에 있어서, 상기 모금속이 실리콘이며, 구리와 철이 첨가제로 사용되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제29항에 있어서, 상기 모금속이 알루미늄이고, 마그네슘이 첨가제로 사용되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법
- 제1항 또는 제2항에 있어서, 모금속의 일부가 산화되고, 성질들에 소망의 변화를 가져오기 위해 상기 금속의 산화되지 않은 부분과 합금하도록 합금 첨가물들이 제공되는 것을 특징으로 하는 독립다결정 물질을 구비하는 합성물의 제조방법※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
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US4600481A (en) * | 1982-12-30 | 1986-07-15 | Eltech Systems Corporation | Aluminum production cell components |
DE3381519D1 (de) * | 1983-02-16 | 1990-06-07 | Moltech Invent Sa | Gesinterte metall-keramikverbundwerkstoffe und ihre herstellung. |
NZ211405A (en) * | 1984-03-16 | 1988-03-30 | Lanxide Corp | Producing ceramic structures by oxidising liquid phase parent metal with vapour phase oxidising environment; certain structures |
NZ212704A (en) * | 1984-07-20 | 1989-01-06 | Lanxide Corp | Producing self-supporting ceramic structure |
US4851375A (en) * | 1985-02-04 | 1989-07-25 | Lanxide Technology Company, Lp | Methods of making composite ceramic articles having embedded filler |
JPS6283378A (ja) * | 1985-10-07 | 1987-04-16 | トヨタ自動車株式会社 | 強化された窒化ケイ素焼結体の製造方法 |
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1986
- 1986-09-16 US US06/907,927 patent/US4824625A/en not_active Expired - Fee Related
-
1987
- 1987-09-01 DE DE8787630164T patent/DE3782304T2/de not_active Expired - Fee Related
- 1987-09-01 EP EP87630164A patent/EP0261055B1/en not_active Expired - Lifetime
- 1987-09-01 AT AT87630164T patent/ATE81647T1/de not_active IP Right Cessation
- 1987-09-08 FI FI873883A patent/FI873883A/fi not_active IP Right Cessation
- 1987-09-09 NZ NZ221750A patent/NZ221750A/xx unknown
- 1987-09-10 PL PL1987267690A patent/PL156554B1/pl unknown
- 1987-09-10 IL IL83858A patent/IL83858A/xx not_active IP Right Cessation
- 1987-09-11 AU AU78341/87A patent/AU600973B2/en not_active Ceased
- 1987-09-11 CS CS876608A patent/CS275617B6/cs unknown
- 1987-09-11 CN CN87106244A patent/CN1036191C/zh not_active Expired - Fee Related
- 1987-09-14 PH PH35813A patent/PH25259A/en unknown
- 1987-09-14 NO NO873827A patent/NO873827L/no unknown
- 1987-09-14 SU SU874203283A patent/SU1830057A3/ru active
- 1987-09-14 BG BG81169A patent/BG47031A3/xx unknown
- 1987-09-14 MX MX8313A patent/MX165196B/es unknown
- 1987-09-14 IE IE248087A patent/IE60943B1/en not_active IP Right Cessation
- 1987-09-15 HU HU874096A patent/HU204244B/hu not_active IP Right Cessation
- 1987-09-15 BR BR8704766A patent/BR8704766A/pt not_active IP Right Cessation
- 1987-09-15 ZA ZA876903A patent/ZA876903B/xx unknown
- 1987-09-15 DK DK481287A patent/DK169917B1/da not_active IP Right Cessation
- 1987-09-15 IN IN738/CAL/87A patent/IN168487B/en unknown
- 1987-09-15 CA CA000547461A patent/CA1307386C/en not_active Expired - Fee Related
- 1987-09-15 TR TR87/0623A patent/TR23693A/xx unknown
- 1987-09-15 PT PT85704A patent/PT85704B/pt not_active IP Right Cessation
- 1987-09-16 YU YU172387A patent/YU46715B/sh unknown
- 1987-09-16 KR KR1019870010273A patent/KR950008595B1/ko not_active IP Right Cessation
- 1987-09-16 JP JP62231977A patent/JP2612577B2/ja not_active Expired - Lifetime
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