KR860008130A - α-폴리할로케톡심의 제조방법 - Google Patents

α-폴리할로케톡심의 제조방법 Download PDF

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KR860008130A
KR860008130A KR1019860002741A KR860002741A KR860008130A KR 860008130 A KR860008130 A KR 860008130A KR 1019860002741 A KR1019860002741 A KR 1019860002741A KR 860002741 A KR860002741 A KR 860002741A KR 860008130 A KR860008130 A KR 860008130A
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alkyl
optionally substituted
halogen
alkoxy
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아담치-통휴
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윌리암이. 람버트 3세
롬엔드 하스캄파니
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Publication of KR860008130A publication Critical patent/KR860008130A/ko

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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/12—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reactions not involving the formation of oxyimino groups
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group; Thio analogues thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
    • A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • A01N37/48—Nitro-carboxylic acids; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
    • A01N43/08—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings with oxygen as the ring hetero atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
    • A01N47/06—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom containing —O—CO—O— groups; Thio analogues thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/24—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing the groups, or; Thio analogues thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32—Oximes
    • C07C251/62—Oximes having oxygen atoms of oxyimino groups esterified
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
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  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
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  • Agricultural Chemicals And Associated Chemicals (AREA)
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Abstract

내용 없음

Description

α-폴리할로케톡심의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (2)

  1. 약 0℃∼80℃온도의 비활성 용매 또는 용매 혼합물 내에서 염기 존재하에 하기 일반식(Ⅱ)의 옥심을 상기 옥심 단위 몰당 약 1∼1.2몰의 하기 일반식(Ⅲ) 화합물과 반응시킴을 특징으로 하는 하기 일반식(Ⅰ)의 알파-폴리할로케톡심의 제조방법.
    [식중, X 및 X′는 동일하거나 다른 할로겐이고; R은 메틸 또는 할로 메틸이며; R1은 1 또는 그 이상의 할로겐, 저급(C1∼C4) 알콕시, 시아노 또는 니트로로 임의 치환된 직쇄 또는 측쇄(C1∼C12)알킬, (C3∼C6)시클로알킬, 1 또는 그 이상의 할로겐으로 임의 치환된 직쇄 또는 측쇄 저급 (C1∼C4)알콕시, 일반식 SR3로써, R3가 1 또는 그 이사의 동일하거나 다른 할로겐으로 임의 치환된 직쇄 또는 측쇄 저급(C1∼C4) 알킬 또는 아릴인티오기, 1 또는 그 이상의 할로겐으로 임의 치환된 직쇄 또는 측쇄저급(C2∼C6)알케필, 1 또는 그 이상의 동일하거나 다른 할로겐, 시아노, 니트로, 저급 (C1∼C4)알킬, 저급(C1∼C4)알콕시 또는 저급(C|1∼C4)할로겐알킬로 임의 치환된 아릴, 복소환, 알킬잔기가 1∼4개의 탄소원자를 갖고, 및 페필고리가 1 또는 그 이상의 동일하거나 다른 할로겐, 시아노, 니트로, 저급(C1∼C4) 알킬, 저급(C1∼C4) 알콕시 또는 저급(C1∼C4) 할로 알킬로 임의 치환된 펜알킬, 알케닐잔기가 2∼5개의 탄소원자를 갖고, 및 페필고리가 1 또는 그 이상의 동일하거나 다른 할로겐, 시아노, 니트로, 저급(C1∼C4)알킬, 저급(C1∼C4)알콕시 또는 저급(C1∼C4)할로알킬로 임의 치환된 펜알케필, 1 또는 그 이상의 동일하거나 다른 할로겐, 시아노, 니트로, 저급(C1∼C4) 알킬, 저급(C1∼C4)알콕시 또는 저급(C|1∼C4)할로 알킬로 임의 치환된 페녹시 또는 페필 고리가 1 또는 그 이상의 동일하거나 다른 할로겐, 시아노, 니트로, 저급(C1∼C4)알킬, 저급(C1∼C4)알콕시 또는 저급(C1∼C4)할로 알킬로 임의 치환된 벤질 옥시이고; 및 Z는 할로겐, 바람직하기로는 염소, 또는 OCOR1으로써, R1는 상술한 것과 같다]
  2. 약 0℃∼110℃의 비활성 용매 또는 용매혼합물 내에서 촉매 존재하에 하기 일반식(Ⅱ)의 옥심을 상기 옥심단위 몰당 약 1∼4몰의 하기 일반식(Ⅳ)의 이소시아네이트와 빈응시킴을 특징으로 하는 하기 일반식(Ⅰ)의 알파-폴리할로케톡심의 제조방법.
    (식중, X 및 X′는 동일하거나 다른 할로겐이고; R은 메틸 또는 할로메틸이며; 및 R1은 일반식 NHR2로써, R2가 수소, 1 또는 그 이상의 동일하거나 다른 할로겐으로 임의 치환된 직쇄 또는 측쇄저급(C1∼C4)알킬, (C3∼C6)시클로알킬, 직쇄 또는 측쇄(C2∼C6)알케필 또는 아릴인 아미노기이다)
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019860002741A 1985-04-12 1986-04-11 α-폴리할로케톡심의 제조방법 KR860008130A (ko)

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US72255685A 1985-04-12 1985-04-12
US722556 1985-04-12

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EP (1) EP0198687A3 (ko)
JP (1) JPS61267543A (ko)
KR (1) KR860008130A (ko)
CN (1) CN86102353A (ko)
AU (1) AU5577286A (ko)
BR (1) BR8601647A (ko)
DK (1) DK167486A (ko)
ES (1) ES8708209A1 (ko)
FI (1) FI861549A (ko)
GR (1) GR860937B (ko)
IL (1) IL78461A0 (ko)
NO (1) NO861388L (ko)
NZ (1) NZ215752A (ko)
PH (1) PH22191A (ko)
PT (1) PT82376B (ko)
ZA (1) ZA862698B (ko)

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IL99078A0 (en) * 1990-08-06 1992-07-15 Du Pont Bis-(hydroximidoyl chloride)derivatives,fungicidal compositions containing them and their use as fungicides

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DE2631522A1 (de) * 1976-07-14 1978-01-19 Bayer Ag Oximcarbamate fluorierter ketone, verfahren zu ihrer herstellung und ihre verwendung als insektizide, akarizide und nematizide

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FI861549A0 (fi) 1986-04-11
PH22191A (en) 1988-06-28
GR860937B (en) 1986-08-07
PT82376B (pt) 1988-05-27
NO861388L (no) 1986-10-13
DK167486D0 (da) 1986-04-11
JPS61267543A (ja) 1986-11-27
FI861549A (fi) 1986-10-13
AU5577286A (en) 1986-10-16
EP0198687A3 (en) 1987-09-23
ES553934A0 (es) 1987-10-01
ES8708209A1 (es) 1987-10-01
BR8601647A (pt) 1986-12-16
EP0198687A2 (en) 1986-10-22
ZA862698B (en) 1988-05-25
DK167486A (da) 1986-10-13
PT82376A (en) 1986-05-01
CN86102353A (zh) 1986-10-08
NZ215752A (en) 1989-10-27
IL78461A0 (en) 1986-08-31

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