KR860008124A - 알카노일 아닐리드의 제조방법 - Google Patents

알카노일 아닐리드의 제조방법 Download PDF

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KR860008124A
KR860008124A KR1019860002563A KR860002563A KR860008124A KR 860008124 A KR860008124 A KR 860008124A KR 1019860002563 A KR1019860002563 A KR 1019860002563A KR 860002563 A KR860002563 A KR 860002563A KR 860008124 A KR860008124 A KR 860008124A
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페터 가유스키 로버트
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일라이 릴리 앤드 캄파니
메어리 앤 턱커
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Abstract

내용 없음

Description

알카노일 아닐리드의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. 활성제로서, 구조식(Ⅰ),(Ⅱ), 또는 (Ⅲ)의 알카노일 아닐리드와 그 나트륨, 칼륨 및 구조식(Ⅳ)의 암모늄염류를 함유하는 농여화학적 조성물 :
    상기식에서 R0는 브로모, 클로로, 또는 플루오르이고; R1은
    CF3, C2F5, C3F7또는 하나의 n-, iso-, 또는 sec-E4F9; R2는 CF3, C2F5, C3F7, 또는, R0가 플루오로인 경우 R2는 아울러 -ORf, -N(Rf)2, -CN, -CF2-ORf, 또는 -CF2-N(Rf)2이고 각 Rf는 독립적으로 C1-C3의 퍼플루오로저급알킬, 또는 -N(Rf)2,에서 Rf모두 N과 결합하여 퍼플루오로 피롤리디노, 피플루오로피페리디노, 피플루오로모르폴리디노, 또는 N-(트리플루오로메틸)퍼플루오로피페라지노이고; R3는 수소, 또는 메틸; 그리고 R4는 (1) p-니트로기, 또는 (2) 2-5개의 독립적으로선택된 R5기, 여기서 R5는 브로모, 클로로, 또는 플루오로이다, 또는 (3) 2개의 독립적으로 선택된 R6기, 여기서 R6는 요도, 니트로, 시아노, 트리플루오로메틸, 플루오로메틸, 플루오로설포닐, 메틸설포닐, 에틸설포닐, 카르보메톡시, 또는 카르보에톡시이다, 또는 (4) 1개의 R5기와 1개의 R6기를 포함하는 2개의 기들, 또는 (5) 1개의 메틸기와 1개의 R5또는 니트로를 포함하는 2개의 기들, 또는 (6) 1개의 메틸기와 1개의 플루오로설포닐기를 포함하는 2개의 기들, 또는 (7) 2개의 독립적으로 선택된 R5기와 1개의 R6기를 포함하는 3개의 기들, 또는 (8) 2개의 독립적으로 선택된 R6기와 1개의 R5기를 포함하는 3개의 기들, 또는 (9) 2개의 니트로기와 1개의 트리프루오로메틸기를 포함하는 3개의 기들, 또는 (10) 2-, 4-위치에서의 2개의 니트로기와 3-, 또는 5-위치에서의 C1-C4알콕시 또는 C1-C4알킬티오기를 포함하는 3개의 기들, 또는 (11) 1개의 티오시아토기 그리고 R5, 요도 및 니트로중에서 선택된 1개의 기를 포함하는 2개의 기들, 또는 R4는 2 또는 3개의 독립적으로 선택된 R5또는 R6기로 치환된 나트틸기, 또는 R4는 5-니트로-2-피리딜이다;
    상기식에서 각 R8은 독립적으로 C1-O20알킬, 벤질, 2-하이드록시에틸, 2-하이드록시프로필, 또는 3-하이드록시프로필; 그리고 R9은 수소 또는 R8이며, 모든 R8과 R9잔여기에서는 전체 탄소 원자수는 12-60인데, 하나 이상의 R8이 2-하이드록시에틸, 2-하이드록시프로필, 또는 3-하이드록시프로필이면 모든 R8과 R9잔여기에서의 전체 탄소 원자수는 6-60이 된다.
  2. 제1항에서, 활성제가 제1항에서 기술된 구조식(Ⅰ) 또는 (Ⅱ)의 알카노일 아닐리드; 여기서 R1은 CF3, C2F5, C3F7또는 n-E4F9; R2은 CF3, C2F5, C3F7또는 n-E4F9이고, 만약 R0가 플루오로이면, R2는 아울러 -ORf, -N(Rf)2, 또는 -CN이며 각 Rf는 독립적으로 C1-C3의 퍼플루오로저급알킬이고; 그리고 R4는 만약 (6),(10) 또는 (11)절에서 정의도지 않으면 제1항에서 정의한 바와같다, 또는 나트륨, 칼륨 또는 염류인 농여화학적 조성물.
  3. 제1항에서 활성제가 제1항에서 기술된 구조식(Ⅰ) 또는 (Ⅱ)의 알카노일 아닐리드; 여기서 R0는 플루오로이며 또는 그 나트륨, 칼륨 또는NR9R9R9R9염인 농여화학적 조성물.
  4. 제1항에서, 활성제가 제1항에서 기술된 구조식(Ⅰ)의 알카노일 아닐리드; 여기서 R0는 풀루오로, R1은 CF3, C2F5, C3F7, 그리고 R3는 수소이며, 또는 그 나트륨, 칼륨, 또는NR9R9R9R9염인 농여화학적 조성물.
  5. 제1항에서, 활성제가 제1,2,3 또는 4항에서 기술된 구조식(Ⅰ)의 알카노일 아닐리드; 여기서 R4는 2-브로모-4-니트로페닐이며, 또는 그 나트륨, 칼륨, 또는NR9R9R9R9염인 농여화학적 조성물.
  6. 제1항에서, 활성제가 2´-브로모-4´-니트로-2,3,3,3-테트라플루오로-2-(트리플루오로메틸)프로피오나닐리드 또는 그 나트륨, 칼륨, 도는NR9R9R9R9염인 농여화학적 조성물.
  7. 활성성분으로서 제 1-6항중 어느 한항에서 정의된 바와같은 구조식(Ⅰ), (Ⅱ) 또는 (Ⅲ)의 알카노일아닐리드 또는 그 나트륨, 칼륨, 또는NR9R9R9R9염을 농학적으로 사용가능한 보조제와 함께 함유하는 살충작용 및 살지주작용 조성물.
  8. 활성성분으로서 제 1-6항중 어느 한항에서 정의된 바와같은 구조식(Ⅰ), (Ⅱ) 또는 (Ⅲ)의 알카노일아닐리드 또는 그 나트륨, 칼륨, 또는NR9R9R9R9염을 농학적으로 사용가능한 보조제와 혼합하여 함유하는 살충작용 및 제초작용 조성물.
  9. 제 1-6항중 어느 한항에서 정의된 바와같은 구조식(Ⅰ), (Ⅱ) 또는 (Ⅲ)의 알카노일아닐리드 또는 그 나트륨, 칼륨, 또는+NR9R9R9R9염의 효과용량을 곤충 또는 지주류의 기관에 투약하여 살충 또는 살지주류하는 방법.
  10. (a) 구조식 HNR3R4의 아민을 여기서 R3와 R4는 진술한 바와같다, 구조식 (CR0R1R2)COX, (CF3)3CCOX, 또는 (CF3)2(CH3)CCOX의 알카노일 할라이드와 반응시키거나, 또는 (B) 구조식 CF3-CF=CF2의 올레핀을 플루오라이드 존재하에서 구조식 0=C=NR4의 이소시아네이트와 반응시켜 구조식(Ⅰ)의 화합물을; 여기서 R0는 플루오로, R1과 R2는 CF3, 그리고 R3는 수소이다. 제조하거나, 또는 (c) 구조식(Ⅰ), (Ⅱ) 또는 (Ⅲ)의 화합물을; 여기서 R3는 수소이다, 메틸기화시켜 R3가 메틸기인 상응화합물을 제조하고, 그리고 (d) 화합물을 임의로 염류화시켜 그 나트륨, 카륨, 또는 염을 제조함을 포함하는 제1항에서 정의된 바와같은 구조식(Ⅰ), (Ⅱ), 또는 (Ⅲ)의 알카노일 아닐리드, 또는 그 나트륨, 칼륨, 또는 암모늄염을 제조하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019860002563A 1985-04-05 1986-04-04 알카노일 아닐리드의 제조방법 KR900006518B1 (ko)

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IL78392A (en) * 1985-04-05 1989-08-15 Lilly Co Eli Insecticidal compositions for inhibiting diabrotica larvae,comprising fluorinated cyclopentane(or hexane)carboxanilides
US4826841A (en) * 1985-04-05 1989-05-02 Eli Lilly And Company Alkanoyl anilides as pesticides
US4962284A (en) * 1985-04-05 1990-10-09 Eli Lilly And Company Alkanoyl anilides
GB8607033D0 (en) * 1986-03-21 1986-04-30 Lilly Industries Ltd Molluscicides
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DE2042300A1 (de) * 1970-08-26 1972-03-23 Farbwerke Hoechst AG, vormals Meister Lucius & Brüning, 6000 Frankfurt Halogencarbonsäureanilide, ihre Herstellung und Verwendung als Herbizide
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