KR860008095A - 나트륨 함유 유리 또는 세라믹 제품의 제조방법 - Google Patents

나트륨 함유 유리 또는 세라믹 제품의 제조방법 Download PDF

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KR860008095A
KR860008095A KR1019860000505A KR860000505A KR860008095A KR 860008095 A KR860008095 A KR 860008095A KR 1019860000505 A KR1019860000505 A KR 1019860000505A KR 860000505 A KR860000505 A KR 860000505A KR 860008095 A KR860008095 A KR 860008095A
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sodium
glass
product
vapor
compound
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KR1019860000505A
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English (en)
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로렌스 복코 피터
알렌 톰프슨 데이비드
조셉와인 윌리엄
Original Assignee
알프레드 엘, 마이클센
코오닝 글라스 워어크스
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Publication of KR860008095A publication Critical patent/KR860008095A/ko

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    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01—Manufacture of glass fibres or filaments
    • C03B37/012—Manufacture of preforms for drawing fibres or filaments
    • C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
    • C03B37/01413—Reactant delivery systems
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00—Other methods of shaping glass
    • C03B19/14—Other methods of shaping glass by gas- or vapour- phase reaction processes
    • C03B19/1415—Reactant delivery systems
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64—Burning or sintering processes
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00—Type of glass produced
    • C03B2201/06—Doped silica-based glasses
    • C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
    • C03B2201/32—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with aluminium
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00—Type of glass produced
    • C03B2201/06—Doped silica-based glasses
    • C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
    • C03B2201/50—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with alkali metals
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/04—Multi-nested ports
    • C03B2207/06—Concentric circular ports
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/04—Multi-nested ports
    • C03B2207/08—Recessed or protruding ports
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/04—Multi-nested ports
    • C03B2207/12—Nozzle or orifice plates
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/20—Specific substances in specified ports, e.g. all gas flows specified
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/30—For glass precursor of non-standard type, e.g. solid SiH3F
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/80—Feeding the burner or the burner-heated deposition site
    • C03B2207/85—Feeding the burner or the burner-heated deposition site with vapour generated from liquid glass precursors, e.g. directly by heating the liquid
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/80—Feeding the burner or the burner-heated deposition site
    • C03B2207/85—Feeding the burner or the burner-heated deposition site with vapour generated from liquid glass precursors, e.g. directly by heating the liquid
    • C03B2207/86—Feeding the burner or the burner-heated deposition site with vapour generated from liquid glass precursors, e.g. directly by heating the liquid by bubbling a gas through the liquid
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S65/00—Glass manufacturing
    • Y10S65/15—Nonoxygen containing chalogenides
    • Y10S65/16—Optical filament or fiber treatment with fluorine or incorporating fluorine in final product

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Structural Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Glass Compositions (AREA)
  • Glass Melting And Manufacturing (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Telescopes (AREA)
  • Exhaust Silencers (AREA)
  • Heat Treatment Of Steel (AREA)

Abstract

내용 없음

Description

나트륨 함유 유리 또는 세라믹 제품의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명에 유용한 나트륨 플루오로알콕시드 화합물의 열중량 분석곡선.
제2도는 본 발명의 실시에 적합한 장치의 개요도.
제3도는 제2도의 버너면에 대한 단면 획대도.
도면의 부호 설명
10:증발기, 12:오일욕 가열기, 14:3목 유리용기, 16:배기 라인, 18:진공펌프, 20:가스공급기, 26:버너, 28:불꽃, 30:발포기, 33,35:유량제어기.

Claims (8)

  1. 나트륨 함유 유리 또는 세라믹 제품의 제조를 위한 것으로서, (a) 증기상으로 서로 반응하여 증착유리 또는 세라믹용 조성물을 형성할 수 있고 그중의 하나가 나트륨 플루오로알콕시드 화합물인 적어도 2가지의 증발성 성분의 증기를 함유하는 증기 반응 혼합물을 생성하는 단계와, (b) 상기 증기 혼합물에 화학증착반응을 개시하여 미립의 나트륨 함유 증착생성물을 얻고 그 증착 생성물을 수집하는 단계 및, (c)증착생성물을 가열하여 적어도 일부를 나트륨 함유 유리 또는 세라믹 생성물로 소결하는 단계로 구성됨을 특징으로 하는 나트륨 함유 유리 또는 세라믹 제품의 제조방법.
  2. 제1항에 있어서, 상기 증발성 성분의 혼합물이 증기상으로 서로 반응하여 투화성 조성물로 생성하고, 나트륨 함유 증착 생성물을 가열하여 비다공성 나트륨 함유유리로 소결함을 특징으로 하는 나트륨 함유 유리 또는 세라믹 제품의 제조방법.
  3. 제2항에 있어서, 상기 유리가 Na2O와 SiO2를 구성하는 나트륨-도우핑 융합 실리카 유리임을 특징으로 하는 나트륨 함유 유리 또는 세라믹 제품의 제조방법.
  4. 제2항에 있어서, 상기 유리가 Na2O와 AI2O3및 SiO2를 구성하는 나트륨 알루미노실리케이트 유리인 것을 특징으로 하는 나트륨 함유 유리 또는 세라믹 제품의 제조방법.
  5. 제1항에서 제4항중 어느 한항에 있어서, 상기 나트륨 플루오로알콕시드 화합물이 250℃ 이하의 어느 온도에서 크게 분해되지 않고 증발될 수 있는 휘발성임을 특징으로 하는 나트륨 함유 유리 또는 세라믹 제품의 제조방법.
  6. 제5항에 있어서, 나트륨 플루오로알콕시드 화합물의 분자식이 Na-O-R 임을 특징으로 하는 나트륨 함유 유리 또는 세라믹 제품의 제조방법. O:산소, R:3∼5 탄소원자의 플루오로카아본 또는 플루오로히드로카아본기.
  7. 제6항에 있어서, 나트륨 플루오로알콕시드 화합물이 나트륨 헥사플루오로이소프로폭시드와 나트륨 퍼플루오로-t-부톡시드로 구성된 군에서 선정하는 것을 특징으로 하는 나트륨 함유유리 또는 세라믹 제품의 제조방법.
  8. 유리의 성분에 대한 증발원 화합물이 증발 및 서로 반응하여 고형의 미립 증착생성물을 생성하고, 이를 수집하여 유리로 소결하는 증착법에 의한 유리 제조에 있어서, 유리가 나트륨 함유 유리이며, 증발원 화합물에 증발성 나트륨 플루오로알콕시 화합물이 포함됨을 특징으로 하는 증착법에 의한 유리 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019860000505A 1985-04-22 1986-01-27 나트륨 함유 유리 또는 세라믹 제품의 제조방법 KR860008095A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US725,928 1985-04-22
US06/725,928 US4645524A (en) 1985-04-22 1985-04-22 Method for making sodium-containing glass

Publications (1)

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KR860008095A true KR860008095A (ko) 1986-11-12

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KR1019860000505A KR860008095A (ko) 1985-04-22 1986-01-27 나트륨 함유 유리 또는 세라믹 제품의 제조방법

Country Status (14)

Country Link
US (1) US4645524A (ko)
EP (1) EP0198980B1 (ko)
JP (1) JPH0637311B2 (ko)
KR (1) KR860008095A (ko)
AT (1) ATE72558T1 (ko)
AU (1) AU578505B2 (ko)
BR (1) BR8506567A (ko)
CA (1) CA1236854A (ko)
DE (1) DE3585390D1 (ko)
DK (1) DK563385A (ko)
ES (1) ES8800655A1 (ko)
FI (1) FI78890C (ko)
IN (1) IN166814B (ko)
NO (1) NO165912C (ko)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4767429A (en) * 1986-12-11 1988-08-30 American Telephone & Telegraph Co., At&T Bell Laboratories Glass body formed from a vapor-derived gel and process for producing same
US5069701A (en) * 1987-07-13 1991-12-03 Hughes Aircraft Company Preparation of fluoride glass by chemical vapor deposition
US4940477A (en) * 1989-07-19 1990-07-10 Corning Incorporated Method for synthesizing topaz
US5613995A (en) * 1993-04-23 1997-03-25 Lucent Technologies Inc. Method for making planar optical waveguides
US6849334B2 (en) * 2001-08-17 2005-02-01 Neophotonics Corporation Optical materials and optical devices
US6207522B1 (en) * 1998-11-23 2001-03-27 Microcoating Technologies Formation of thin film capacitors
KR20060124678A (ko) * 2003-12-12 2006-12-05 코닝 인코포레이티드 알칼리 도핑된 광섬유, 이의 예비성형체 및 이의 제조방법
US20060130530A1 (en) * 2004-12-21 2006-06-22 Anderson James G Method of doping silica glass with an alkali metal, and optical fiber precursor formed therefrom
GB2432371B (en) * 2005-11-17 2011-06-15 Epichem Ltd Improved bubbler for the transportation of substances by a carrier gas
CN101583891A (zh) * 2005-11-23 2009-11-18 康宁股份有限公司 低衰减非零色散位移光纤
US7848606B1 (en) 2008-03-13 2010-12-07 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Eliminating crystals in non-oxide optical fiber preforms and optical fibers
JP5898624B2 (ja) 2009-11-02 2016-04-06 シグマ−アルドリッチ・カンパニー、エルエルシー 蒸発器
EP3950611A1 (de) 2020-08-06 2022-02-09 Heraeus Quarzglas GmbH & Co. KG Alternative fluorierungsmittel zur herstellung von fluoriertem quarzglas
EP3950610A1 (de) 2020-08-06 2022-02-09 Heraeus Quarzglas GmbH & Co. KG Alternative fluorierungsmittel ii: fluosil und sootaufbau

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3883336A (en) * 1974-01-11 1975-05-13 Corning Glass Works Method of producing glass in a flame
US4021253A (en) * 1974-04-05 1977-05-03 Kms Fusion, Inc. Method for manufacturing glass frit
US4260406A (en) * 1978-08-17 1981-04-07 Corning Glass Works Gelled solder glass suspensions for sealing glass or ceramic parts
JPS5632344A (en) * 1979-08-25 1981-04-01 Nippon Telegr & Teleph Corp <Ntt> Manufacture of optical fiber base material
CA1166527A (en) * 1979-09-26 1984-05-01 Shiro Takahashi Method and apparatus for producing multi-component glass fiber preform
DE3031147A1 (de) * 1980-08-18 1982-03-18 Siemens AG, 1000 Berlin und 8000 München Verfahren zum herstellen von glas mit einem vorbestimmten brechzahlprofil und alkalifreies glas aus einem oxis eines grundstoffes, das mit einem oder mehreren weiteren stoffen dotiert ist
US4378987A (en) * 1981-10-15 1983-04-05 Corning Glass Works Low temperature method for making optical fibers
US4501602A (en) * 1982-09-15 1985-02-26 Corning Glass Works Process for making sintered glasses and ceramics
US4472510A (en) * 1982-12-23 1984-09-18 Dow Corning Corporation Carbon-containing monolithic glasses and ceramics prepared by a sol-gel process
JPS59184740A (ja) * 1983-04-05 1984-10-20 Shin Etsu Chem Co Ltd 光フアイバ−用石英系母材の製造方法
US4666247A (en) * 1985-02-08 1987-05-19 American Telephone And Telegraph Company, At&T Bell Laboratories Multiconstituent optical fiber
EP0223853A1 (en) * 1985-06-03 1987-06-03 Hughes Aircraft Company Method for introducing dopants in optical fiber preforms

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FI854955A (fi) 1986-10-23
JPS61247626A (ja) 1986-11-04
EP0198980B1 (en) 1992-02-12
NO165912B (no) 1991-01-21
AU5081285A (en) 1986-10-30
ES8800655A1 (es) 1987-11-16
US4645524A (en) 1987-02-24
ES554216A0 (es) 1987-11-16
EP0198980A2 (en) 1986-10-29
DE3585390D1 (de) 1992-03-26
DK563385A (da) 1986-10-23
FI78890C (fi) 1989-10-10
FI78890B (fi) 1989-06-30
BR8506567A (pt) 1987-02-17
NO165912C (no) 1991-05-02
JPH0637311B2 (ja) 1994-05-18
NO854922L (no) 1986-10-23
DK563385D0 (da) 1985-12-05
IN166814B (ko) 1990-07-21
EP0198980A3 (en) 1988-01-07
AU578505B2 (en) 1988-10-27
ATE72558T1 (de) 1992-02-15
CA1236854A (en) 1988-05-17
FI854955A0 (fi) 1985-12-13

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